WO1999000619A1 - Method and apparatus for on-line detection of leaky emergency shut down or other valves - Google Patents

Method and apparatus for on-line detection of leaky emergency shut down or other valves Download PDF

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Publication number
WO1999000619A1
WO1999000619A1 PCT/US1998/012868 US9812868W WO9900619A1 WO 1999000619 A1 WO1999000619 A1 WO 1999000619A1 US 9812868 W US9812868 W US 9812868W WO 9900619 A1 WO9900619 A1 WO 9900619A1
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WO
WIPO (PCT)
Prior art keywords
upstream
downstream
valve
seal
fluid
Prior art date
Application number
PCT/US1998/012868
Other languages
French (fr)
Inventor
Robert L. Leon
David Q. Heagerty
Original Assignee
Crane Nuclear, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Crane Nuclear, Inc. filed Critical Crane Nuclear, Inc.
Priority to DE69817821T priority Critical patent/DE69817821D1/en
Priority to AU81567/98A priority patent/AU8156798A/en
Priority to AT98931431T priority patent/ATE249000T1/en
Priority to EP98931431A priority patent/EP0991888B1/en
Publication of WO1999000619A1 publication Critical patent/WO1999000619A1/en
Priority to NO19996403A priority patent/NO320881B1/en
Priority to NO20055161A priority patent/NO335721B1/en

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • G01M3/28Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for pipes, cables or tubes; for pipe joints or seals; for valves ; for welds
    • G01M3/2876Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for pipes, cables or tubes; for pipe joints or seals; for valves ; for welds for valves
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16KVALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
    • F16K37/00Special means in or on valves or other cut-off apparatus for indicating or recording operation thereof, or for enabling an alarm to be given
    • F16K37/0025Electrical or magnetic means
    • F16K37/005Electrical or magnetic means for measuring fluid parameters
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16KVALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
    • F16K5/00Plug valves; Taps or cocks comprising only cut-off apparatus having at least one of the sealing faces shaped as a more or less complete surface of a solid of revolution, the opening and closing movement being predominantly rotary
    • F16K5/06Plug valves; Taps or cocks comprising only cut-off apparatus having at least one of the sealing faces shaped as a more or less complete surface of a solid of revolution, the opening and closing movement being predominantly rotary with plugs having spherical surfaces; Packings therefor
    • F16K5/0663Packings
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/04Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
    • G01M3/24Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using infrasonic, sonic, or ultrasonic vibrations

Abstract

A method and apparatus for on-line detection of leaky emergency shut down or other valves (10) in a fluid transport system having an upstream pipe, a downstream pipe and the valve (10) connected between the upstream pipe and the downstream pipe for controlling fluid flow through the system.

Description

TITLE OF THE INVENTION
Method and Apparatus for On-Line Detection of
Leaky Emergency Shut Down or Other Valves
CROSS REFERENCE TO RELATED APPLICATIONS
This application claims priority from Provisional Application number
60/055,728 filed June 26, 1997 and Provisional Application number 60/060,590 filed October
1, 1997.
BACKGROUND OF THE INVENTION
The present invention generally relates to the leak testing of Emergency Shut
Down valves, more commonly known as ESD valves. ESD valves are in use in many
commercial and industrial facilities and, in particular, are used on all or virtually all of the
approximately 2,000 off-shore oil and gas platforms around the world to isolate the platform
in the event of an emergency. The purpose of the present invention is to provide a means for
more easily determining, on-line, whether an individual ESD valve on such a platform or in
any other location or application might leak if called upon to close in an emergency or other
situation, and thus might fail to perform its intended isolation or other function. The need to
verify the integrity of ESD valves has been made more apparent by the Piper Alpha disaster in the British sector of the North Sea, which led to the sinking of a platform and a significant
loss of life in the late 1980's.
There are many different types of valves on each off-shore platform, and more
than ten such valves are ESD valves. The ESD valves are typically placed in a closed
position or condition only during normal or other production shutdowns, as well as during
emergencies. The majority of the ESD valves are ball valves, while most of the remainder of
the ESD valves are gate valves. On the platform, the ESD valves are usually situated in-line
or in series with other valves that are also closed off in emergency shutdown and production
shutdown situations. However, the ESD valve is considered to be the valve of last resort, the
valve that must perform and must provide isolation should all of the other in-line valves fail
to close or fail to fully close or to otherwise leak. Since the other upstream, in-line valves
usually do properly close and do not usually leak, and because in an emergency shutdown or
production shutdown situation, many of the other, in-line valves close before the ESD valve
closes, there is often no differential pressure applied across the ESD valve which could
produce a detectable leak. Thus, in emergency or production shutdown situations, commonly
used methods for detecting leaks in valves such as high frequency acoustic leak detection
cannot be used in most cases to identify a leaky ESD valve, and certainly cannot be used to
identify a partially leaky ESD valve. A partially leaky ESD valve is defined herein as an
ESD valve in which at least one, but not all, of the internal seals is leaky. Usually the other
seals, will prevent a partially leaky ESD valve from leaking, but it is still important to be able
to detect a partially leaky ESD valve because such an ESD valve could become a fully leaky
ESD valve in the next or some future closure attempt, and it would be wise to repair any such
ESD valve at the first available opportunity to prevent a possible leaky situation in the future. Presently on off-shore platforms, in order to identify leaky or partially leaky
ESD valves, platform operators sometime resort to pressurizing the inner cavity of each ESD
valve with nitrogen to see if the ESD valve can hold the pressure. This is usually
accomplished during costly (up to $300,000 per hour) production shutdowns. It would
certainly be better if a method and apparatus could be devised to identify leaky and partially
leaky ESD and other valves on-line during production, or during planned and unplanned
shutdowns, using equipment and techniques that don't involve costly and time consuming
additional steps such as injecting high pressure nitrogen.
The present invention provides a method and apparatus for on-line detection of
leaky and partially leaky ESD and other valves during actual production as well as during a
shutdown, and without employing additional steps such as the injection of nitrogen gas. The
method and apparatus of the present invention can be used on the majority of ESD valves that
are installed on off-shore platforms during actual production, enabling for the first time, leaky
and partially leaky ESD and other valves to be identified periodically and/or continuously
without any loss of production or associated costs. For all ESD valves, including the
remainder that can not be identified during production, the present invention can be employed
following a shutdown, either a planned or an unplanned shutdown. And as indicated before,
no additional steps are required.
The present invention involves the analysis of simultaneous dynamic signals
from one pressure transducer located in the cavity of the ESD or other valve and another
pressure transducer located upstream or downstream from the valve. On most platforms,
appropriate pressure taps are already in place on the ESD valves and on the valve piping. The
inventive principles, as hereinafter described, are based on combining an understanding of the design of ESD valves, with an understanding of the physical principles involved in the flow
of fluids through pipes and the transients that occur in the cessation of such flow, with an
understanding of how sound travels in fluid filled pipes, and finally with an understanding of
the processing of dynamic signals.
BRIEF SUMMARY OF THE INVENTION
Briefly stated, the present invention comprises a method and apparatus for on¬
line detection of leaky emergency shutdown or other valves. The apparatus is for use with a
fluid transport system having an upstream pipe, a downstream pipe and a valve connected
between the upstream pipe and the downstream pipe for controlling fluid flow through the
system. The valve has at least one upstream seal, at least one downstream seal and an inner
cavity effectively isolated by the seals from the fluid flow stream. The apparatus for
detecting a leak in at least one of the seals comprises a first transducer in fluid
communication with the fluid flow stream at at least one of: a predetermined distance
upstream of the upstream seal; and, a predetermined distance downstream of the downstream
seal. The first transducer is for sensing pressure pulsations resulting from at least one of:
dynamic energy due to fluid flow through the fluid transport system; and, transient energy
within the fluid in the transport system after the valve is closed and for generating
representative electrical signals as a function of time. A second transducer is in fluid
communication with the inner cavity for sensing substantially simultaneous pressure
pulsations within the inner cavity and for generating second representative electrical signals
as a function of time. An analyzer is provided for receiving the first and second electrical
signals and for generating at least one of a frequency response function, and a coherence
function. The generated function is sufficiently averaged to provide a meaningful measure of the degree to which the two electrical signals are related to thereby indicate whether, and to
what extent, sensed pressure pulsations within the fluid transport system are passed through
at least one of the seals to the inner cavity.
In one embodiment, the apparatus is employed for detecting and identifying
the location of a leak in at least one of the seals when the valve is closed. In this
embodiment, an external sound source is in fluid communication with the fluid transport
system for generating sound energy within the system. The first and second transducers are
for sensing pressure pulsations resulting from acoustic energy generated by the sound source.
Another embodiment involves a method for use with a fluid transport system
having an upstream pipe, a downstream pipe and a valve connected between the upstream
pipe and the downstream pipe for controlling fluid flow within the system. The valve has at
least one upstream seal, at least one downstream seal and an inner cavity effectively isolated
by the seals from the fluid flow stream. The method is for detecting the presence of a leak in
both of the seals when the valve is closed and a differential pressure exists across the valve.
The steps of the method comprise: determining the magnitude of the differential pressure
across the valve; sensing the presence of pressure pulsations within the inner cavity resulting
from fluid flowing through the seals into and out of the inner cavity and generating
representative electrical signals as a function of time; analyzing the electrical signals and
generating an auto spectrum representation; and using the auto spectrum representation in
conjunction with the determined differential pressure magnitude to indicate the existence and
extent of a leak. BRIEF DESCRIPTION OF THE DRAWINGS
The foregoing summary, as well as the following detailed description-of a
preferred embodiment of the invention, will be better understood when read in conjunction
with the appended drawings. For the purpose of illustrating the invention, there is shown in
the drawings particular arrangements and methodologies. It should be understood, however,
that the invention is not limited to the precise arrangements shown, or methodologies of the
detailed description. In the drawings:
Fig. 1 is a cross sectional elevational view of a ball-type emergency shutdown
valve (mostly commonly used on off-shore petroleum and gas platforms), shown in the open
position to allow fluid flow;
Fig. 2 is a cross sectional elevational view of a less commonly used ball-type
emergency shutdown valve, similar to the valve of Fig. 1, but modified to include a bleed
hole in the ball to equalize the pressure to the cavity space when the valve is in the open
position;
Fig. 3. is a cross sectional elevational view of a gate-type emergency shutdown
valve (least commonly used on off-shore petroleum and gas platforms), shown in the open
position to allow fluid flow;
Fig. 4 is a schematic diagrammatic illustration of the valve of Fig. 1 in the
open position with a section of upstream pipe and two pressure transducers;
Fig. 5 is a schematic diagrammatic illustration of the valve, pipe, and pressure
transducer arrangement of Fig. 4, but with the valve in the closed position;
Fig. 6a is a plot of the magnitude representation of the Frequency Response
Function (FRF) of the output of the two transducers of Fig. 4 as a function of frequency, over the range from I to 50 Hertz for various degrees of seal leakiness;
Fig. 6b is a plot of the coherence as a function of frequency from I to -50 Hertz
for various degrees of seal leakiness;
Fig. 7 is a view similar to Fig. 5 showing an alternate embodiment of the
invention;
Figs. 8a and 8b are plots similar to those of Figs. 6a and 6b made in
conjunction with the embodiment of Fig. 7; and
Figs. 9a and 9b are schematic block diagrams of an on-line system utilizing
the present invention.
DETAILED DESCRIPTION OF THE INVENTION
Fig. 1 is a cross sectional elevational view of the type of valve 10 used in most
ESD applications, illustrated in the open position. The valve 10 is a ball valve with a spring-
loading mechanism on each side (not shown) that pushes the two valve seats 12, 14 up
against the ball 16 in a manner well known in the art. The sealing of the valve seats 12, 14
against the ball 16 is accomplished by means of two generally annular elastomeric rings, one
ring 18 located in the upstream seat 12, and one ring 20 located in the downstream seat 14.
The spring-loading of the seats 12, 14 holds the elastomeric rings 18, 20 tightly against the
ball 16, even as these components wear. Because the seats 12, 14 can move, they also have to
be sealed against the valve body 22 and this is accomplished with two O-ring seals 24, 26,
one for each seat 12, 14.
The generally open space 28 between the valve body 22, and the seats 12, 14
and ball 16, is known as the inner valve cavity. The inner cavity or cavity 28 is generally
fluid filled, but is effectively isolated from the fluid stream flowing through the valve 10 by the upstream elastomeric ring 18 and O-ring 24, and by the downstream elastomeric ring 20
and O-ring 26, each in parallel for the purpose of providing such isolation. Thus if any one of
the elastomeric rings 20, 22 or O-rings 24, 26 doesn't seal perfectly, the isolation of the cavity
28 is compromised. Also in the closed position of the valve 10 (not shown), the cavity 28
remains isolated from the upstream fluid as long as both the upstream elastomeric ring 18 and
the upstream O-ring 24 afford a perfect seal, and remains isolated from the downstream fluid
as long as both the downstream elastomeric ring 20 and the downstream O-ring 26 afford a
perfect seal.
For the valve 10 to actually be leaky when closed, at least one of the two
upstream seals 18, 24 would have to leak and at least one of the two downstream seals 20, 26
would also have to leak to provide a complete leakage path through the cavity 28. Thus, a
test that is sensitive to even one leaky seal would be a conservative, yet valuable test. Such is
the case for the present practice of pressurized nitrogen injection into the cavity 28. If any
one of the seals 18, 20, 24, 26 leaks, the high pressure nitrogen leaks out of the cavity 28 and
the pressure reduction of the nitrogen within the cavity 28 is noted. The method and
apparatus of the present invention similarly identifies if any one of the seals 18, 20, 24, 26
leaks, but without requiring the additional and costly nitrogen injection procedure. The
method and apparatus of the present invention involves obtaining and analyzing test data to
determine if a leaky seal is present.
Fig. 2 is a cross sectional elevational view of a ball valve 110 similar to the
ball valve 10 of Fig. 1. Close examination, however, reveals a bleed hole 130 in the ball 116
which connects the fluid flow stream through the ball 116 to the cavity 128 while the valve
110 is in the open position as shown. The purpose of the bleed hole 130 is to equalize the pressure between the cavity 128 and the flow stream prior to valve closure. In valves known
as double block and bleed valves, if one seat seal leaks, the bleed hole provides additional
closing force for the other seat seal. Because the bleed hole 130 itself provides a fluid path
between the cavity 128 and the flow stream while the valve is in the open position, the effect
of the bleed hole 130 is to obviate the usage of the present invention to test the seals 118, 120,
124, 126 when the valve is in the open position. Ball valves 110 with bleed holes are not as
commonly used for ESD applications as are ball valves 10 without bleed holes.
Fig. 3 is a cross sectional elevational view of a slide type gate valve 210,
illustrated in the open position. While in the open position, the cavity 228 is isolated from
the fluid flow stream by the upstream and downstream seals 218, 220. In the closed position
(not shown), the upstream seal 218 isolates the cavity 228 from the fluid in the upstream pipe,
and the downstream seal 220 isolates the cavity 228 from the fluid in the downstream pipe.
This type of valve 210 is used sparingly in ESD applications.
Fig. 4 shows schematically a ball valve 10 without a bleed hole of the type
shown in Fig. 1. In Fig. 4, the single illustrated upstream seal 19 represents either of the
upstream seals 18, 24 of the actual valve 10 of Fig. 1, and the single illustrated downstream
seal 21 represents either of the downstream seals 20, 26 of the actual valve 10 of Fig. 1. The
valve 10 in Fig. 4 is illustrated in the open position. Shown are two pressure taps 29, 31, one
29 in the cavity and one 31 upstream of the inner cavity 20 of the valve 10. Note that the
upstream tap 31 could be replaced with a downstream tap located downstream of the inner
cavity 28 with no change in functionality. The taps 29, 31 are standard taps of a type
typically used on oil or gas platform rigs, and the open end of the tap is typically a standard
1/4 inch NPT fitting of a type well known in the art and capable of mating with a pressure transducer or pressure transducer adapter to provide fluid communication with the flow
stream or inner cavity 28 respectively. It is also useful to have a hand valve installed-above
the fitting location (not shown) so that transducers may be replaced when the line is filled and
pressurized. Also shown are two pressure transducers 30, 32 of a type well known in the art
and capable of sensing dynamic pressure and generating representative electrical signals, read
p as a function of time, or p(t). Such pressure transducers 30, 32 are of a type well known to
those skilled in the art and are often already in position on existing ESD valves. The
electrical signal p}(t) from the first pressure transducer 30 representing the upstream dynamic
pressure, and p2(t) from the second pressure transducer 32 representing the cavity dynamic
pressure are input to an analyzer (not shown) that is capable of digitizing and analyzing the
simultaneous signals in the frequency domain. The analyzer may be circuitry, software, or a
complete commercially available analyzer. One such commercially available analyzer in
fairly common use is the Hewlett Packard Model 5423.
When a ball-type ESD valve 10 is fully open and the fluid is flowing through
it, if none of the seals 19, 21 are leaky, the fluid in the inner cavity 28 of the valve 10 is
effectively isolated from the fluid flowing through the valve 10 and thus from the fluid in the
pipe either upstream or downstream from the valve 10. If any of the seals 19, 21 are leaky,
however, that isolation of the cavity 28 will be compromised. The greater the degree of
leakiness in the seals 19, 21, the greater the degree of compromise of the isolation of the
cavity 28.
A leaky seal condition is manifested by a transmission of the dynamic pressure
pulsations from the fluid flowing through the valve 10 to the fluid contained in its inner
cavity 28. The greater the degree of leakiness, and the lower the frequency of the pulsations, the greater the amount of the transmission of the pulsations into the cavity 28. The amount of
transmission can be quantified from the Frequency Response Function (FRF) (sometimes
called the transfer function) between the dynamic pressure in the cavity 28 as measured by
transducer 32 and the dynamic pressure in the pipe as measured by transducer 30. Two
frequency domain representations are useful in this regard. The first representation is the
FRF magnitude, indicating the relative energy in the two pressure signals as a function of
frequency. The second frequency domain representation is the coherence, indicating the
degree of similarity between the two pressure signals as a function of frequency. The second
representation is actually a measure of how constant the magnitude and phase relationship is
between the two pressure signals as a function of frequency. To see how constant something
is, successive traces over time need to be analyzed, and compared. That is accomplished
through a process called averaging. Exactly what frequency range the analysis should
encompass, and how much averaging is required depends upon the physical situation for a
particular valve or application.
The ideal frequency range for analysis is determined in part by the distance L
between the pressure transducer 30 and the valve cavity pressure transducer 32 or valve
cavity 28. In order not to have to worry about standing wave nodes at certain frequencies,
and the effects of multiple acoustic paths, the pressure transducer 30 should be no more than
a quarter wavelength from the valve cavity transducer 32. The wavelength is a function of
the speed of sound in the fluid and the upper frequency. The relationship is
λ _ 1 C 7 7
where λ is the wavelength, C is the speed of sound in the medium and F is the upper frequency. The speed of sound in petroleum at a temperature of 15°C is 4,367 feet per
second. Using that figure for C, and 50 Hz for the upper frequency (F) yields a quarter
wavelength of about 22 feet. The speed of sound in natural gas is less than 1,000 feet per
second. Keeping 50 Hz as the upper frequency (F) yields a quarter wavelength of about 5
feet. So frequencies up to 50 Hz are clearly acceptable if the upstream or downstream pipe
tap is kept to within 22 feet of the valve for oil, and to within 5 feet for gas. If one wishes to
increase the usable frequency range, or the pipe tap distances given above, or both, the effect
of nodal frequencies and multiple paths can be minimized by using the mean spectral values
over the spectral band. The pressure pulsations in the flow stream come about as a result of
turbulence in the flow. But occasionally with extremely high flow, highly localized
turbulence near one of the sensors can cause pulsations that overshadow the desired more
global pulsations, especially at low frequencies. Thus, extending the frequency range of
interest up to, or into, the 1,000 Hz region is sometimes desirable, but in no case would it be
necessary or desirable to extend it up to, or beyond 10,000 Hz. In any event, the sample rate
of each pressure signal, after anti-alias filtering, must be more than twice the maximum
frequency. If 50 Hz is to be the maximum frequency, a sample rate of 150 Hz could be used;
if 1000 Hz is the maximum frequency, then a 2,500 Hz sample rate is appropriate.
The required duration of each trace record to be used for averaging is
determined by the desired frequency resolution. The relationship is inverse. One second
yields one Hz resolution, two seconds yields one-half Hz resolution, etc. One Hz resolution
should be acceptable in most cases. As indicated previously, averaging of several trace
records over time is required to get a meaningful measure of the degree to which the two
signals are related and thereby indicating whether, and to what extent the pressure pulsations are passing through at least one of the seals to the inner cavity 28. Typically about 30
averages will suffice. The confidence in the result improves by the square root of the- number
of averages. So to double the confidence, one needs four times the number of averages. This
typically is not a problem for ESD valves without bleed holes that can be tested in the
production mode, where virtually unlimited averaging time is available.
However, this is not the case when the test data must be obtained immediately
following a shutdown. In a shutdown situation, the data acquisition time may be limited to
less than a minute because after that, the transient energy in the pipe might effectively
dissipate. ESD ball type valves such as valve 110 with bleed holes in the ball cannot be
tested in the production mode and can only be tested in a shutdown mode. This presents a
limit to the number of averages, which at one second per record seems like 60 averages for 60
seconds of data, or 30 averages for 30 seconds of data, etc. But overlap processing can be
used to improve that situation, so at even with one second per record, 120 averages can be
achieved for 60 seconds of data, and 60 averages can be achieved for 30 seconds of data, etc.
Fig. 5 shows schematically a ball valve 10 following closure. Fig. 5 represents
not only a ball valve 10 without a bleed hole as does Fig. 4, but also represents a ball valve
110 with a bleed hole. That is because when the valve 10 is in the closed position, the bleed
hole no longer provides a pathway from the pipe to the internal cavity 28, and so only the
seals 19, 21, if leaky, provide such a pathway. Thus, this is the same situation that exists for
ball valves without bleed holes in the open position. Where those valves without bleed holes
can be tested in the preferred open position production situation, those with bleed holes can
only be tested right after being placed in the closed position. In both situations, dynamic
energy is required to exist in the pipe. This will always be the case for oil or a mixture of oil and gas, for valves in the open position, production situation, but in the closed position
following a shutdown, such dynamic energy may only exist for a minute or less while all the
various fluid motions (not just the flow) and pressure fluctuations come to rest following
closure. Thus the time limits previously discussed.
Figs. 6a and 6b show the resulting averaged Frequency Response Function
(FRF) magnitude and the coherence function for various degrees of leakiness. The curves (X,
Y, Z, R, S, T) represent the analyzed results for data obtained in either mode, either the
production mode for ball type ESD valves 10 without bleed holes and ESD gate valves 210,
or immediately following shutdown mode for any of the types of ESD valves 10, 110, 210.
Fig. 6a shows different magnitude representations of the FRF, P2(f)/P,(f) for
different seal leakiness conditions. Here, P,(f) and P2 (f) are the complex frequency domain
representations of p,(t) and p2(t) respectively. For a valve with no leaky seals (curve X), the
magnitude of the FRF is seen to start out fairly high at very low frequency, but then it
plummets to a very low value and stays there at higher frequencies. The fairly high value at
very low frequency is due to the very low frequency motions of the platform and the pipe and
valve assembly which cause similar, but not equal, low frequency pressure fluctuations in
both the upstream pipe and the valve cavity. It has nothing to do with a leaky seal. For a
valve whose seal leakiness is significant (curve Z), the magnitude of the FRF starts out a little
higher at very low frequency, and then stays high, only gradually failing off with increasing
frequency. For a valve with moderate seal leakiness (curve Y), the magnitude of the FRF just
above the very low frequency approximates more the curve of the large leak case (curve Z),
but then as the frequency increases further it rapidly decreases to better approximate the curve
of the no leak case (curve X). Above the quarter wavelength frequency, the magnitude will be seen to vary up and down as the nodal frequencies and multiple paths manifest their effect.
Nevertheless, the mean value over the spectrum of curve Z should still exceed that of curve
Y, which should in turn still exceed that of curve X.
Fig. 6b shows different coherence representations, P2(f)/P,(f) for the same
three seal leakiness conditions. Unlike the magnitude representation of the FRF (Fig. 6a)
where the highest value could be anything, in the coherence representation, the highest value
is always 1.0 indicating perfect coherence. This enhancement in numerical meaning it makes
the interpretation of the resulting curves much more definitive. Even for a valve with no
leaky seals (curve R), the coherence at just above zero Hz may be at or close to one. This is
because the upstream and cavity pressure fluctuations at very low frequency have essentially
the same cause - that is the low frequency motions of the platform and pipe run. It doesn't
matter if the pressure fluctuations are of different amplitudes, if the cause is the same, the
coherence will be nearly 1.0. But for a valve with no leaky seals, the coherence plummets
above the very low frequency region. This is because in the higher frequency region, the
pressure fluctuation source in the pipe is the flow noise, and this noise is effectively blocked
by the seals as it tries to enter the internal cavity. When not testing in production but rather
just after a shutdown, the source of the noise is not flow but transients such as sloshing and
the like, which arise from the sudden momentum change. For a valve with moderate seal
leakiness (curve S), the flow noise or sloshing noise gets through to some degree, especially
at the lower frequencies, and this is manifested by a coherence value above 0.5 at low
frequency, probably dipping to below 0.5 at higher frequencies. And finally for a valve that
has significant seal leakiness (curve T), even more noise gets through to the inner cavity 28,
and the coherence although it still dips with increasing frequency, may remain above 0.5 throughout the indicated frequency range. As with the FRF magnitude representation, the
coherence representation, above the quarter wavelength frequency, will be seen to vary up
and down as the nodal frequencies and multiple paths manifest their effects. But as before,
the mean value over the spectrum of curve T should still exceed that of curve S, which in turn
should still exceed that of curve R.
Using both the magnitude representation of the FRF, and the coherence, is
sure to be more definitive than using either alone. For example, above the very low
frequency peak, high magnitudes that are not accompanied by a corresponding reasonable
coherence value ,will have no seal leakiness significance. Other representations of the FRF,
such as the phase representation (not shown), and the real and imaginary representations (not
shown), may have some inteφretive value as might the auto spectra of each of the two signals
(also not shown). All these representations as a function of frequency could be available for
inspection following the averaged FRF analysis of the data.
Seal leakiness as mentioned above refers to the leakiness of any of the
upstream or downstream seals (18, 20, 24, 26 in Fig. 1). Recall that for the valve 10 itself to
be leaky, at least one upstream seal and at least one downstream seal must leak. As a result,
the present invention is a very conservative test for valve leakiness. It will effectively catch
most problems in the early one-seal-leak stage before it becomes a dangerous two-seal-leak
situation. And because of its conservative nature, it will find a use as an adjunct to local leak
rate testing (LLRT) in nuclear power plants and in many other valve applications, with or
without modification.
There are times when no sound energy exists in the fluid in the pipe, for
example during periods of non-production when no fluid is flowing, or well after a production shutdown when the transient energy has already dissipated in the pipeline. In
either case, the Frequency Response Function magnitude and the coherence methodology,
previously discussed, may still be used if an external sound source is introduced to provide
the necessary sonic energy to the fluid.
The sound source could be of any type known to those skilled in the art, for
example a piezoelectric transducer. On an oil or gas rig, it may actually be preferable to use a
hydraulically-actuated or pneumatically-actuated sound source in order to eliminate any
potential explosion hazard, and to more efficiently couple low frequency energy into the
fluid.
Fig. 7 shows the preferred location and arrangement of an external sound
source 34. As seen, the sound source 34 is connected to or otherwise in fluid communication
with the inner cavity 28 by a small pipe section 36 extending through a port 38 in the cavity
28 in a manner similar to the manner in which connecting pipe sections are employed for
providing fluid communication with the dynamic pressure transducers 30 and 32. The pipe
section 36 to the sound source 34 is filled with the working fluid, either oil or gas. As an
alternative, if a second inner cavity port 38 is not available, the sound source 34 may be
connected into the line to the inner cavity pressure transducer 32 utilizing a "T" connection or
the like. A third pressure transducer 40 (p3(t)) is located downstream from the inner cavity 28
of the valve 10. With the valve 10 as shown in the closed position, the only way that sound
from the sound source 34 can get to the upstream pressure transducer 30 is for an upstream
seal 19 to be leaky, and the only way that sound from the sound source 32 can get to the
downstream pressure transducer 40 is for a downstream seal 21 to be leaky. The sound from
the source 32 inside the inner cavity 28 of course will be present regardless of whether there are upstream or downstream seal leaks. Connecting the sound source 34 to the inner cavity
28 enables a leak in an upstream seal 19 to be detected in the closed-off position, if an
upstream pressure transducer 30 is installed. It also enables a leak in a downstream seal 21 to
be detected in the closed-off position, if a downstream pressure transducer 40 is installed.
And if both an upstream pressure transducer 30 and a downstream pressure transducer 40 are
installed, leaks in both upstream and downstream seals 19, 21 can be detected, and
furthermore, they can be differentiated, one from another. The methodology used in the
present embodiment is exactly as described above, except now the FRF is formed as
P,(f)/P2(f) for detecting an upstream seal leak, and as P3(f)/P2(f) for detecting a downstream
seal leak.
Unlike the situations described above where the sound was broadband as a
result of fluid flow noise and transient excitation, in the present embodiment, the utilized
sound from the sound source 34 may be sinusoidal. But as before, the upstream and
downstream pressure transducers 30, 40 are preferentially placed within a quarter wavelength
of the valve 10, for the frequency of the sound source 34 which is employed. With no flow,
there is no possibility of highly localized turbulence near one of the sensors, and thus no need
to extend the frequency range. At a sound source frequency of 50 Hz, the distance translates
to about 22 feet for oil and about 5 feet for gas. If necessary to extend that distance, due to a
physical limitation, a sound source frequency of 10 Hz will extend the distance for gas, to
over 20 feet. The lowered sound source frequency limit is acceptable for gas, because very
low frequency sloshing noise that might otherwise exist for a liquid (such as oil) due to very
low frequency platform motions, won't exist for gas.
As discussed above, a high coherence value and high value of the FRF magnitude signals a leaky seal, except that with the present embodiment which uses a
sinusoidal sound source 34, the measurement is viewed only at that single sound source
frequency to make the determination. With no fluid flow, that single sound source frequency
predominates over the surrounding values, in the coherence measurement, and even in the
FRF magnitude, because the background sound or noise is small relative to the sound from
the sound source 34. The surrounding magnitude values may appear larger than the sound
source single frequency component, but only as a result of the inner cavity background
sounds being smaller than the upstream and downstream background sounds.
An alternative to a single frequency (sinusoidal) sound source is a repetitive
sound pulse or click, the click repetition rate showing up as the fundamental sinusoidal
frequency of the sound source, furthermore including all of the harmonics of that fundamental
sinusoidal frequency. For example, if there are ten clicks every second, the fundamental
frequency component present is 10 Hz, but harmonic frequency components at 20 Hz, 30 Hz,
40 Hz, and 50 Hz, within the 0 to 50 Hz range will also be present.
Fig. 8a and 8b show the resulting averaged, 0 to 50 Hz., Frequency Response
Function, (either P1(f)/P2(f) or P3(f)/P2(f)) for various degrees of seal leakiness, using a sound
source with a repetitive click at 10 Hz. The curves represent the analyzed results for data
obtained with the valve 10 closed off as shown in Fig. 7, for any of the types of ESD valves.
As a result, there is information at 10 Hz, at 20 Hz, at 30 Hz, at 40 Hz, and at 50 Hz. Less
averaging time would be required if a sinusoidal sound source were used instead of a
repetitive click because all of the energy would go into the single frequency component, but
the seal leakiness information would only exist at that single frequency component. Thus, the
use of a repetitive click instead of a sinusoid provides more diagnostic information. This is especially helpful in quantifying the size of the seal leak, as larger size leaks tend to allow
more of the higher frequency sound through, while smaller leaks tend to block the higher
frequency sound. The previous discussion about the magnitude representation of the FRF
and the associated coherence representation still applies, but now the pertinent information
exists only at the discreet frequency components.
Although the sound-source approach described herein could be used when
there is significant broadband acoustic energy in the line (as in the previously discussed
cases), to use it in those cases would not be efficient because it might take an enormous
amount of averaging (even synchronous averaging) to be able to "see" or detect the discreet
components over the noise. In those previous cases, the flow noise, itself, is the sound
source.
In the present embodiment, the sound source 34 is preferably located in fluid
communication with the inner cavity 28. But by reciprocity, the same information can be
obtained by locating the sound source either upstream or downstream of the valve cavity 28
near the upstream or downstream pressure transducers 30, 40 and using the cavity pressure
transducer 32 as a sound detector. This approach is acceptable when there is only an
upstream or a downstream pressure transducer, but if both transducers are present, only the
inner cavity location allows an upstream or downstream seal leak to be detected using a
single sound source 34.
A through leak can be further verified in the valve closed position if a known
or determinable differential pressure exists across the closed valve. In that case, fluid will
only flow from the high pressure side to the low pressure side through upstream and
downstream seal leaks, and in the process, the flowing fluid makes a noise. The noise can be picked up by the internal cavity pressure transducer 32 already in place, and the resulting
auto-spectrum (magnitude at a function of frequency) can be obtained through the existing
analysis circuitry, and evaluated. If both seals aren't leaking, there is no through leak, and
even in the case of a massive upstream or downstream seal leak, there will be no fluid flow
and no noise. As a result, a very low valued auto-spectrum will be obtained, with a
characteristic 1/f shape. But if a through leak exists, the noise generated in the low
frequency range will increase the spectral floor. The greater the leak and the greater the
differential pressure, the greater the increase. The effect is particularly apparent near cavity
natural frequencies which are typically less than a few hundred Hz. If the differential
pressure is known or repeatable, an approximate quantification of the through leak may be
feasible. This method differs from an acoustics emission approach, where the frequencies
considered are much higher, usually well above 10 KHz.
But the approach above is not universally applicable since differential pressure
is not always present, and even when it is, the differential pressure level may not be known.
By contrast, the sound source approach described previously is universally applicable for the
closed valve situation, since it doesn't depend on sound energy from somewhere else. And
like the open valve situation, this approach is independent of sound level since the FRF
magnitude and the coherence representations are automatically normalized. That provides
repeatable approximate leak quantification, possibly even as a single number answer using
the mean value over the spectrum discussed previously. The ability to approximately
quantify leaky seals and through valve leaks is important since certain leaks may be deemed
acceptable if they are judged to not exceed the capacity of the on-board fire protection
system. The only trade-off in employing the sound source 34 to the inner cavity 28
occurs when either the upstream pressure transducer 30 or the downstream pressure -
transducer 40 isn't utilized. This situation will sometimes occur for riser (sea side) ESD
valves where the use of an upstream tap 31 may be frowned upon as a potential separate leak
source, and for export (to shore) ESD valves where the use of a downstream tap may be
similarly frowned upon.
Fig. 9a and 9b show an on-line system approach for the present invention with
the sensors and sound source located on or near the valve 10, and with data acquisition
circuitry and analysis circuitry 52 located in a nearby (safe) equipment room 54. More than
one equipment room 54 may be used on a platform, and several valves may connect to the
circuitry 52 in each equipment room. An on-shore control room computer or server 56 may
be connected by radio link. Engineers at various locations may connect to the server 56 to
obtain the relevant data. A portable version of the system (not shown), using the same
sensors and possibly the sound source is of course also feasible.
The illustrated on-line version acquires production (open valve) data
periodically, sampling each signal at 1 ,000 samples per second, forming and averaging the
FRF magnitude and coherence functions and analyzing the results. It also automatically
triggers on the breakaway torque or thrust signal from a torque or thrust sensor 58, and uses
changes in that signal, including the pretrigger portion, to assess valve degradation. On oil
platforms, immediately at the end of that trace (signaling valve closed in the closing stroke),
pressure data may be acquired by the various transducers 30, 32, 40 using residual fluid noise
in the pipe for a short period of time. The system may also be used to acquire inner cavity
auto-spectrum data in closed valve situations where known differential pressure exists across the valve 10. And finally, also for closed valve situations, the sound source is activated and
data is acquired from the pressure transducers 30, 32, 40 and the signals are analyzed-and
evaluated using the FRF magnitude and coherence functions as above.
It will be appreciated by those skilled in the art that changes or modifications
could be made to the above described embodiment without departing from the broad
inventive concepts of the invention. It should be appreciated, therefore, that the present
invention is not limited to the particular embodiment disclosed but is intended to cover all
embodiments within the scope or spirit of the described invention.

Claims

1. An apparatus for use with a fluid transport system having an upstream
pipe, a downstream pipe and a valve connected between the upstream pipe and the
downstream pipe for controlling fluid flow through the system, the valve having at least one
upstream seal, at least one downstream seal and an inner cavity effectively isolated by the
seals from the fluid flow stream, the apparatus for detecting a leak in at least one of the seals,
the apparatus comprising:
a first transducer in fluid communication with the fluid flow stream at
at least one of: (1) a predetermined distance upstream of the upstream seal and, (2) a
predetermined distance downstream of the downstream seal, the first transducer for sensing
pressure pulsations resulting from at least one of: (1) dynamic energy due to fluid flow
through the fluid transport system and, (2) transient energy within the fluid in the transport
system after the valve is closed, and for generating first representative electrical signals as a
function of time;
a second transducer in fluid communication with the inner cavity for
sensing substantially simultaneous pressure pulsations within the inner cavity and for
generating second representative electrical signals as a function of time; and
an analyzer for receiving the first and second electrical signals and for
generating at least one of the following functions: (1) a frequency response function and, (2)
a coherence function, the generated function being sufficiently averaged to provide a
meaningful measure of the degree to which the two electrical signals are related to thereby
indicate whether, and to what extent, sensed pressure pulsations within the fluid transport
system are passing through at least one of the seals to the inner cavity.
2. The apparatus as recited in claim 1 wherein the frequency response
function is a magnitude representation.
3. The apparatus as recited in claim 1 wherein both the frequency
response function and the coherence function are generated by the analyzer.
4. The apparatus as recited in claim 1 wherein the first transducer is
positioned for sensing pulsations upstream of the upstream seal for identifying a leak in the
upstream seal after the valve is closed.
5. The apparatus as recited in claim 1 wherein the first pressure
transducer is positioned downstream of the downstream seal for identifying a leak in the
downstream seal after the valve is closed.
6. The apparatus as recited in claim 1 wherein the predetermined distance
is established based upon the frequency range selected for analysis and the type of fluid in the
transport system.
7. The apparatus as recited in claim 6 wherein the maximum frequency is
less than or equal to 50 Hz.
8. The apparatus as recited in claim 6 wherein the maximum frequency is
less than or equal to 10,000 Hz.
9. An apparatus for use with a fluid transport system having an upstream
pipe, a downstream pipe and a valve connected between the upstream pipe and the
downstream pipe for controlling fluid flow through the system, the valve having at least one
upstream seal, at least one downstream seal and an inner cavity effectively isolated by the
seals from the fluid flow stream, the apparatus for detecting and identifying the location of a leak in at least one of the seals when the valve is closed, the apparatus comprising:
an external sound source in fluid communication with the fluid
transport system for generating sound energy within the system;
a first transducer in fluid communication with the fluid in the system at
at least one of: (1) a predetermined distance upstream of the upstream seal and, (2) a
predetermined distance downstream of the downstream seal, the first transducer for sensing
pressure pulsations resulting from the acoustic energy generated by the sound source and for
generating first representative electrical signals as a function of time;
a second transducer in fluid communication with the inner cavity for
sensing substantially simultaneous pressure pulsations within the inner cavity resulting from
the acoustic energy generated by the sound source and for generating second representative
electrical signals as a function of time; and
an analyzer for receiving the first and second electrical signals and for
generating at least one of the following functions: (1) a frequency response function and, (2)
a coherence function, the generated function being sufficiently averaged to provide a
meaningful measure of the degree to which the two electrical signals are related to thereby
indicate whether, and to what extent, sensed pressure pulsations within the fluid transport
system are passing through at least one of the seals to the inner cavity.
10. The apparatus as recited in claim 9 wherein the sound source is
positioned for generating sound energy within one of: upstream of the upstream seal, and the
inner cavity, and the first transducer is positioned for sensing pressure pulsations upstream of
the upstream seal for identifying a leak in an upstream seal.
11. The apparatus as recited in claim 9 wherein the sound source is positioned for generating sound energy within one of: downstream of the downstream seal,
and the inner cavity, and the first transducer is positioned for sensing pulsations downstream
of the downstream seal for identifying a leak in a downstream seal.
12. The apparatus as recited in claim 9 wherein the sound generated by the
sound source is sinusoidal.
13. The apparatus as recited in claim 12 wherein the frequency of the
sound source is less than or equal to 50 Hz.
14. The apparatus as recited in claim 9 wherein the sound source generates
a repetitive sound pulse at a predetermined repetition rate.
15. The apparatus as recited in claim 14 wherein the fundamental
frequency of the repetitive pulse generated by the sound source less than or equal to 10 Hz.
16. The apparatus as recited in claim 9 wherein the sound source is
positioned for generating sound energy within the inner cavity and the first transducer is
positioned for sensing pulsations within one of: upstream of the upstream seal, and
downstream of the downstream seal.
17. The apparatus as recited in claim 9 wherein the frequency response
function is a magnitude representation.
18. The apparatus as recited in claim 9 wherein both the frequency
response function and the coherence function are generated by the analyzer.
19. The apparatus as recited in claim 9 wherein the predetermined distance
is established based upon the frequency range selected for analysis and the type of fluid in the
transport system.
20. A method for use with a fluid transport system having an upstream pipe, a downstream pipe and a valve connected between the upstream pipe and the
downstream pipe for controlling fluid flow through the system, the valve having at least one
upstream seal, at least one downstream seal and an inner cavity effectively isolated by the
seals from the fluid flow stream, the method for detecting a leak in at least one of the seals,
comprising the steps of:
sensing pressure pulsations within the fluid flow stream at at least one
of: (1) a predetermined distance upstream of the upstream seal and, (2) a predetermined
distance downstream of the downstream seal and generating first representative electrical
signals as a function of time, the pressure pulsations resulting from at least one of: (1) a
dynamic energy due to fluid flow through the fluid transport system and, (2) transient energy
within the fluid in the transport system after the valve is closed;
sensing substantially simultaneous pressure pulsations within the inner
cavity and generating second representative electrical signals as a function of time; and
analyzing the first and second electrical signals and generating at least
one of the following functions: (1) a frequency response function and, (2) a coherence
function, the generated function being sufficiently averaged to provide a meaningful measure
of the degree to which the two electrical signals are related to thereby indicate whether, and to
what extent, sensed pressure pulsations within the flow stream are passing through at least
one of the seals to the inner cavity.
21. The method as recited in claim 20 wherein the frequency response
function is a magnitude representation.
22. The method as recited in claim 20 wherein both the frequency response
function and the coherence function are generated.
23. The method as recited in claim 20 wherein the predetermined distance
is established based upon the frequency range selected for analysis and the type of fluid in the
transport system.
24. A method for use with a fluid transport system having an upstream
pipe, a downstream pipe and a valve connected between the upstream pipe and the
downstream pipe for controlling fluid flow through the system, the valve having at least one
upstream seal, at least one downstream seal and an inner cavity effectively isolated by the
seals from the fluid flow stream, the method for detecting a leak in at least one of the seals
when the valve is closed, comprising the steps of:
generating sound energy within the fluid transport system utilizing an
external sound source in fluid communication with the system;
sensing pressure pulsations in the system at at least one of: (1) a
predetermined distance upstream of the upstream seal and, (2) a predetermined distance
downstream of the downstream seal and generating first representative electrical signals as a
function of time, the pressure pulsations resulting from the acoustic energy generated by the
sound source;
sensing substantially simultaneous pressure pulsations within the inner
cavity and generating second representative electrical signals as a function of time; and
analyzing the first and second electrical signals and generating at least
one of the following functions: (1) a frequency response function and, (2) a coherence
function, the generated function being sufficiently averaged to provide a meaningful measure
of the degree to which the two electrical signals are related to thereby indicate whether, and to
what extent, sensed pressure pulsations within the fluid transport system are passing through at least one of the seals to the inner cavity.
25. The method as recited in claim 24 wherein the sound source is~
positioned for generating sound energy within the inner cavity.
26. The method as recited in claim 24 wherein the frequency response
function is a magnitude representation.
27. The method as recited in claim 24 wherein both the frequency response
function and the coherence function are generated.
28. The method as recited in claim 24 wherein the predetermined distance
is established based upon the frequency range selected for analysis and the type of fluid in the
transport system.
29. A method for use with a fluid transport system having an upstream
pipe, a downstream pipe and a valve connected between the upstream pipe and the
downstream pipe for controlling fluid flow through the system, the valve having at least one
upstream seal, at least one downstream seal and an inner cavity effectively isolated by the
seals from the fluid flow stream, the method for detecting the presence of a leak in both of the
seals when the valve is closed and a differential pressure exists across the valve, comprising
the steps of:
determining the magnitude of the differential pressure across the valve;
sensing the presence of pressure pulsations within the inner cavity
resulting from fluid flowing through the seals into and out of the inner cavity and generating
representative electrical signals as a function of time;
analyzing the electrical signals and generating an auto spectrum
representation; and using the auto spectrum in conjunction with the determined differential
pressure magnitude to indicate the existence and extent of a leak.
PCT/US1998/012868 1997-06-26 1998-06-18 Method and apparatus for on-line detection of leaky emergency shut down or other valves WO1999000619A1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE69817821T DE69817821D1 (en) 1997-06-26 1998-06-18 METHOD AND DEVICE FOR ONLINE LEAKAGE MONITORING OF EMERGENCY SHUT-OFF VALVES OR OTHER VALVES
AU81567/98A AU8156798A (en) 1997-06-26 1998-06-18 Method and apparatus for on-line detection of leaky emergency shut down or othervalves
AT98931431T ATE249000T1 (en) 1997-06-26 1998-06-18 METHOD AND DEVICE FOR ONLINE LEAKAGE MONITORING OF EMERGENCY STOP VALVE OR OTHER VALVES
EP98931431A EP0991888B1 (en) 1997-06-26 1998-06-18 Method and apparatus for on-line detection of leaky emergency shut down or other valves
NO19996403A NO320881B1 (en) 1997-06-26 1999-12-22 Method and apparatus for directly detecting leakage in node shut-off valves or other valves
NO20055161A NO335721B1 (en) 1997-06-26 2005-11-03 Method for direct detection of leakage in emergency shut-off valves or other valves

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US5572897P 1997-06-26 1997-06-26
US60/055,728 1997-06-26
US6059097P 1997-10-01 1997-10-01
US60/060,590 1997-10-01

Publications (1)

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ID=26734566

Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (7)

Country Link
US (2) US6128946A (en)
EP (1) EP0991888B1 (en)
AT (1) ATE249000T1 (en)
AU (1) AU8156798A (en)
DE (1) DE69817821D1 (en)
NO (2) NO320881B1 (en)
WO (1) WO1999000619A1 (en)

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US6128946A (en) 2000-10-10
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EP0991888B1 (en) 2003-09-03
EP0991888A1 (en) 2000-04-12

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