USRE39399E1 - Segmented die for applying hot melt adhesives or other polymer melts - Google Patents

Segmented die for applying hot melt adhesives or other polymer melts Download PDF

Info

Publication number
USRE39399E1
USRE39399E1 US10/420,569 US42056903A USRE39399E US RE39399 E1 USRE39399 E1 US RE39399E1 US 42056903 A US42056903 A US 42056903A US RE39399 E USRE39399 E US RE39399E
Authority
US
United States
Prior art keywords
die
air
manifold
flow passage
polymer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US10/420,569
Inventor
Martin A. Allen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nordson Corp
Original Assignee
Nordson Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nordson Corp filed Critical Nordson Corp
Priority to US10/420,569 priority Critical patent/USRE39399E1/en
Application granted granted Critical
Publication of USRE39399E1 publication Critical patent/USRE39399E1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05CAPPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C5/00Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work
    • B05C5/001Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work incorporating means for heating or cooling the liquid or other fluent material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/02Spray pistols; Apparatus for discharge
    • B05B7/08Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point
    • B05B7/0807Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point to form intersecting jets
    • B05B7/0861Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point to form intersecting jets with one single jet constituted by a liquid or a mixture containing a liquid and several gas jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05CAPPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C5/00Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work
    • B05C5/02Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work the liquid or other fluent material being discharged through an outlet orifice by pressure, e.g. from an outlet device in contact or almost in contact, with the work
    • B05C5/027Coating heads with several outlets, e.g. aligned transversally to the moving direction of a web to be coated
    • B05C5/0275Coating heads with several outlets, e.g. aligned transversally to the moving direction of a web to be coated flow controlled, e.g. by a valve
    • B05C5/0279Coating heads with several outlets, e.g. aligned transversally to the moving direction of a web to be coated flow controlled, e.g. by a valve independently, e.g. individually, flow controlled
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D4/00Spinnerette packs; Cleaning thereof
    • D01D4/02Spinnerettes
    • D01D4/025Melt-blowing or solution-blowing dies
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/08Melt spinning methods
    • D01D5/098Melt spinning methods with simultaneous stretching
    • D01D5/0985Melt spinning methods with simultaneous stretching by means of a flowing gas (e.g. melt-blowing)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05CAPPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C5/00Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work
    • B05C5/02Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work the liquid or other fluent material being discharged through an outlet orifice by pressure, e.g. from an outlet device in contact or almost in contact, with the work
    • B05C5/0225Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work the liquid or other fluent material being discharged through an outlet orifice by pressure, e.g. from an outlet device in contact or almost in contact, with the work characterised by flow controlling means, e.g. valves, located proximate the outlet
    • B05C5/0237Fluid actuated valves

Definitions

  • This invention relates generally to dies for applying hot melt adhesives to a substrate or producing nonwovens.
  • the invention relates to a modular die provided with at least one air-assisted die tip or nozzle.
  • the invention relates to a segmented die assembly comprising a plurality of separate die units, each unit including a manifold segment and a die module mounted thereon.
  • Modular dies have been developed to provide the user with flexibility in selecting the effective length of the die. For short die lengths only a few modules need be mounted on a manifold block. (See U.S. Pat. No. 5,618,566). Longer dies can be achieved by adding more modules to the manifold. U.S. Pat. No. 5,728,219 teaches that the modules may be provided with different types of die tips or nozzles to permit the selection of not only the die length but also the deposition pattern.
  • the most commonly used adhesive applicators are intermittently operated air-assisted dies. These include meltblowing dies, spiral nozzles, and spray nozzles.
  • Meltblowing is a process in which high velocity hot air (normally referred to as “primary air”) is used to blow molten filament extruded from a die onto a collector to form a nonwoven web or onto a substrate to form an adhesive pattern, a coating, or composite.
  • the process employs a die provided with (a) a plurality of openings (e.g. orifices) formed in the apex of a triangular shaped die tip and (b) flanking air plates which define converging air passages.
  • openings e.g. orifices
  • flanking air plates which define converging air passages.
  • the openings are in the form of slots.
  • the die tips are adapted to form a row of filaments which upon contact with the converging sheets of hot air are carried to and deposited on a collector or a substrate in a random pattern.
  • Meltblowing technology was originally developed for producing nonwoven fabrics but recently has been utilized in the meltblowing of adhesives onto substrates.
  • filaments extruded from the air-assisted die may be continuous or discontinuous.
  • filament is used interchangeably with the term “fiber” and refers to both continuous and discontinuous strands.
  • Spiral spray nozzles such as those described in U.S. Pat Nos. 4,949,668 and 5,102,484, operate on the principle of a thermoplastic adhesive filament being extruded through a nozzle while a plurality of hot air jets are angularly directed onto the extruded filament to impart a circular or spiral motion thereto.
  • the filaments thus assume an expanding swirling cone shape pattern while moving from the extrusion nozzle to the substrate.
  • a circular or spiral or helical bead is continuously deposited on the substrate, each circular cycle being displaced from the previous cycle by a small amount in the direction of substrate movement.
  • the meltblowing die tips offer superior coverage whereas the spiral nozzles provide better edge control.
  • the segmented die assembly of the present invention is of modular construction, comprising a plurality of side-by-side and interconnected die units.
  • Each die unit includes a manifold segment and a die module mounted on the manifold segment.
  • the die module has mounted thereon an air-assisted die tip or nozzle.
  • the die tip may be a meltblowing type and the nozzle may be a spiral nozzle or a spray nozzle.
  • nozzle is used herein in the generic sense, meaning any air-assisted die tip or nozzle; and the term “air-assisted” means a nozzle through which is extruded a molten thermoplastic filament or filaments, and air jets, air streams, or air sheets which contact the molten filaments to divert, attenuate or change the flow pattern of the filament(s) and impart a desired characteristic to the filaments, either in terms of the size of the filaments or the deposition pattern.
  • each die unit the manifold segment and the module, are provided with (a) air passages for delivering air to the nozzles and (b) a polymer flow passage for delivering a polymer melt to the nozzle.
  • the nozzle is a meltblowing die tip provided with a row of orifices and flanking air slits, so that as a row of filaments are extruded through the meltblowing die tip, they are contacted with converging sheets of hot air that attenuate or draw down the filaments to microsize.
  • the nozzle may also be a spiral or spray nozzle.
  • the die assembly may include segmented units having different types of nozzles.
  • the segmented die units are assembled by interconnecting several identical manifold segments, wherein the air passages and the polymer flow passage of each segment are in fluid communication.
  • the interconnected manifold segments function much in the manner of an integrated manifold.
  • a die module is mounted on each manifold segment and, in combination with other die modules, form a row thereon.
  • polymer melt is extruded as a row of filaments from the array of modules and deposited on a moving substrate positioned under the assembly.
  • each module is provided with an air-actuated valve to selectively open and close the polymer flow passage.
  • the instrument air for activating the valve is delivered through each manifold segment to the module.
  • the valves may be individually actuated or actuated as a bank, depending on the instrument air passages and the number of control valves used.
  • FIG. 1 is a top plan view of a segmented meltblowing die constructed according to the present invention showing polymer flow lines.
  • FIG. 2 is a top plan view of the present segmented die showing process air (primary air) flow lines.
  • FIG. 3 is front elevation view of the segmented die illustrating the discharge of filaments onto a substrate.
  • FIG. 4 is an enlarged sectional, view taken along plane 4 — 4 of FIG. 1 illustrating middle section of the segmented manifold.
  • FIG. 5 is a sectional view taken along cutting plane 5 — 5 of FIG. 1 illustrating an end plate of the segmented manifold.
  • FIG. 6 is a sectional view taken along cutting plane 6 — 6 of FIG. 1 illustrating the end plate of the segmented manifold opposite that shown in FIG. 5 .
  • FIG. 7 is a sectional view of the segmented manifold taken along plane 7 — 7 of FIG. 4 illustrating the polymer flow passages.
  • FIG. 8 is a sectional view of the segmented manifold taken along section 8 — 8 of FIG. 4 illustrating the process air flow passages.
  • the meltblowing die 10 of the present invention comprises a plurality of side-by-side die units 15 comprising manifold segments 11 and die modules 12 .
  • the manifold segments are labeled 11 A through 11 F and the die modules are labeled 12 A through 12 F for the 6 segment structure.
  • each die unit 15 comprises a manifold segment 11 , a die module 12 mounted thereon, and a valve actuator 20 for controlling the flow of polymer melt through the die segment.
  • each die module 12 has a die tip 13 which discharges filaments 14 onto a moving substrate (or collector) forming a layer or pattern of filaments on the substrate in a somewhat random fashion.
  • the preferred die modules 12 are the type described in U.S. Pat. Nos. 5,618,566 and 5,728,219, the disclosures of which are which are incorporated herein by reference. It should be understood, however, that other die modules may be used. See, for example, U.S. patent application Ser. No. 09/021,426, filed Feb. 10, 1998, entitled “MODULAR DIE WITH QUICK CHANGE DIE TIP OR NOZZLE.”
  • each die module 12 consists of a die body 16 and a die tip 13 .
  • the die body 16 has formed therein an upper circular recess 17 and a lower circular recess 18 which are interconnected by a narrow opening 19 .
  • the upper recess 17 defines a cylindrical chamber 23 which is closed at its top by threaded plug 24 .
  • Valve assembly 21 mounted within chamber 23 comprises piston 22 having depending therefrom stem 25 .
  • the piston 22 is reciprocally movable within chamber 23 , with adjustment pin 24 a limiting the upward movement.
  • Conventional o-rings may be used at the interface of the various surfaces for fluid seals as illustrated at 28 .
  • Side ports 26 and 27 are formed in the wall of the die body 16 to provide communication to chamber 23 above and below piston 22 , respectively. As described in more detail below, the ports 26 and 27 serve to conduct air (referred to as instrument gas or air) to and from each side of piston 22 .
  • instrument gas or air air
  • a threaded valve insert member 30 Mounted in the lower recess 18 is a threaded valve insert member 30 having a central opening 31 extending axially therethrough and terminating in valve port 32 at its lower extremity.
  • the lower portion of insert member 30 is of reduced diameter and in combination with the die body inner wall defined a downwardly facing cavity 34 .
  • Upper portion 36 of insert member 30 abuts the top surface of recess 18 and has a plurality (e.g. 4) of circumferential ports 37 formed therein and in fluid communication with the central passage 31 .
  • An annular recess extends around the upper portion 36 interconnecting the ports 37 .
  • Valve stem 25 extends through body opening 19 and axial opening 31 of insert member 30 , and terminates at end 40 which is adapted to section valve port 32 .
  • the annular space 45 between stem 25 and opening 31 is sufficient for polymer melt to flow therethrough.
  • End 40 of stem 25 seats on port 32 with piston 22 in its lower position within chamber 23 as illustrated in FIG. 4 .
  • actuation of the valve assembly 21 moves stem end 40 away from port 32 (open position), permitting the flow of polymer melt therethrough. Melt flows from the manifold 11 through side port 38 , through 37 , through annular space 45 discharging through port 32 into the die tip assembly 13 .
  • Conventional o-rings may be used at the interface of the various surfaces as illustrated in the drawings.
  • the die tip assembly 13 comprises a stack up of four parts; a transfer plate 41 , a die tip 42 , and two air plates 43 a and 43 b.
  • the assembly 13 can be preassembled and adjusted prior to mounting onto the body 16 using bolts 50 .
  • Transfer plate 41 is a thin metal member having a central polymer opening 44 formed therein. Two rows of air holes 49 flank the opening 44 as illustrated in FIG. 4 . When mounted on the lower mounting surface of body 16 , the transfer plate 41 covers the cavity 34 and therewith defines an air chamber with the air holes 49 providing outlets for air from cavity 34 . Opening 44 registers with port 32 with an o-ring between these providing a fluid seal at the interface surrounding port 32 . Holes 49 register with air holes 57 formed in die tip 42 .
  • the die tip 42 comprises a base member which is co-extensive with the transfer plate 41 and the mounting surface die body 16 , and a triangular nose piece 52 which may be integrally formed with the base.
  • the nose piece 52 terminates in apex 56 which has a row of orifices 53 spaced therealong.
  • Air plates 43 a and 43 b are in flanking relationship to the nose piece 52 and define coverging air slits which discharge at the apex of nose piece 52 .
  • Air (referred to as process air) is directed to opposite sides of the nose piece 52 into the converging slits and discharge therefrom as converging air sheets which meet at the apex of nose piece 52 and contact the filaments 14 emerging from the row of orifices 53 .
  • the module 12 of the type disclosed in FIG. 4 is described in more detail in the above referenced U.S. Pat. No. 5,618,566. Also usable in the present invention are modules disclosed in U.S. Pat. No. 5,728,219 and U.S. patent application Ser. Nos 08/820,559 and 09/021,426. Other types of modules may also be used.
  • the modules may dispense meltblown fibers, spirals, beads, sprays, or polymer coatings from the nozzle.
  • the module may be provided with a variety of nozzles including meltblowing nozzles, spiral spray nozzles, bead nozzles and coating nozzles.
  • segmented manifold 11 comprises end plates 61 and 62 having sandwiched therebetween a plurality of middle section 11 A-F.
  • End plates 61 and 62 are designed to provide fluid seals at each end of the die as well as provide inlet ports for a polymer melt at 64 and an inlet for process air at 66 .
  • Inlet 64 may have removable filter cartridge 68 for removing impurities from the melt stream.
  • air inlet 67 in plate 62 provides air, referred to as instrument air for opening control valves 20 A-F in the modules 12 A-F, respectively.
  • end plate 62 has threaded bolt holes 71 a-d which align with countersunk bolt holes 72 a-d in middle plate 11 A (only 72 a and b shown in FIGS. 1 and 2 , respectively).
  • End plate 61 has countersunk holes 73 a-d which align with thread holes 74 a-d (only 74 a, b shown) in middle plate 11 F.
  • Countersunk bolts 79 thus join plate 62 to plate 11 A leaving surface 81 flush for adjoining middle plate 11 B to 11 A, and flush surface 82 for joining end plate 61 to middle plate 11 F.
  • middle sections 11 A-F are joined by bolts 85 arranged in an alternating pattern of threaded and countersunk bolt holes.
  • middle section 11 D has four bored and countersunk bolt holes 86 a-d and four threaded bolt holes 87 a-d.
  • Plates 11 C and 11 E flank 11 D and have bolt holes which align with holes 86 a-d and 87 a-d, however, the pattern of countersunk holes and threaded holes are interchanged in the flanking plates.
  • the countersunk bored holes 86 a-d in plate 11 D will align with threaded holes in plate 11 C, and threaded holes 87 a-d will align with bored and countersunk holes in plate 11 E (see FIGS. 1 and 2 ).
  • Countersunk holes 86 a-d are of sufficient depth so that the heads of bolt 85 do not protrude beyond the outer lateral surface of the middle sections and thus permits the abutting surfaces of adjacent sections to be flush when bolts 85 are tightened. Tightening of bolts 85 establishes a metal-on-metal fluid seal between adjacent plates. O-rings may also be used to seal adjacent plates.
  • middle sections 11 A-F have central polymer flow passage 91 (see FIG. 4 ) which, when bolted together define continuous flow passage 92 which extends the length of the die.
  • Polymer passage 92 interconnects manifold segments 11 A-F.
  • a polymer melt enters the die through inlet 64 and flows into passage 92 .
  • Each middle plate has a hole 93 A-F (see FIG. 7 ) which leads from passage 92 into second continuous passage 94 and holes 96 A-F which is the outlet of the manifold and feeds polymer to die modules 12 A-F in parallel.
  • the outlet of passages 96 A-F register with the polymer inlet 38 (see FIG. 4 ) of each die module.
  • the lateral surfaces of middle plates 11 A-F and end plates 61 and 62 are precisely machined whereby a fluid seal is established at the interfaces when the plates are bolted together by bolts 85 as has been described.
  • Polymer melt thus enters the die through plate 61 at 64 , fills passage 92 , flows in parallel through holes 93 A-F, fills continuous passage 94 , flows in parllel through holes 96 A-F, and enters die modules 12 A-F through passages 38 (see FIG. 4 ).
  • the polymer which enters the die modules is extruded to form filaments 14 as has been described.
  • the polymer manifold design wherein the polymer flows between the two continuous passages 92 and 94 via a plurality of parallel holes serves to equalize the flow over the die length.
  • Heating element 97 maintains the polymer of the proper operating temperature.
  • Heated process air enters through inlet 66 which registers with the circular groove 101 ( FIG. 6 ) formed along the inner wall of end plate 62 .
  • Middle sections 11 A-F have a plurality of holes 102 a-d which define continuous flow passages 103 a-d which travel the length of the die as seen in FIG. 2 ( 103 c, d shown only).
  • Air passages 103 a-d interconnect manifold segments 11 A-F.
  • the inlets of passages 103 a-d register with groove 101 to that air entering the groove will flow the length of the die from plate 62 to plate 61 .
  • passage 103 a-d register with groove 106 in plate 61 passages which turns the air and feeds the air passages 103 e, f whereby the air flows back along the length of the die in the direction opposite that a passages 103 a-d.
  • the outlets to passages 103 e, f register with groove 107 formed in plate 62 which receives the air and turns the air to travel back along the length of the die through passage 103 g which discharges into groove 108 of end plate 61 .
  • Groove 108 feeds passage 103 h and a portion of the air travels back along the die length through passage 103 h while the rest of the air flows towards the manifold discharge through slot 109 in plate 61 .
  • Central heating element 112 heats the multi-pass air to the operating temperature.
  • Arrows 128 in FIG. 2 indicate the direction of air flow. Because the process of temperature is hotter than the polymer operating temperature a plurality of isolation holes 115 are provided in plates 61 , 62 and 11 A-F to disrupt heat flow between the process air flow and polymer flow passages of the manifold.
  • process air flows towards the manifold discharge along both sides of the manifold through slots 109 and 111 .
  • Plates 11 A-F have holes which define air passage 113 which extends the length of the die. Slots 109 and 111 discharge from opposite sides into passage 113 which feeds in parallel holes 114 A-Fwhich in turn feed associated air input 39 in die modules 12 A-F.
  • the air flows through the die modules as has been described and is discharged as converging sheets of air onto fibers 14 extruded at die tip apex 56 .
  • Each die module comprises a valve assembly 21 which is actuated by compressed air acting above or below piston 22 .
  • Instrument air is supplied to the top and bottom air chambers on each side of valve piston 22 (see FIG. 4 ) by flow lines 116 and 117 , respectively, formed in each middle plate 11 A-F.
  • Three way solenoid valve 20 D with electronic controller 120 D controls the flow of instrument air.
  • Instrument air inlet 118 is a continuous flow passage over the length of the die.
  • Passage 119 in each plate delivers the air in parallel to each of solenoid valves 20 A-F (shown schematically in FIG. 4 ). The valve delivers the air to enter passage 116 or 117 depending on whether the valve 21 is to be opened or closed. As illustrated in FIG.
  • pessurized instrument air is delivered via line 116 to the top of the piston 22 which acts to force the piston downward, while the controller 20 D simultaneously opens the air chamber below the piston to exhaust port 121 via lines 117 and 122 .
  • valve stem 25 seats on port 32 thereby closing the polymer flow passage to the die tip.
  • solenoid 20 D would deliver pressurized air to the under side of piston 22 through line 17 and would simultaneously open the upper side of the piston exhaust port 123 via line 124 .
  • the pressure beneath the piston forces the piston upward and unseats valve stem 25 to open the polymer flow passage to the die tip.
  • each die module 12 has a separate solenoid valve such that the polymer flow can be controlled through each die module independently.
  • side holes 126 and 27 which intersect passages 116 and 117 , respectively, are plugged.
  • a single solenoid valve may be used to activate valve 21 in a plurality of adjacent die modules.
  • the tops of holes 116 and 117 (labeled 116 a and 117 a) are plugged and side holes 126 and 127 opened.
  • Side holes 126 and 127 are continuous holes and will intersect each of the flow lines 116 and 117 to be controlled. This is the closed position, pressurized air would be delivered to all of the modules simultaneously through hole 126 while hole 127 would be opened to the exhaust. The instrument air flow is reversed to open the valve.
  • the modular die assembly 10 of the present invention an be tailored to meet the needs of a particular operation.
  • six die segments 11 A-F each about 0.75 inches in width are used in the assembly 10 .
  • the manifold segments 11 are bolted together as described previously, and the heater elements 97 , 112 installed.
  • the length of the heater elements 97 , 112 will be selected based on the number of segments 11 employed and will extend through most segments.
  • the die modules 12 may be mounted on each manifold segment 11 before or after interconnecting the segment 11 , and may include any of the nozzles 13 previously described.
  • FIG. 3 illustrates four modules 12 b-e with meltblowing die tips and two end modules 12 a, 12 f with spiral nozzles.
  • a particularly advantageous feature of the present invention is that it permits (a) the construction of a meltblowing die with a wide range of possible lengths, interchangeable manifold segments, and self contained modules, and (b) variation of die nozzles (e.g. meltblowing, spiral, or bead applicators) to achieve a predetermined and varied pattern.
  • Variable die length and adhesive patterns may be important for applying adhesives to substrates of different sizes from one application to another. The following sizes and numbers are illustrative of the versatility of the module die construction of the present invention.
  • a hot melt adhesive is delivered to the die 10 through line 64 , process air is delivered to the die through line 66 , and instrument air or gas is delivered through line 67 .
  • Actuation of the control valves 21 opens port 32 of each module 12 as described previously, causing polymer melt to flow through each die module 12 .
  • the melt flows through manifold passages 91 , 93 , 94 , 96 , through side ports 38 , through passages 37 and annular space 45 , and through port 32 into the die tip assembly 13 .
  • the polymer melt is distributed laterally in the die tip 13 and discharges through orifices 53 as side-by-side filaments 14 .
  • Multi-pass process air meanwhile flows through manifold passages 103 where it is heated, into slots 109 and 111 , through air passage 113 and is delivered to modules 20 A-F through ports 114 A-F, respectively.
  • the converging air sheets contact the filaments 14 discharging from the orifices 53 and by drag forces stretch them and deposit them onto the underlying substrate in a random pattern. This forms a generally uniform deposit of meltblown material on the substrate.
  • each of the flanking spiral nozzle modules 12 the polymer and air flows are basically the same, with the difference being the nozzle tip.
  • a monofilament is extruded and air jets are directed to impart a swirl on the monofilament.
  • the swirling action draws down the monofilament and deposits it as overlapping swirls on the substrate as described in the above referenced U.S. Pat. No. 5,728,129.
  • the die assembly 10 may be used in meltblowing any polymeric material, but meltblowing adhesives is the preferred polymer.
  • the adhesives include EVA's (e.g. 20-40 wt % EVA). These polymers generally have lower viscosities than those used in meltblown webs.
  • Conventional hot melt adhesives usable include those disclosed in U.S. Pat. Nos. 4,497,941, 4,325,853, and 4,315,842, the disclosures of which are incorporated herein by reference.
  • the preferred hot melt adhesives include SIS and SBS block copolymer based adhesives.
  • the adhesives contain block copolymer, tackifier, and oil in various ratios. The above melt adhesives may also be used.
  • the typical meltblowing web forming resins include a wide range of polyolefins such as propylene and ethylene homopolymers and copolymers.
  • Specific thermoplastics include ethylene acrylic copolymers, nylon, polyamides, polyesters, polystyrene, poly(methyl metharylate), polytrifluoro-chloroethylene, polyurethanes, polycarboneates, silicone sulfide, and poly(ethylene terephthalate), pitch, and blends of the above.
  • the preferred resin is polypropylene. The above list is not intended to be limiting, as new and improved meltblowing thermoplastic resins continue to be developed.
  • the invention may also be used with advantage in coating substrates of objects with thermoplastics.
  • thermoplastic polymer hot melt adhesives or those used in meltblowing webs
  • hot melt adhesives may be delivered to the die by a variety of well known means including extruders metering pumps and the like.

Abstract

A segmented die assembly comprises a plurality of side-by-side and separate units. Each die unit, includes a manifold segment and a die module mounted thereon. The manifold segments are interconnected and function to deliver process air and polymer melt to the modules. Each module including a nozzle through which the polymer melt is extruded forming a row of filament(s). The filaments from the array of modules are deposited on a substrate or collector. The die assembly is preferably used to apply a hot melt adhesive to a substrate, but also may be used to produce meltblown webs.

Description

RELATED APPLICATIONS
This application claims the benefit of U.S. Provisional Application Ser. No. 60/077,780, filed Mar. 13, 1998.
BACKGROUND OF THE INVENTION
This invention relates generally to dies for applying hot melt adhesives to a substrate or producing nonwovens. In one aspect the invention relates to a modular die provided with at least one air-assisted die tip or nozzle. In another aspect, the invention relates to a segmented die assembly comprising a plurality of separate die units, each unit including a manifold segment and a die module mounted thereon.
The deposition of hot melt adhesives onto substrates has been used in a variety of applications including diapers, sanitary napkins, surgical drapes, and the like. This technology has evolved from the application of linear beads such as that disclosed in U.S. Pat. No. 4,687,137, to air-assisted deposition such as that disclosed in U.S. Pat. No. 4,891,249, to spiral deposition such as that disclosed in U.S. Pat. Nos. 4,949,668 and 4,983,109. More recently, meltblowing dies have been adapted for the application of hot melt adhesives (see U.S. Pat. No. 5,145,689).
Modular dies have been developed to provide the user with flexibility in selecting the effective length of the die. For short die lengths only a few modules need be mounted on a manifold block. (See U.S. Pat. No. 5,618,566). Longer dies can be achieved by adding more modules to the manifold. U.S. Pat. No. 5,728,219 teaches that the modules may be provided with different types of die tips or nozzles to permit the selection of not only the die length but also the deposition pattern.
At the present, the most commonly used adhesive applicators are intermittently operated air-assisted dies. These include meltblowing dies, spiral nozzles, and spray nozzles.
Meltblowing is a process in which high velocity hot air (normally referred to as “primary air”) is used to blow molten filament extruded from a die onto a collector to form a nonwoven web or onto a substrate to form an adhesive pattern, a coating, or composite. The process employs a die provided with (a) a plurality of openings (e.g. orifices) formed in the apex of a triangular shaped die tip and (b) flanking air plates which define converging air passages. As extruded rows of the polymer melt emerge from the openings as filaments, the converging high velocity hot air from the air passages contacts the filaments and by drag forces stretches and draws them down forming microsized filaments. In some meltblowing dies, the openings are in the form of slots. In either design, the die tips are adapted to form a row of filaments which upon contact with the converging sheets of hot air are carried to and deposited on a collector or a substrate in a random pattern.
Meltblowing technology was originally developed for producing nonwoven fabrics but recently has been utilized in the meltblowing of adhesives onto substrates.
The filaments extruded from the air-assisted die may be continuous or discontinuous. For the purpose of the present invention the term “filament” is used interchangeably with the term “fiber” and refers to both continuous and discontinuous strands.
Another popular die head is a spiral spray nozzle. Spiral spray nozzles, such as those described in U.S. Pat Nos. 4,949,668 and 5,102,484, operate on the principle of a thermoplastic adhesive filament being extruded through a nozzle while a plurality of hot air jets are angularly directed onto the extruded filament to impart a circular or spiral motion thereto. The filaments thus assume an expanding swirling cone shape pattern while moving from the extrusion nozzle to the substrate. As the substrate is moved in the machine direction with respect to the nozzle, a circular or spiral or helical bead is continuously deposited on the substrate, each circular cycle being displaced from the previous cycle by a small amount in the direction of substrate movement. The meltblowing die tips offer superior coverage whereas the spiral nozzles provide better edge control.
Other adhesive applications include the older non-air assisted bead nozzles such as bead nozzles and coating nozzles.
SUMMARY OF THE INVENTION
The segmented die assembly of the present invention is of modular construction, comprising a plurality of side-by-side and interconnected die units. Each die unit includes a manifold segment and a die module mounted on the manifold segment. The die module has mounted thereon an air-assisted die tip or nozzle. The die tip may be a meltblowing type and the nozzle may be a spiral nozzle or a spray nozzle. For convenience of description, the term “nozzle” is used herein in the generic sense, meaning any air-assisted die tip or nozzle; and the term “air-assisted” means a nozzle through which is extruded a molten thermoplastic filament or filaments, and air jets, air streams, or air sheets which contact the molten filaments to divert, attenuate or change the flow pattern of the filament(s) and impart a desired characteristic to the filaments, either in terms of the size of the filaments or the deposition pattern.
The main components of each die unit, the manifold segment and the module, are provided with (a) air passages for delivering air to the nozzles and (b) a polymer flow passage for delivering a polymer melt to the nozzle. In the preferred embodiment, the nozzle is a meltblowing die tip provided with a row of orifices and flanking air slits, so that as a row of filaments are extruded through the meltblowing die tip, they are contacted with converging sheets of hot air that attenuate or draw down the filaments to microsize. As described in detail below, the nozzle may also be a spiral or spray nozzle. In practice, the die assembly may include segmented units having different types of nozzles.
The segmented die units are assembled by interconnecting several identical manifold segments, wherein the air passages and the polymer flow passage of each segment are in fluid communication. In the assembled condition, the interconnected manifold segments function much in the manner of an integrated manifold. A die module is mounted on each manifold segment and, in combination with other die modules, form a row thereon. Thus, polymer melt is extruded as a row of filaments from the array of modules and deposited on a moving substrate positioned under the assembly.
In a preferred embodiment, each module is provided with an air-actuated valve to selectively open and close the polymer flow passage. The instrument air for activating the valve is delivered through each manifold segment to the module. The valves may be individually actuated or actuated as a bank, depending on the instrument air passages and the number of control valves used.
The segmented die assembly of the present invention offers several advantages over the prior art:
    • (a) Die modules may be repeated by merely removing an existing module from an assembled manifold segment, and replacing it with a new module. This feature not only permits the replacement of faulty modules, but also permits changing the die nozzle.
    • (b) The length of the die assembly determines the effective length of the die discharge (i.e. length of the row of nozzles). In prior art designs, the length was determined by the manifold length which had to be preformed. For example, a manifold would be built to accommodate a maximum number of modules. Frequently, however, less than the maximum number would be required. This meant that several manifold sites (i.e. those without modules) would have to be sealed off. In the present invention, the manifold is made up of only the active manifold segments (i.e. those which have modules mounted thereon).
    • (c) The manifold segments are substantially identical and interchangeable, and are simple in construction. The machining of the small segments is much easier than that required for bulky integrated manifolds.
    • (d) If a manifold segment becomes plugged or damaged, it can easily be replaced by a new manifold segment. In the prior art device, the entire manifold would have to be replaced.
    • (e) The solid block manifold of the prior art, in some operations, any may include dormant polymer flow passages, as in situations where the active die length is substantially less than the length of the manifold. These dormant passages at the end of the manifold could become partially or completely plugged.
These and other advantages of the assembly of the present invention will be apparent to those skilled in the art.
BRIEF DESCRIPTION OF THE DRAWINGS
FIG. 1 is a top plan view of a segmented meltblowing die constructed according to the present invention showing polymer flow lines.
FIG. 2 is a top plan view of the present segmented die showing process air (primary air) flow lines.
FIG. 3 is front elevation view of the segmented die illustrating the discharge of filaments onto a substrate.
FIG. 4 is an enlarged sectional, view taken along plane 44 of FIG. 1 illustrating middle section of the segmented manifold.
FIG. 5 is a sectional view taken along cutting plane 55 of FIG. 1 illustrating an end plate of the segmented manifold.
FIG. 6 is a sectional view taken along cutting plane 66 of FIG. 1 illustrating the end plate of the segmented manifold opposite that shown in FIG. 5.
FIG. 7 is a sectional view of the segmented manifold taken along plane 77 of FIG. 4 illustrating the polymer flow passages.
FIG. 8 is a sectional view of the segmented manifold taken along section 88 of FIG. 4 illustrating the process air flow passages.
DESCRIPTION OF THE PREFERRED EMBODIMENTS
With reference to FIGS. 1, 2 and 3, the meltblowing die 10 of the present invention comprises a plurality of side-by-side die units 15 comprising manifold segments 11 and die modules 12. (In FIGS. 1, 2 and 3, the manifold segments are labeled 11A through 11F and the die modules are labeled 12A through 12F for the 6 segment structure.
In FIGS. 4 through 8, the manifold segments are labeled 11, it being understood that all the manifold segments are substantially identical).
In the embodiment illustrated in FIGS. 1, 2 and 3, each die unit 15 comprises a manifold segment 11, a die module 12 mounted thereon, and a valve actuator 20 for controlling the flow of polymer melt through the die segment. As shown in FIG. 3, each die module 12, has a die tip 13 which discharges filaments 14 onto a moving substrate (or collector) forming a layer or pattern of filaments on the substrate in a somewhat random fashion.
Each of the main components, manifold segment, die module, and controls is described in detail below.
Die Modules
The preferred die modules 12 are the type described in U.S. Pat. Nos. 5,618,566 and 5,728,219, the disclosures of which are which are incorporated herein by reference. It should be understood, however, that other die modules may be used. See, for example, U.S. patent application Ser. No. 09/021,426, filed Feb. 10, 1998, entitled “MODULAR DIE WITH QUICK CHANGE DIE TIP OR NOZZLE.”
As best seen in FIG. 4, each die module 12 consists of a die body 16 and a die tip 13. The die body 16 has formed therein an upper circular recess 17 and a lower circular recess 18 which are interconnected by a narrow opening 19. The upper recess 17 defines a cylindrical chamber 23 which is closed at its top by threaded plug 24. Valve assembly 21 mounted within chamber 23 comprises piston 22 having depending therefrom stem 25. The piston 22 is reciprocally movable within chamber 23, with adjustment pin 24a limiting the upward movement. Conventional o-rings may be used at the interface of the various surfaces for fluid seals as illustrated at 28.
Side ports 26 and 27 are formed in the wall of the die body 16 to provide communication to chamber 23 above and below piston 22, respectively. As described in more detail below, the ports 26 and 27 serve to conduct air (referred to as instrument gas or air) to and from each side of piston 22.
Mounted in the lower recess 18 is a threaded valve insert member 30 having a central opening 31 extending axially therethrough and terminating in valve port 32 at its lower extremity. The lower portion of insert member 30 is of reduced diameter and in combination with the die body inner wall defined a downwardly facing cavity 34. Upper portion 36 of insert member 30 abuts the top surface of recess 18 and has a plurality (e.g. 4) of circumferential ports 37 formed therein and in fluid communication with the central passage 31. An annular recess extends around the upper portion 36 interconnecting the ports 37.
Valve stem 25 extends through body opening 19 and axial opening 31 of insert member 30, and terminates at end 40 which is adapted to section valve port 32. The annular space 45 between stem 25 and opening 31 is sufficient for polymer melt to flow therethrough. End 40 of stem 25 seats on port 32 with piston 22 in its lower position within chamber 23 as illustrated in FIG. 4. As discussed below, actuation of the valve assembly 21 moves stem end 40 away from port 32 (open position), permitting the flow of polymer melt therethrough. Melt flows from the manifold 11 through side port 38, through 37, through annular space 45 discharging through port 32 into the die tip assembly 13. Conventional o-rings may be used at the interface of the various surfaces as illustrated in the drawings.
The die tip assembly 13 comprises a stack up of four parts; a transfer plate 41, a die tip 42, and two air plates 43a and 43b. The assembly 13 can be preassembled and adjusted prior to mounting onto the body 16 using bolts 50.
Transfer plate 41 is a thin metal member having a central polymer opening 44 formed therein. Two rows of air holes 49 flank the opening 44 as illustrated in FIG. 4. When mounted on the lower mounting surface of body 16, the transfer plate 41 covers the cavity 34 and therewith defines an air chamber with the air holes 49 providing outlets for air from cavity 34. Opening 44 registers with port 32 with an o-ring between these providing a fluid seal at the interface surrounding port 32. Holes 49 register with air holes 57 formed in die tip 42.
The die tip 42 comprises a base member which is co-extensive with the transfer plate 41 and the mounting surface die body 16, and a triangular nose piece 52 which may be integrally formed with the base.
The nose piece 52 terminates in apex 56 which has a row of orifices 53 spaced therealong.
Air plates 43a and 43b are in flanking relationship to the nose piece 52 and define coverging air slits which discharge at the apex of nose piece 52. Air (referred to as process air) is directed to opposite sides of the nose piece 52 into the converging slits and discharge therefrom as converging air sheets which meet at the apex of nose piece 52 and contact the filaments 14 emerging from the row of orifices 53.
The module 12 of the type disclosed in FIG. 4 is described in more detail in the above referenced U.S. Pat. No. 5,618,566. Also usable in the present invention are modules disclosed in U.S. Pat. No. 5,728,219 and U.S. patent application Ser. Nos 08/820,559 and 09/021,426. Other types of modules may also be used. The modules may dispense meltblown fibers, spirals, beads, sprays, or polymer coatings from the nozzle. Thus the module may be provided with a variety of nozzles including meltblowing nozzles, spiral spray nozzles, bead nozzles and coating nozzles.
Manifold
As seen in FIGS. 1-3, segmented manifold 11 comprises end plates 61 and 62 having sandwiched therebetween a plurality of middle section 11A- F. End plates 61 and 62 are designed to provide fluid seals at each end of the die as well as provide inlet ports for a polymer melt at 64 and an inlet for process air at 66. Inlet 64 may have removable filter cartridge 68 for removing impurities from the melt stream. As described in detail below air inlet 67 in plate 62 provides air, referred to as instrument air for opening control valves 20A-F in the modules 12A-F, respectively.
As seen in FIGS. 1, 2, 5 and 6 end plate 62 has threaded bolt holes 71a-d which align with countersunk bolt holes 72a-d in middle plate 11A (only 72a and b shown in FIGS. 1 and 2, respectively). End plate 61 has countersunk holes 73a-d which align with thread holes 74a-d (only 74a, b shown) in middle plate 11F. Countersunk bolts 79 thus join plate 62 to plate 11 A leaving surface 81 flush for adjoining middle plate 11B to 11A, and flush surface 82 for joining end plate 61 to middle plate 11F.
Adjacent middle sections 11A-F are joined by bolts 85 arranged in an alternating pattern of threaded and countersunk bolt holes. As seen in FIG. 4, middle section 11D has four bored and countersunk bolt holes 86a-d and four threaded bolt holes 87a-d. Plates 11C and 11E flank 11D and have bolt holes which align with holes 86a-d and 87a-d, however, the pattern of countersunk holes and threaded holes are interchanged in the flanking plates. The countersunk bored holes 86a-d in plate 11D will align with threaded holes in plate 11C, and threaded holes 87a-d will align with bored and countersunk holes in plate 11E (see FIGS. 1 and 2). This design of interchanging the pattern of countersunk holes and threaded holes in adjacent plates is repeated over the length of the die. Countersunk holes 86a-d are of sufficient depth so that the heads of bolt 85 do not protrude beyond the outer lateral surface of the middle sections and thus permits the abutting surfaces of adjacent sections to be flush when bolts 85 are tightened. Tightening of bolts 85 establishes a metal-on-metal fluid seal between adjacent plates. O-rings may also be used to seal adjacent plates.
Polymer Flow
Referring to FIGS. 1, 4 and 7, middle sections 11A-F have central polymer flow passage 91 (see FIG. 4) which, when bolted together define continuous flow passage 92 which extends the length of the die. Polymer passage 92 interconnects manifold segments 11A-F. A polymer melt enters the die through inlet 64 and flows into passage 92. Each middle plate has a hole 93A-F (see FIG. 7) which leads from passage 92 into second continuous passage 94 and holes 96A-F which is the outlet of the manifold and feeds polymer to die modules 12A-F in parallel. The outlet of passages 96A-F register with the polymer inlet 38 (see FIG. 4) of each die module. The lateral surfaces of middle plates 11A-F and end plates 61 and 62 are precisely machined whereby a fluid seal is established at the interfaces when the plates are bolted together by bolts 85 as has been described.
Polymer melt thus enters the die through plate 61 at 64, fills passage 92, flows in parallel through holes 93A-F, fills continuous passage 94, flows in parllel through holes 96A-F, and enters die modules 12A-F through passages 38 (see FIG. 4). The polymer which enters the die modules is extruded to form filaments 14 as has been described. The polymer manifold design wherein the polymer flows between the two continuous passages 92 and 94 via a plurality of parallel holes serves to equalize the flow over the die length. Heating element 97 maintains the polymer of the proper operating temperature.
Process Air
Referring to FIGS. 2, 4, 5 and 6. Heated process air enters through inlet 66 which registers with the circular groove 101 (FIG. 6) formed along the inner wall of end plate 62. Middle sections 11A-F have a plurality of holes 102a-d which define continuous flow passages 103a-d which travel the length of the die as seen in FIG. 2 (103c, d shown only). Air passages 103a-d interconnect manifold segments 11A-F. The inlets of passages 103a-d register with groove 101 to that air entering the groove will flow the length of the die from plate 62 to plate 61. The outlets of passage 103a-d register with groove 106 in plate 61 passages which turns the air and feeds the air passages 103e, f whereby the air flows back along the length of the die in the direction opposite that a passages 103a-d. The outlets to passages 103e, f register with groove 107 formed in plate 62 which receives the air and turns the air to travel back along the length of the die through passage 103g which discharges into groove 108 of end plate 61. Groove 108 feeds passage 103h and a portion of the air travels back along the die length through passage 103h while the rest of the air flows towards the manifold discharge through slot 109 in plate 61. Air which returns to plate 62 via 103h flows towards the manifold discharge through slot 111. Thus the air makes three or four passes along the length of the die before being discharge to the die modules. Central heating element 112 heats the multi-pass air to the operating temperature. Arrows 128 in FIG. 2 indicate the direction of air flow. Because the process of temperature is hotter than the polymer operating temperature a plurality of isolation holes 115 are provided in plates 61, 62 and 11A-F to disrupt heat flow between the process air flow and polymer flow passages of the manifold.
As seen in FIGS. 2 and 8, process air flows towards the manifold discharge along both sides of the manifold through slots 109 and 111. Plates 11A-F have holes which define air passage 113 which extends the length of the die. Slots 109 and 111 discharge from opposite sides into passage 113 which feeds in parallel holes 114A-Fwhich in turn feed associated air input 39 in die modules 12A-F. The air flows through the die modules as has been described and is discharged as converging sheets of air onto fibers 14 extruded at die tip apex 56.
Instrument Air
Each die module comprises a valve assembly 21 which is actuated by compressed air acting above or below piston 22. Instrument air is supplied to the top and bottom air chambers on each side of valve piston 22 (see FIG. 4) by flow lines 116 and 117, respectively, formed in each middle plate 11A-F. Three way solenoid valve 20D with electronic controller 120D controls the flow of instrument air. Instrument air inlet 118 is a continuous flow passage over the length of the die. Passage 119 in each plate delivers the air in parallel to each of solenoid valves 20A-F (shown schematically in FIG. 4). The valve delivers the air to enter passage 116 or 117 depending on whether the valve 21 is to be opened or closed. As illustrated in FIG. 4, pessurized instrument air is delivered via line 116 to the top of the piston 22 which acts to force the piston downward, while the controller 20D simultaneously opens the air chamber below the piston to exhaust port 121 via lines 117 and 122. In the downward position, valve stem 25 seats on port 32 thereby closing the polymer flow passage to the die tip. In the open position, solenoid 20D would deliver pressurized air to the under side of piston 22 through line 17 and would simultaneously open the upper side of the piston exhaust port 123 via line 124. The pressure beneath the piston forces the piston upward and unseats valve stem 25 to open the polymer flow passage to the die tip. Thus in the preferred mode each die module 12 has a separate solenoid valve such that the polymer flow can be controlled through each die module independently. In this mode side holes 126 and 27 which intersect passages 116 and 117, respectively, are plugged.
In a second preferred embodiment a single solenoid valve may be used to activate valve 21 in a plurality of adjacent die modules. In this configuration the tops of holes 116 and 117 (labeled 116a and 117a) are plugged and side holes 126 and 127 opened. Side holes 126 and 127 are continuous holes and will intersect each of the flow lines 116 and 117 to be controlled. This is the closed position, pressurized air would be delivered to all of the modules simultaneously through hole 126 while hole 127 would be opened to the exhaust. The instrument air flow is reversed to open the valve.
Assembly and Operation
As indicated above, the modular die assembly 10 of the present invention an be tailored to meet the needs of a particular operation. As exemplified in FIGS. 1, 2 and 3, six die segments 11A-F, each about 0.75 inches in width are used in the assembly 10. The manifold segments 11 are bolted together as described previously, and the heater elements 97, 112 installed. The length of the heater elements 97, 112 will be selected based on the number of segments 11 employed and will extend through most segments. The die modules 12 may be mounted on each manifold segment 11 before or after interconnecting the segment 11, and may include any of the nozzles 13 previously described. FIG. 3 illustrates four modules 12b-e with meltblowing die tips and two end modules 12a, 12f with spiral nozzles.
A particularly advantageous feature of the present invention is that it permits (a) the construction of a meltblowing die with a wide range of possible lengths, interchangeable manifold segments, and self contained modules, and (b) variation of die nozzles (e.g. meltblowing, spiral, or bead applicators) to achieve a predetermined and varied pattern. Variable die length and adhesive patterns may be important for applying adhesives to substrates of different sizes from one application to another. The following sizes and numbers are illustrative of the versatility of the module die construction of the present invention.
Preferred
Die Assembly Broad Range Range Best Mode
Number of    2-1.000  2-100  5-50
Units (15)
Length of each  0.25-1.50″  0.5-1.00″  0.5-0.8″
Unit (15) (inches)
Orifice (53)  0.005-0.050″  0.01-0.040″  0.015-0.030″
Diameter (inches)
Orifices/Inch*  5-50 10-40 10-30
Different Types 2-4 2-3 2
of Nozzles (13)
*filaments per inch per slot.
The lines, instruments, and controls are connected and operation commenced. A hot melt adhesive is delivered to the die 10 through line 64, process air is delivered to the die through line 66, and instrument air or gas is delivered through line 67.
Actuation of the control valves 21 opens port 32 of each module 12 as described previously, causing polymer melt to flow through each die module 12. In the meltblowing modules 15, the melt flows through manifold passages 91, 93, 94, 96, through side ports 38, through passages 37 and annular space 45, and through port 32 into the die tip assembly 13. The polymer melt is distributed laterally in the die tip 13 and discharges through orifices 53 as side-by-side filaments 14. Multi-pass process air meanwhile flows through manifold passages 103 where it is heated, into slots 109 and 111, through air passage 113 and is delivered to modules 20A-F through ports 114A-F, respectively. Air enters each module 12 through port 39 and flows through holes 49 and 57 and into slits discharging as converging air sheets at or near the die tip apex of the nose piece 52. The converging air sheets contact the filaments 14 discharging from the orifices 53 and by drag forces stretch them and deposit them onto the underlying substrate in a random pattern. This forms a generally uniform deposit of meltblown material on the substrate.
In each of the flanking spiral nozzle modules 12, the polymer and air flows are basically the same, with the difference being the nozzle tip. In the spiral nozzle, a monofilament is extruded and air jets are directed to impart a swirl on the monofilament. The swirling action draws down the monofilament and deposits it as overlapping swirls on the substrate as described in the above referenced U.S. Pat. No. 5,728,129.
Typical operational parameters are as follows:
Polymer Hot melt adhesive
Temperature of the 280° F. to 325° F.
Die and Polymer
Temperature of Air 280° F. to 325° F.
Polymer Flow Rate 0.1 to 10 grms/hole/min.
Hot air Flow Rate 0.1 to 2 SCFM/inch
Deposition 0.05 to 500 g/m2
As described above, the die assembly 10 may be used in meltblowing any polymeric material, but meltblowing adhesives is the preferred polymer. The adhesives include EVA's (e.g. 20-40 wt % EVA). These polymers generally have lower viscosities than those used in meltblown webs. Conventional hot melt adhesives usable include those disclosed in U.S. Pat. Nos. 4,497,941, 4,325,853, and 4,315,842, the disclosures of which are incorporated herein by reference. The preferred hot melt adhesives include SIS and SBS block copolymer based adhesives. The adhesives contain block copolymer, tackifier, and oil in various ratios. The above melt adhesives may also be used.
Although the present invention has been described with reference to meltblowing hot melt adhesive, it is to be understood that the invention may also be used to meltblow polymer in the manufacture of webs. The dimensions of the die tip may have a small difference in certain features as described in the above referenced U.S. Pat. Nos. 5,145,689 and 5,618,566.
The typical meltblowing web forming resins include a wide range of polyolefins such as propylene and ethylene homopolymers and copolymers. Specific thermoplastics include ethylene acrylic copolymers, nylon, polyamides, polyesters, polystyrene, poly(methyl metharylate), polytrifluoro-chloroethylene, polyurethanes, polycarboneates, silicone sulfide, and poly(ethylene terephthalate), pitch, and blends of the above. The preferred resin is polypropylene. The above list is not intended to be limiting, as new and improved meltblowing thermoplastic resins continue to be developed.
The invention may also be used with advantage in coating substrates of objects with thermoplastics.
The thermoplastic polymer, hot melt adhesives or those used in meltblowing webs, may be delivered to the die by a variety of well known means including extruders metering pumps and the like.

Claims (16)

1. A segmented die assembly, comprising:
(a) a plurality of manifold segments, each manifold segment having a polymer flow passage and an air flow passage formed therein; said manifold segment being interconnected in side-by-side relationship wherein said air passages and polymer passages are in fluid communication, respectively;
(b) a die module mounted on each manifold segment, said die module comprising a die body having a polymer flow passage and an air flow passage in fluid communication with said polymer flow passage and said air flow passage of its associated manifold segment, respectively; and a die tip or nozzle mounted on said die body and having a polymer flow passage in fluid communication with said polymer flow passage of its associated die body for receiving the polymer melt and discharging a filament or filaments therefrom;
(c) means for delivering a polymer melt to at least one manifold segment whereby the melt is distributed through said other interconnected manifold segments and flows through each die module discharging as a filament or filaments from each die tip or nozzle; and
(d) means for delivering air to at least one manifold segment whereby air is distributed in said interconnected manifold segments and flows through each die module discharging through said die tip or nozzle.
2. The die assembly of claim 1 wherein said die tip or nozzle is selected from the group consisting of meltblowing die tip, spiral spray nozzle, spray nozzle, bead nozzle, and coating nozzle.
3. The assembly of claim 2 wherein said die tip on at least one module is a meltblowing die tip.
4. The die assembly of claim 1 wherein said die tip on each die module is air assisted having air passages formed therein, said air passages of said die tip being in fluid communication with said air flow passages of said die body on which it is mounted.
5. The die assembly of claim 1 wherein each die module has an air actuated valve mounted therein to open and close said polymer flow passage therein and each manifold segment having instrument air flow passages formed therein for delivering air to and from said air actuated valve, said assembly further comprising control means for selectively delivering air to and from said instrument air passages of said manifold segment.
6. The die assembly of claim 1 wherein said manifold segments are identical.
7. The die assembly of claim 1 wherein said assembly comprises from 2 to 100 die segments.
8. The die assembly of claim 1 wherein each manifold segment and said die module mounted thereon is from 0.25 to 1.5 inches in width.
9. The die assembly of claim 1 wherein each manifold segment includes electric heaters for heating said polymer and said air and wherein said air flow passage of a particular manifold segment is in fluid communication with said air passages of said other manifold segments whereby air flows through each manifold segment before flowing to said die module mounted on said particular manifold segment.
10. A meltblowing die comprising:
(a) a manifold with at least two manifold segments, each segment having a polymer flow passage and an air flow passage, said polymer flow passages and air flow passages being interconnected, respectively;
(b) a die module secured in each manifold segment, each die module having a polymer flow passage which registers with its associated manifold segment polymer flow passage, an air flow passage which registers with its associated manifold segment air flow passage, a die tip or nozzle for discharging polymer as a filament or filaments, and an air flow discharge for delivering air onto said filament or filaments;
(c) means for delivering a polymer melt to at least one of said manifold segments whereby said melt flows through said interconnected polymer flow passages of each manifold segment and is delivered to said associated die modules; and
(d) means for delivering air to at least one of said interconnected manifold segments whereby said air flows through each manifold segment and is delivered to said associated die modules.
11. The meltblowing die of claim 10 further comprising valve means for selectively controlling the flow of polymer melt through each die module independently.
12. A segmented die assembly comprising a plurality of separate air-assisted die units interconnected in side-by-side relationship, each die unit comprising:
a) a manifold segment having formed therein (i) a process air flow passage, (ii) a polymer flow passage, and (iii) and instrument air flow passage, said process air flow passages and said polymer flow passages respectively being in fluid communication;
b) a die module having a die body detachably mounted on said manifold segment, and an air-assisted die tip or nozzle mounted on said die body, said die body having formed therein (i) a process air flow passage, (ii) a polymer flow passage and (iii) an instrument air flow passage which, respectively, are in fluid communication with said process air flow passage, said polymer flow passage, and said instrument air flow passage of said manifold segment, said die body further having an air-actuated valve mounted therein for opening and closing said polymer flow passage thereof, which is in fluid communication with instrument air flow passage thereof;
said tip having (i) a process air flow passage and (ii) a polymer flow passage which, respectively, are in fluid communication with said process air flow passage and said polymer flow passage of said die body; and
c) means for selectively delivering air to and from said instrument air flow passages of said manifold segment for actuating said air-actuated valve.
13. The segmented die assembly of claim 12 wherein said die assembly comprises from 5 to 50 die units.
14. A die assembly comprising:
a manifold having first and second sections, a fluid passageway in said first section for conveying therethrough a material to be dispensed, and an air passageway in said second section for conveying therethrough process air to be discharged adjacent the material being dispensed,
first and second heaters respectively contained in said first and second sections and configured to separately heat the material in said fluid passageway and the process air in said air passageway to different temperatures,
a plurality of holes positioned between said first and second sections to disrupt the flow of heat between said fluid passageway and said air passageway,
a dispensing valve coupled with said manifold for receiving and dispensing the material conveyed through said fluid passageway of said first section and for receiving and discharging the process air conveyed through said air passageway of said second section.
15. A segmented die assembly comprising first and second side by side die units, each of said first and second die units comprising:
(a) an integral manifold block formed from a single piece of material having first and second sections, a fluid passageway in said first section for conveying therethrough a material to be dispensed, an air passageway in said second section for conveying therethrough process air to be discharged adjacent the material being dispensed, a front wall and a pair of oppositely disposed side walls,
(b) first and second heaters respectively contained in said first and second sections and configured to separately heat the material in said fluid passageway and the process air in said air passageway to different temperatures,
(c) a thermal isolator hole positioned between said first and second manifold block sections to disrupt the flow of heat between said fluid passageway and said air passageway, and
(d) a dispensing valve mounted upon said front wall of said manifold block for receiving and dispensing the material conveyed through said fluid passageway of said first section and for receiving and discharging the process air conveyed through said air passageway of said second section, and
a fastener connecting one of said oppositely disposed side walls of said manifold block of said first die unit to one of said oppositely disposed side walls of said manifold block of said second die unit.
16. The segmented die assembly of claim 15, wherein said thermal isolator comprises a plurality of holes in said manifold block, said holes located between said first and second sections.
US10/420,569 1998-03-13 2003-04-22 Segmented die for applying hot melt adhesives or other polymer melts Expired - Lifetime USRE39399E1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US10/420,569 USRE39399E1 (en) 1998-03-13 2003-04-22 Segmented die for applying hot melt adhesives or other polymer melts

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US7778098P 1998-03-13 1998-03-13
US09/138,039 US6220843B1 (en) 1998-03-13 1998-08-20 Segmented die for applying hot melt adhesives or other polymer melts
US10/420,569 USRE39399E1 (en) 1998-03-13 2003-04-22 Segmented die for applying hot melt adhesives or other polymer melts

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
US09/138,039 Reissue US6220843B1 (en) 1998-03-13 1998-08-20 Segmented die for applying hot melt adhesives or other polymer melts

Publications (1)

Publication Number Publication Date
USRE39399E1 true USRE39399E1 (en) 2006-11-14

Family

ID=26759661

Family Applications (2)

Application Number Title Priority Date Filing Date
US09/138,039 Ceased US6220843B1 (en) 1998-03-13 1998-08-20 Segmented die for applying hot melt adhesives or other polymer melts
US10/420,569 Expired - Lifetime USRE39399E1 (en) 1998-03-13 2003-04-22 Segmented die for applying hot melt adhesives or other polymer melts

Family Applications Before (1)

Application Number Title Priority Date Filing Date
US09/138,039 Ceased US6220843B1 (en) 1998-03-13 1998-08-20 Segmented die for applying hot melt adhesives or other polymer melts

Country Status (7)

Country Link
US (2) US6220843B1 (en)
EP (1) EP1062051B1 (en)
JP (1) JP4611521B2 (en)
CN (1) CN1102079C (en)
AU (1) AU3001699A (en)
DE (1) DE69917234T2 (en)
WO (1) WO1999046057A1 (en)

Cited By (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090065611A1 (en) * 2006-01-06 2009-03-12 Nordson Corporation Liquid dispenser having individualized process air control
US20100018996A1 (en) * 2002-01-28 2010-01-28 Nordson Corporation Process air-assisted dispensing systems
US20100155323A1 (en) * 2008-12-23 2010-06-24 Weiss Douglas E Functionalized nonwoven article
WO2010151447A1 (en) 2009-06-23 2010-12-29 3M Innovative Properties Company Functionalized nonwoven article
US20110052811A1 (en) * 2009-08-31 2011-03-03 Illinois Tool Works Inc. Metering system for simultaneously dispensing two different adhensives from a single metering device or applicator onto a common substrate
US20110052812A1 (en) * 2009-08-31 2011-03-03 Illinois Tool Works Inc. Metering system for simultaneously dispensing two different adhesives from a single metering device or applicator onto a common substrate
WO2012012172A2 (en) 2010-06-30 2012-01-26 3M Innovative Properties Company Filter plate article having a water-absorbent filter assembly
US8377672B2 (en) 2010-02-18 2013-02-19 3M Innovative Properties Company Ligand functionalized polymers
US8435776B2 (en) 2010-03-03 2013-05-07 3M Innovative Properties Company Ligand functionalized polymers
US20130206062A1 (en) * 2012-02-10 2013-08-15 Palo Alto Research Center Incoproated Micro-Extrusion Printhead With Offset Orifices For Generating Gridlines On Non-Square Substrates
WO2013162695A1 (en) 2012-04-24 2013-10-31 3M Innovative Properties Company Nonwoven article gafter with copolymer
US8586338B2 (en) 2008-05-30 2013-11-19 3M Innovative Properties Company Ligand functionalized substrates
US8652582B2 (en) 2008-05-30 2014-02-18 3M Innovative Properties Company Method of making ligand functionalized substrates
US8906645B2 (en) 2010-12-29 2014-12-09 3M Innovative Properties Company Microbial detection article having a water-absorbent filter assembly
US8939330B2 (en) 2013-03-13 2015-01-27 Graco Minnesota Inc. Removable module service seat
US9120190B2 (en) 2011-11-30 2015-09-01 Palo Alto Research Center Incorporated Co-extruded microchannel heat pipes
US9126222B2 (en) 2009-07-17 2015-09-08 Illinois Tool Works Inc. Metering system for hot melt adhesives with variable adhesive volumes
US9156053B2 (en) 2011-10-27 2015-10-13 Graco Minnesota Inc. Melter
US9174231B2 (en) 2011-10-27 2015-11-03 Graco Minnesota Inc. Sprayer fluid supply with collapsible liner
US9796492B2 (en) 2015-03-12 2017-10-24 Graco Minnesota Inc. Manual check valve for priming a collapsible fluid liner for a sprayer
US10371468B2 (en) 2011-11-30 2019-08-06 Palo Alto Research Center Incorporated Co-extruded microchannel heat pipes
US10526729B2 (en) 2014-02-24 2020-01-07 Nanofiber, Inc. Melt blowing die, apparatus and method
US10988827B2 (en) 2015-03-16 2021-04-27 3M Innovative Properties Company Coalescing elements in copper production
US11110483B2 (en) * 2017-10-31 2021-09-07 Nordson Corporation Liquid material dispensing system having a sleeve heater
US20210387225A1 (en) * 2018-11-09 2021-12-16 Illinois Tool Works Inc. Modular fluid application device for varying fluid coat weight
WO2022136968A1 (en) 2020-12-23 2022-06-30 3M Innovative Properties Company Method of separating a virus from a composition using copolymer-grafted nonwoven substrates
WO2023031696A1 (en) 2021-09-01 2023-03-09 3M Innovative Properties Company Nonwoven with bio particles and methods of making the same
WO2023037178A1 (en) 2021-09-08 2023-03-16 3M Innovative Properties Company Method of harvesting biologics
US11707753B2 (en) 2019-05-31 2023-07-25 Graco Minnesota Inc. Handheld fluid sprayer
US11752517B2 (en) 2020-09-29 2023-09-12 C3 Corporation Hotmelt application system and process

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6422428B1 (en) * 1998-04-20 2002-07-23 Nordson Corporation Segmented applicator for hot melt adhesives or other thermoplastic materials
DE10023673B4 (en) 2000-05-16 2007-11-22 Nordson Corp., Westlake Distribution device for distributing fluids and device for dispensing and applying fluid, in particular adhesive
US6260583B1 (en) * 2000-05-24 2001-07-17 Illinois Tool Works Inc. Segmented stackable head design
US6499631B2 (en) * 2001-01-26 2002-12-31 Illinois Tool Works Inc. Hot melt adhesive applicator
US6861025B2 (en) * 2002-06-20 2005-03-01 3M Innovative Properties Company Attenuating fluid manifold for meltblowing die
US6846450B2 (en) 2002-06-20 2005-01-25 3M Innovative Properties Company Method for making a nonwoven web
US6874708B2 (en) 2003-02-13 2005-04-05 Illinois Tool Works Inc. Automatic air-assisted manifold mounted gun
US7018188B2 (en) * 2003-04-08 2006-03-28 The Procter & Gamble Company Apparatus for forming fibers
DE10330751A1 (en) * 2003-07-07 2005-02-10 Windmöller & Hölscher Kg Floor laying device for paper sacks
US20050015050A1 (en) * 2003-07-15 2005-01-20 Kimberly-Clark Worldwide, Inc. Apparatus for depositing fluid material onto a substrate
US7632086B2 (en) * 2003-10-03 2009-12-15 Exxonmobil Chemical Patents Inc. Melt fracture reduction
US7168932B2 (en) * 2003-12-22 2007-01-30 Kimberly-Clark Worldwide, Inc. Apparatus for nonwoven fibrous web
US6972104B2 (en) * 2003-12-23 2005-12-06 Kimberly-Clark Worldwide, Inc. Meltblown die having a reduced size
US20050233667A1 (en) * 2004-04-16 2005-10-20 Tamko Roofing Products, Inc. System and method for manufacturing polymer mat with reduced capacity spinning pumps
US20050242108A1 (en) * 2004-04-30 2005-11-03 Nordson Corporation Liquid dispenser having individualized process air control
US20050284338A1 (en) * 2004-06-01 2005-12-29 Dwyer Patrick A Hot melt adhesive
US7316552B2 (en) * 2004-12-23 2008-01-08 Kimberly-Clark Worldwide, Inc. Low turbulence die assembly for meltblowing apparatus
US7908997B2 (en) * 2007-06-04 2011-03-22 Illinois Tool Works Inc. Hybrid hot melt adhesive or other thermoplastic material dispensing system
ES2334958B1 (en) * 2007-12-03 2011-02-03 Meler Aplicadores De Hot-Melt S.A. MODULAR ASSEMBLY FOR APPLICATION OF TERMOFUSIBLE PRODUCTS.
US8584613B2 (en) * 2008-06-30 2013-11-19 Lam Research Corporation Single substrate processing head for particle removal using low viscosity fluid
DE102009020077A1 (en) * 2009-05-06 2010-11-11 Dürr Systems GmbH Coating agent device and coating device
EP2248599B1 (en) * 2009-05-07 2013-08-07 Robatech AG Device with multiple high pressure nozzles and protection chamber and method for discharging an adhesive
EP2248598B2 (en) * 2009-05-07 2016-06-08 Robatech AG Device with multiple dry air nozzles and method for discharging an adhesive
JP5784025B2 (en) * 2009-10-05 2015-09-24 ノードソン コーポレーションNordson Corporation Two-component liquid discharge gun and system
DE102010051809A1 (en) 2009-12-17 2011-06-22 Heidelberger Druckmaschinen AG, 69115 Method for producing security features on a printing- or packaging product, comprises producing a random pattern on a substrate through material deposition, where the material is applied as a fiber, which is produced by a coating nozzle
WO2011123503A1 (en) 2010-04-01 2011-10-06 B & H Manufacturing Company, Inc. Extrusion application system
CN204805172U (en) 2012-08-10 2015-11-25 安德烈·尤利维奇·亚济科夫 Automatic pump bracket
JP2014100644A (en) * 2012-11-19 2014-06-05 Anest Iwata Corp Spray gun
US9587329B2 (en) * 2013-12-11 2017-03-07 Kyung-Ju Choi Process for making a polymeric fibrous material having increased beta content
DE102014001897A1 (en) * 2014-02-14 2015-08-20 Focke & Co. (Gmbh & Co. Kg) Valve arrangement for applying flowable media to surfaces
US10363567B2 (en) * 2016-02-29 2019-07-30 The Boeing Company Apparatuses for applying a glutinous substance
CN111556909B (en) 2017-11-22 2024-04-09 挤压集团公司 Meltblowing die tip assembly and method
US20200291261A1 (en) 2017-11-30 2020-09-17 Axalta Coating Systems Gmbh Coating compositions for application utilizing a high transfer efficiency applicator and methods and systems thereof
CN110409031B (en) * 2019-08-23 2021-08-06 江苏工程职业技术学院 Micro-nanofiber multilayer structure covering yarn spinning device and production process thereof

Citations (50)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3849241A (en) 1968-12-23 1974-11-19 Exxon Research Engineering Co Non-woven mats by melt blowing
US3985481A (en) 1974-12-09 1976-10-12 Rothmans Of Pall Mall Canada Limited Extrusion head for producing polymeric material fibres
US4051861A (en) 1975-11-03 1977-10-04 Skinner Precision Industries, Inc. Arrangement for connecting manifold blocks
US4073850A (en) 1974-12-09 1978-02-14 Rothmans Of Pall Mall Canada Limited Method of producing polymeric material
US4079864A (en) 1976-12-15 1978-03-21 Cox James R Manifold for liquid dispensing apparatus
US4138208A (en) * 1977-02-07 1979-02-06 The Dow Chemical Company Die face cutter
US4478624A (en) 1981-08-06 1984-10-23 Isover Saint-Gobain Process and apparatus for improving the distribution on a receiving device of fibers carried by a gas current
US4526733A (en) 1982-11-17 1985-07-02 Kimberly-Clark Corporation Meltblown die and method
DE8534594U1 (en) 1985-12-09 1986-02-06 Claassen, Henning J., 2120 Lüneburg Spray head for spraying a thermoplastic material, in particular a hot melt adhesive
US4687137A (en) 1986-03-20 1987-08-18 Nordson Corporation Continuous/intermittent adhesive dispensing apparatus
US4708619A (en) 1985-02-27 1987-11-24 Reifenhauser Gmbh & Co. Maschinenfabrik Apparatus for spinning monofilaments
US4785996A (en) 1987-04-23 1988-11-22 Nordson Corporation Adhesive spray gun and nozzle attachment
US4815660A (en) 1987-06-16 1989-03-28 Nordson Corporation Method and apparatus for spraying hot melt adhesive elongated fibers in spiral patterns by two or more side-by-side spray devices
US4891249A (en) 1987-05-26 1990-01-02 Acumeter Laboratories, Inc. Method of and apparatus for somewhat-to-highly viscous fluid spraying for fiber or filament generation, controlled droplet generation, and combinations of fiber and droplet generation, intermittent and continuous, and for air-controlling spray deposition
US4983109A (en) 1988-01-14 1991-01-08 Nordson Corporation Spray head attachment for metering gear head
US5145689A (en) 1990-10-17 1992-09-08 Exxon Chemical Patents Inc. Meltblowing die
US5156715A (en) * 1987-02-09 1992-10-20 Southwire Company Apparatus for applying two layers of plastic to a conductor
US5165940A (en) * 1992-04-23 1992-11-24 E. I. Du Pont De Nemours And Company Spinneret
US5236641A (en) 1991-09-11 1993-08-17 Exxon Chemical Patents Inc. Metering meltblowing system
WO1994001221A1 (en) 1992-07-08 1994-01-20 Nordson Corporation Segmented slot die for air spray of fibers
US5294258A (en) * 1992-04-08 1994-03-15 Nordson Corporation Apparatus for producing an integral adhesive matrix
US5336320A (en) 1992-06-30 1994-08-09 Nordson Corporation Fast response film coater
US5368233A (en) 1993-09-01 1994-11-29 Nordson Corporation Spray disk for close centerline spacing
US5382312A (en) 1992-04-08 1995-01-17 Nordson Corporation Dual format adhesive apparatus for intermittently disrupting parallel, straight lines of adhesive to form a band
US5445674A (en) 1992-03-06 1995-08-29 The Pillsbury Company Device for dispensing thixotropic sauce onto pizza crusts
US5453129A (en) * 1991-05-08 1995-09-26 Exxon Chemical Patents Inc. Oil spill recovery method
US5478224A (en) 1994-02-04 1995-12-26 Illinois Tool Works Inc. Apparatus for depositing a material on a substrate and an applicator head therefor
US5605720A (en) 1996-04-04 1997-02-25 J & M Laboratories Inc. Method of continuously formulating and applying a hot melt adhesive
US5618566A (en) 1995-04-26 1997-04-08 Exxon Chemical Patents, Inc. Modular meltblowing die
US5645743A (en) 1995-05-18 1997-07-08 Illinois Tool Works Inc. Multiple heat source grid assembly
US5679379A (en) 1995-01-09 1997-10-21 Fabbricante; Anthony S. Disposable extrusion apparatus with pressure balancing modular die units for the production of nonwoven webs
US5683578A (en) 1995-05-15 1997-11-04 Illinois Tool Works Inc. Filter valve system for regulating, filtering, and dispensing a flow of hot melt materials and adhesives
US5728219A (en) 1995-09-22 1998-03-17 J&M Laboratories, Inc. Modular die for applying adhesives
US5728407A (en) * 1995-05-26 1998-03-17 Japan Vilene Company, Ltd. Die for melt-blowing apparatus
US5747102A (en) 1995-11-16 1998-05-05 Nordson Corporation Method and apparatus for dispensing small amounts of liquid material
US5806720A (en) 1996-07-19 1998-09-15 Illinois Tool Works Inc. Multi position palletizer head for adhesive supply unit
US5875922A (en) * 1997-10-10 1999-03-02 Nordson Corporation Apparatus for dispensing an adhesive
US6210141B1 (en) * 1998-02-10 2001-04-03 Nordson Corporation Modular die with quick change die tip or nozzle
US6253957B1 (en) 1995-11-16 2001-07-03 Nordson Corporation Method and apparatus for dispensing small amounts of liquid material
US6260583B1 (en) 2000-05-24 2001-07-17 Illinois Tool Works Inc. Segmented stackable head design
US6296463B1 (en) 1998-04-20 2001-10-02 Nordson Corporation Segmented metering die for hot melt adhesives or other polymer melts
US6422848B1 (en) 1997-03-19 2002-07-23 Nordson Corporation Modular meltblowing die
US6423227B1 (en) 1997-02-07 2002-07-23 Nordson Corporation Meltblown yarn and method and apparatus for manufacturing
US6422428B1 (en) 1998-04-20 2002-07-23 Nordson Corporation Segmented applicator for hot melt adhesives or other thermoplastic materials
US6427745B1 (en) 1998-03-03 2002-08-06 Nordson Corporation Apparatus for the manufacture of nonwoven webs and laminates
US6478563B1 (en) 2000-10-31 2002-11-12 Nordson Corporation Apparatus for extruding multi-component liquid filaments
US6491507B1 (en) 2000-10-31 2002-12-10 Nordson Corporation Apparatus for meltblowing multi-component liquid filaments
US6499982B2 (en) 2000-12-28 2002-12-31 Nordson Corporation Air management system for the manufacture of nonwoven webs and laminates
US6499631B2 (en) * 2001-01-26 2002-12-31 Illinois Tool Works Inc. Hot melt adhesive applicator
US6502615B1 (en) 1999-12-22 2003-01-07 Nordson Corporation Apparatus for making an absorbent composite product

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2142698A (en) 1931-12-23 1939-01-03 Packard Motor Car Co Internal combustion engine
US2055997A (en) 1934-03-28 1936-09-29 Clarence O Brandow Draft equipment
DE2932190A1 (en) 1978-08-09 1980-02-28 Nippon Oil Co Ltd MELTABLE RESIN
US4325853A (en) 1980-07-31 1982-04-20 Gulf Oil Corporation Hot melt adhesive compositions containing rosin esters
US4497941A (en) 1981-10-16 1985-02-05 Exxon Research & Engineering Co. Ethylene copolymers for hot melt systems
US4949668A (en) 1988-06-16 1990-08-21 Kimberly-Clark Corporation Apparatus for sprayed adhesive diaper construction
US5102484A (en) 1990-06-26 1992-04-07 J&M Consultants Inc. Method and apparatus for generating and depositing adhesives and other thermoplastics in swirls

Patent Citations (53)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3849241A (en) 1968-12-23 1974-11-19 Exxon Research Engineering Co Non-woven mats by melt blowing
US3985481A (en) 1974-12-09 1976-10-12 Rothmans Of Pall Mall Canada Limited Extrusion head for producing polymeric material fibres
US4073850A (en) 1974-12-09 1978-02-14 Rothmans Of Pall Mall Canada Limited Method of producing polymeric material
US4051861A (en) 1975-11-03 1977-10-04 Skinner Precision Industries, Inc. Arrangement for connecting manifold blocks
US4079864A (en) 1976-12-15 1978-03-21 Cox James R Manifold for liquid dispensing apparatus
US4138208A (en) * 1977-02-07 1979-02-06 The Dow Chemical Company Die face cutter
US4478624A (en) 1981-08-06 1984-10-23 Isover Saint-Gobain Process and apparatus for improving the distribution on a receiving device of fibers carried by a gas current
US4526733A (en) 1982-11-17 1985-07-02 Kimberly-Clark Corporation Meltblown die and method
US4708619A (en) 1985-02-27 1987-11-24 Reifenhauser Gmbh & Co. Maschinenfabrik Apparatus for spinning monofilaments
DE8534594U1 (en) 1985-12-09 1986-02-06 Claassen, Henning J., 2120 Lüneburg Spray head for spraying a thermoplastic material, in particular a hot melt adhesive
US4687137B1 (en) 1986-03-20 1988-10-25
US4687137A (en) 1986-03-20 1987-08-18 Nordson Corporation Continuous/intermittent adhesive dispensing apparatus
US5156715A (en) * 1987-02-09 1992-10-20 Southwire Company Apparatus for applying two layers of plastic to a conductor
US4785996A (en) 1987-04-23 1988-11-22 Nordson Corporation Adhesive spray gun and nozzle attachment
US4891249A (en) 1987-05-26 1990-01-02 Acumeter Laboratories, Inc. Method of and apparatus for somewhat-to-highly viscous fluid spraying for fiber or filament generation, controlled droplet generation, and combinations of fiber and droplet generation, intermittent and continuous, and for air-controlling spray deposition
US4815660A (en) 1987-06-16 1989-03-28 Nordson Corporation Method and apparatus for spraying hot melt adhesive elongated fibers in spiral patterns by two or more side-by-side spray devices
US4983109A (en) 1988-01-14 1991-01-08 Nordson Corporation Spray head attachment for metering gear head
US5145689A (en) 1990-10-17 1992-09-08 Exxon Chemical Patents Inc. Meltblowing die
EP0701010A1 (en) * 1990-10-17 1996-03-13 Exxon Chemical Patents Inc. Meltblowing Die
US5269670A (en) 1990-10-17 1993-12-14 Exxon Chemical Patents Inc. Meltblowing die
US5453129A (en) * 1991-05-08 1995-09-26 Exxon Chemical Patents Inc. Oil spill recovery method
US5236641A (en) 1991-09-11 1993-08-17 Exxon Chemical Patents Inc. Metering meltblowing system
US5445674A (en) 1992-03-06 1995-08-29 The Pillsbury Company Device for dispensing thixotropic sauce onto pizza crusts
US5382312A (en) 1992-04-08 1995-01-17 Nordson Corporation Dual format adhesive apparatus for intermittently disrupting parallel, straight lines of adhesive to form a band
US5294258A (en) * 1992-04-08 1994-03-15 Nordson Corporation Apparatus for producing an integral adhesive matrix
US5165940A (en) * 1992-04-23 1992-11-24 E. I. Du Pont De Nemours And Company Spinneret
US5336320A (en) 1992-06-30 1994-08-09 Nordson Corporation Fast response film coater
WO1994001221A1 (en) 1992-07-08 1994-01-20 Nordson Corporation Segmented slot die for air spray of fibers
US5368233A (en) 1993-09-01 1994-11-29 Nordson Corporation Spray disk for close centerline spacing
US5478224A (en) 1994-02-04 1995-12-26 Illinois Tool Works Inc. Apparatus for depositing a material on a substrate and an applicator head therefor
US5679379A (en) 1995-01-09 1997-10-21 Fabbricante; Anthony S. Disposable extrusion apparatus with pressure balancing modular die units for the production of nonwoven webs
US5618566A (en) 1995-04-26 1997-04-08 Exxon Chemical Patents, Inc. Modular meltblowing die
US5683578A (en) 1995-05-15 1997-11-04 Illinois Tool Works Inc. Filter valve system for regulating, filtering, and dispensing a flow of hot melt materials and adhesives
US5645743A (en) 1995-05-18 1997-07-08 Illinois Tool Works Inc. Multiple heat source grid assembly
US5728407A (en) * 1995-05-26 1998-03-17 Japan Vilene Company, Ltd. Die for melt-blowing apparatus
US5728219A (en) 1995-09-22 1998-03-17 J&M Laboratories, Inc. Modular die for applying adhesives
US6253957B1 (en) 1995-11-16 2001-07-03 Nordson Corporation Method and apparatus for dispensing small amounts of liquid material
US5747102A (en) 1995-11-16 1998-05-05 Nordson Corporation Method and apparatus for dispensing small amounts of liquid material
US5605720A (en) 1996-04-04 1997-02-25 J & M Laboratories Inc. Method of continuously formulating and applying a hot melt adhesive
US5806720A (en) 1996-07-19 1998-09-15 Illinois Tool Works Inc. Multi position palletizer head for adhesive supply unit
US6423227B1 (en) 1997-02-07 2002-07-23 Nordson Corporation Meltblown yarn and method and apparatus for manufacturing
US6422848B1 (en) 1997-03-19 2002-07-23 Nordson Corporation Modular meltblowing die
US5875922A (en) * 1997-10-10 1999-03-02 Nordson Corporation Apparatus for dispensing an adhesive
US6210141B1 (en) * 1998-02-10 2001-04-03 Nordson Corporation Modular die with quick change die tip or nozzle
US6427745B1 (en) 1998-03-03 2002-08-06 Nordson Corporation Apparatus for the manufacture of nonwoven webs and laminates
US6296463B1 (en) 1998-04-20 2001-10-02 Nordson Corporation Segmented metering die for hot melt adhesives or other polymer melts
US6422428B1 (en) 1998-04-20 2002-07-23 Nordson Corporation Segmented applicator for hot melt adhesives or other thermoplastic materials
US6502615B1 (en) 1999-12-22 2003-01-07 Nordson Corporation Apparatus for making an absorbent composite product
US6260583B1 (en) 2000-05-24 2001-07-17 Illinois Tool Works Inc. Segmented stackable head design
US6491507B1 (en) 2000-10-31 2002-12-10 Nordson Corporation Apparatus for meltblowing multi-component liquid filaments
US6478563B1 (en) 2000-10-31 2002-11-12 Nordson Corporation Apparatus for extruding multi-component liquid filaments
US6499982B2 (en) 2000-12-28 2002-12-31 Nordson Corporation Air management system for the manufacture of nonwoven webs and laminates
US6499631B2 (en) * 2001-01-26 2002-12-31 Illinois Tool Works Inc. Hot melt adhesive applicator

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
European Patent Office, Partial European Search Report, Application No. EP 03 07 9172.
Nordson Corporation, The CF800M Metered Head, Trends, 1993, 2 pgs.
Trends (1993) The CF 800 Metered Head. *

Cited By (52)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8196778B2 (en) 2002-01-28 2012-06-12 Nordson Corporation Process air-assisted dispensing systems
US8453880B2 (en) 2002-01-28 2013-06-04 Nordson Corporation Process air-assisted dispensing systems and methods
US8286833B2 (en) 2002-01-28 2012-10-16 Nordson Corporation Dispensing systems for dispensing a heated liquid
US20100018996A1 (en) * 2002-01-28 2010-01-28 Nordson Corporation Process air-assisted dispensing systems
US20110006082A1 (en) * 2002-01-28 2011-01-13 Nordson Corporation Dispensing systems for dispensing a heated liquid
US20090065611A1 (en) * 2006-01-06 2009-03-12 Nordson Corporation Liquid dispenser having individualized process air control
US9914147B2 (en) 2006-01-06 2018-03-13 Nordson Corporation Liquid dispenser having individualized process air control
US8586338B2 (en) 2008-05-30 2013-11-19 3M Innovative Properties Company Ligand functionalized substrates
US9650470B2 (en) 2008-05-30 2017-05-16 3M Innovative Properties Company Method of making ligand functionalized substrates
US8846203B2 (en) 2008-05-30 2014-09-30 3M Innovative Properties Company Method of making ligand functionalized substrates
US10017461B2 (en) 2008-05-30 2018-07-10 3M Innovative Properties Company Method of making ligand functionalized substrates
US8652582B2 (en) 2008-05-30 2014-02-18 3M Innovative Properties Company Method of making ligand functionalized substrates
US20100155323A1 (en) * 2008-12-23 2010-06-24 Weiss Douglas E Functionalized nonwoven article
US8328023B2 (en) 2008-12-23 2012-12-11 3M Innovative Properties Company Functionalized nonwoven article
US9259689B2 (en) 2009-06-23 2016-02-16 3M Innovative Properties Company Functionalized nonwoven article
US8329034B2 (en) 2009-06-23 2012-12-11 3M Innovative Properties Company Functionalized nonwoven article
WO2010151447A1 (en) 2009-06-23 2010-12-29 3M Innovative Properties Company Functionalized nonwoven article
US9126222B2 (en) 2009-07-17 2015-09-08 Illinois Tool Works Inc. Metering system for hot melt adhesives with variable adhesive volumes
US9573159B2 (en) 2009-08-31 2017-02-21 Illinois Tool Works, Inc. Metering system for simultaneously dispensing two different adhesives from a single metering device or applicator onto a common substrate
US9718081B2 (en) * 2009-08-31 2017-08-01 Illinois Tool Works Inc. Metering system for simultaneously dispensing two different adhesives from a single metering device or applicator onto a common substrate
US20110052812A1 (en) * 2009-08-31 2011-03-03 Illinois Tool Works Inc. Metering system for simultaneously dispensing two different adhesives from a single metering device or applicator onto a common substrate
US20110052811A1 (en) * 2009-08-31 2011-03-03 Illinois Tool Works Inc. Metering system for simultaneously dispensing two different adhensives from a single metering device or applicator onto a common substrate
US8377672B2 (en) 2010-02-18 2013-02-19 3M Innovative Properties Company Ligand functionalized polymers
US9296847B2 (en) 2010-02-18 2016-03-29 3M Innovative Properties Company Ligand functionalized polymers
US8945896B2 (en) 2010-02-18 2015-02-03 3M Innovative Properties Company Ligand functionalized polymers
US10526366B2 (en) 2010-03-03 2020-01-07 3M Innovative Properties Company Ligand functionalized polymers
US9758547B2 (en) 2010-03-03 2017-09-12 3M Innovative Properties Company Ligand functionalized polymers
US8435776B2 (en) 2010-03-03 2013-05-07 3M Innovative Properties Company Ligand functionalized polymers
WO2012012172A2 (en) 2010-06-30 2012-01-26 3M Innovative Properties Company Filter plate article having a water-absorbent filter assembly
US8906645B2 (en) 2010-12-29 2014-12-09 3M Innovative Properties Company Microbial detection article having a water-absorbent filter assembly
US9156053B2 (en) 2011-10-27 2015-10-13 Graco Minnesota Inc. Melter
US9174231B2 (en) 2011-10-27 2015-11-03 Graco Minnesota Inc. Sprayer fluid supply with collapsible liner
US10160071B2 (en) 2011-11-30 2018-12-25 Palo Alto Research Center Incorporated Co-extruded microchannel heat pipes
US9120190B2 (en) 2011-11-30 2015-09-01 Palo Alto Research Center Incorporated Co-extruded microchannel heat pipes
US10371468B2 (en) 2011-11-30 2019-08-06 Palo Alto Research Center Incorporated Co-extruded microchannel heat pipes
US20130206062A1 (en) * 2012-02-10 2013-08-15 Palo Alto Research Center Incoproated Micro-Extrusion Printhead With Offset Orifices For Generating Gridlines On Non-Square Substrates
US8875653B2 (en) * 2012-02-10 2014-11-04 Palo Alto Research Center Incorporated Micro-extrusion printhead with offset orifices for generating gridlines on non-square substrates
WO2013162695A1 (en) 2012-04-24 2013-10-31 3M Innovative Properties Company Nonwoven article gafter with copolymer
US9821276B2 (en) 2012-04-24 2017-11-21 3M Innovative Properties Company Nonwoven article grafted with copolymer
US8939330B2 (en) 2013-03-13 2015-01-27 Graco Minnesota Inc. Removable module service seat
US10526729B2 (en) 2014-02-24 2020-01-07 Nanofiber, Inc. Melt blowing die, apparatus and method
US10315787B2 (en) 2015-03-12 2019-06-11 Graco Minnesota Inc. Manual check valve for priming a collapsible fluid liner for a sprayer
US9796492B2 (en) 2015-03-12 2017-10-24 Graco Minnesota Inc. Manual check valve for priming a collapsible fluid liner for a sprayer
US10988827B2 (en) 2015-03-16 2021-04-27 3M Innovative Properties Company Coalescing elements in copper production
US11110483B2 (en) * 2017-10-31 2021-09-07 Nordson Corporation Liquid material dispensing system having a sleeve heater
US20210387225A1 (en) * 2018-11-09 2021-12-16 Illinois Tool Works Inc. Modular fluid application device for varying fluid coat weight
US11684947B2 (en) * 2018-11-09 2023-06-27 Illinois Tool Works Inc. Modular fluid application device for varying fluid coat weight
US11707753B2 (en) 2019-05-31 2023-07-25 Graco Minnesota Inc. Handheld fluid sprayer
US11752517B2 (en) 2020-09-29 2023-09-12 C3 Corporation Hotmelt application system and process
WO2022136968A1 (en) 2020-12-23 2022-06-30 3M Innovative Properties Company Method of separating a virus from a composition using copolymer-grafted nonwoven substrates
WO2023031696A1 (en) 2021-09-01 2023-03-09 3M Innovative Properties Company Nonwoven with bio particles and methods of making the same
WO2023037178A1 (en) 2021-09-08 2023-03-16 3M Innovative Properties Company Method of harvesting biologics

Also Published As

Publication number Publication date
EP1062051A1 (en) 2000-12-27
JP2002505951A (en) 2002-02-26
US6220843B1 (en) 2001-04-24
JP4611521B2 (en) 2011-01-12
DE69917234T2 (en) 2005-06-23
CN1292733A (en) 2001-04-25
CN1102079C (en) 2003-02-26
WO1999046057A1 (en) 1999-09-16
EP1062051B1 (en) 2004-05-12
AU3001699A (en) 1999-09-27
DE69917234D1 (en) 2004-06-17

Similar Documents

Publication Publication Date Title
USRE39399E1 (en) Segmented die for applying hot melt adhesives or other polymer melts
US6296463B1 (en) Segmented metering die for hot melt adhesives or other polymer melts
US5728219A (en) Modular die for applying adhesives
US6422848B1 (en) Modular meltblowing die
EP0553237B1 (en) Melt-blowing die
US6210141B1 (en) Modular die with quick change die tip or nozzle
EP0835952B1 (en) Meltblowing method and apparatus
US5618566A (en) Modular meltblowing die
AU704281B2 (en) Improved meltblowing method and system
EP1083999A1 (en) Method and apparatus for applying a controlled pattern of fibrous material to a moving substrate
US6680021B1 (en) Meltblowing method and system
EP0866152B1 (en) Meltblowing apparatus and process
US20050092775A1 (en) Liquid material dispensing apparatus and method utilizing pulsed pressurized air
EP1407830A2 (en) Segmented die for applying hot melt adhesives or other polymer melts
EP0987352A2 (en) Modular meltblowing die

Legal Events

Date Code Title Description
FEPP Fee payment procedure

Free format text: PAYOR NUMBER ASSIGNED (ORIGINAL EVENT CODE: ASPN); ENTITY STATUS OF PATENT OWNER: LARGE ENTITY

CC Certificate of correction
FEPP Fee payment procedure

Free format text: PAYOR NUMBER ASSIGNED (ORIGINAL EVENT CODE: ASPN); ENTITY STATUS OF PATENT OWNER: LARGE ENTITY

Free format text: PAYER NUMBER DE-ASSIGNED (ORIGINAL EVENT CODE: RMPN); ENTITY STATUS OF PATENT OWNER: LARGE ENTITY

FPAY Fee payment

Year of fee payment: 8

FPAY Fee payment

Year of fee payment: 12