WO2007103421A3 - Method of preparing ceramic powders using chelate precursors - Google Patents

Method of preparing ceramic powders using chelate precursors Download PDF

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Publication number
WO2007103421A3
WO2007103421A3 PCT/US2007/005808 US2007005808W WO2007103421A3 WO 2007103421 A3 WO2007103421 A3 WO 2007103421A3 US 2007005808 W US2007005808 W US 2007005808W WO 2007103421 A3 WO2007103421 A3 WO 2007103421A3
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WO
WIPO (PCT)
Prior art keywords
ceramic powders
ion
preparing ceramic
chelate precursors
precursors
Prior art date
Application number
PCT/US2007/005808
Other languages
French (fr)
Other versions
WO2007103421A2 (en
Inventor
Richard D Weir
Carl Walter Nelson
Original Assignee
Eestor Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eestor Inc filed Critical Eestor Inc
Priority to EP07752500A priority Critical patent/EP1999283A4/en
Priority to JP2008558371A priority patent/JP2009528974A/en
Priority to CA002643897A priority patent/CA2643897A1/en
Publication of WO2007103421A2 publication Critical patent/WO2007103421A2/en
Publication of WO2007103421A3 publication Critical patent/WO2007103421A3/en

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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G4/00Fixed capacitors; Processes of their manufacture
    • H01G4/002Details
    • H01G4/018Dielectrics
    • H01G4/06Solid dielectrics
    • H01G4/08Inorganic dielectrics
    • H01G4/12Ceramic dielectrics
    • H01G4/1209Ceramic dielectrics characterised by the ceramic dielectric material
    • H01G4/1218Ceramic dielectrics characterised by the ceramic dielectric material based on titanium oxides or titanates
    • H01G4/1227Ceramic dielectrics characterised by the ceramic dielectric material based on titanium oxides or titanates based on alkaline earth titanates
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    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14Methods for preparing oxides or hydroxides in general
    • C01B13/36Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C01B13/363Mixtures of oxides or hydroxides by precipitation
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    • C04B35/46Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
    • C04B35/462Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
    • C04B35/465Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates
    • C04B35/468Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates
    • C04B35/4682Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates based on BaTiO3 perovskite phase
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    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/48Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
    • C04B35/49Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates containing also titanium oxides or titanates
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    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
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  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Structural Engineering (AREA)
  • Power Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Composite Materials (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

Wet-chemical methods involving the use of water-soluble hydrolytically stable metal-ion chelate precursors and the use of a nonmetal-ion-containing strong base can be used in a coprecipitation procedure for the preparation of ceramic powders. Examples of the precipitants used include tetraalkylammonium hydroxides. A composition-modified barium titanate is one of the ceramic powders that can be produced. Certain metal-ion chelates can be prepared from 2-hydroxypropanoic acid and ammonium hydroxide.
PCT/US2007/005808 2006-03-07 2007-03-06 Method of preparing ceramic powders using chelate precursors WO2007103421A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
EP07752500A EP1999283A4 (en) 2006-03-07 2007-03-06 Method of preparing ceramic powders using chelate precursors
JP2008558371A JP2009528974A (en) 2006-03-07 2007-03-06 Method for producing ceramic powder using a plurality of chelate precursors
CA002643897A CA2643897A1 (en) 2006-03-07 2007-03-06 Method of preparing ceramic powders using chelate precursors

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/369,255 US7914755B2 (en) 2001-04-12 2006-03-07 Method of preparing ceramic powders using chelate precursors
US11/369,255 2006-03-07

Publications (2)

Publication Number Publication Date
WO2007103421A2 WO2007103421A2 (en) 2007-09-13
WO2007103421A3 true WO2007103421A3 (en) 2008-06-12

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PCT/US2007/005808 WO2007103421A2 (en) 2006-03-07 2007-03-06 Method of preparing ceramic powders using chelate precursors

Country Status (5)

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US (2) US7914755B2 (en)
EP (1) EP1999283A4 (en)
JP (1) JP2009528974A (en)
CA (1) CA2643897A1 (en)
WO (1) WO2007103421A2 (en)

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