US4288206A - Automatic multiple water sampler - Google Patents

Automatic multiple water sampler Download PDF

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Publication number
US4288206A
US4288206A US06/066,518 US6651879A US4288206A US 4288206 A US4288206 A US 4288206A US 6651879 A US6651879 A US 6651879A US 4288206 A US4288206 A US 4288206A
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United States
Prior art keywords
spool
syringes
frame
sampler
chambers
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Expired - Lifetime
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US06/066,518
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David C. Tigwell
David J. Schaeffer
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F04POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
    • F04BPOSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
    • F04B7/00Piston machines or pumps characterised by having positively-driven valving
    • F04B7/0003Piston machines or pumps characterised by having positively-driven valving the distribution member forming both the inlet and discharge distributor for one single pumping chamber
    • F04B7/0015Piston machines or pumps characterised by having positively-driven valving the distribution member forming both the inlet and discharge distributor for one single pumping chamber and having a slidable movement
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14Suction devices, e.g. pumps; Ejector devices
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/18Devices for withdrawing samples in the liquid or fluent state with provision for splitting samples into portions
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14Suction devices, e.g. pumps; Ejector devices
    • G01N2001/1418Depression, aspiration
    • G01N2001/1427Positive displacement, piston, peristaltic

Definitions

  • This invention relates generally to sampling pumps and more particularly concerns an automatic water sampler providing multiple samples from a source.
  • a related object of the invention is to provide such a sampler that is capable of simultaneously delivering multiple water samples so that different testing strategies can be simultaneously followed.
  • a further object is to provide a sampler of the above character which functions well even when handling relatively dirty water since the critical parts are virtually self-cleaning.
  • a sampler 10 embodying the invention having a valve assembly 11 and syringe assembly 12 mounted in a housing or frame 13.
  • the assembly 12 includes a plurality of syringes 15, three in the illustrated sampler 10, which are of standard commercial type having glass chambers 16 with opening necks 17, and plungers 18 with pistons 19 slidably fitted in the chambers 16.
  • the pistons 19 are preferably formed of non-wetting plastic like polytetrafluoroethylene, i.e., "Teflon".
  • the syringes 15 are held by blocks 21 secured to a cross bar 22 on the frame 13, and the plungers 18 are releasably secured to a drive bar 23 mounted in the frame 13 for tightly confined linear reciprocation.
  • the drive bar 23 has bushings 24 which are slidably fitted on rods 25 fixed in parallel relationship on the frame 13 so that the bar 23 is confined for reciprocation in a path parallel to the axes of the syringes 15.
  • the valve assembly 11 includes a housing 27 containing a glass tube 28 defining a valve chamber 29 in which a valve spool 30 is shiftably mounted.
  • the valve chamber 29 is opened to each of the syringes through the necks 17, and O-rings 31 provide seals between the syringes and the valve assembly 11.
  • the valve assembly 11 and glass tube 28 also have inlet openings 32 and outlet openings 33 for each of the syringes 15, and the inlet openings 32 are connected by a common line 34 to the source of the water being sampled.
  • the outlet openings 33 are connected by lines 35 to independent devices such as a holding vessel to store samples for later analysis or sorption columns designed to isolate one or more specific possible impurities.
  • the spool 30 is formed of non-wetting plastic as are the syringe pistons 19, and the spool 30 is also formed with relieved regions 37 for alternately connecting the syringe chambers 16 with the inlet and outlet openings 32, 33, respectively.
  • the inlet openings 32 are connected to the syringes 15.
  • the spool relieved regions 37 couple the outlet openings 33 to the syringes 15.
  • the glass tube 28 and the spool 30 are cylindrical, and the spool portions defining the outer edges of the relieved portions 37 are slightly flared in diameter to define lips having firm wiping contact with the glass tube 28.
  • valve spool 30 is shifted by a solenoid 40 coupled to a rod-like extension 41 of the spool.
  • the solenoid 40 acts like a locking relay, which, when energized, shifts the spool 30 to the right in the drawing against the bias of a spring 42, whereupon the solenoid is latched.
  • the latch not shown, is released the spring 42 shifts the spool 30 to the left and into the position illustrated.
  • a crank 45 is journaled on a support 46 mounted on the frame 13.
  • the crank 45 is connected by a crank arm 47 to the bar 23 and is also provided with a lobe 48 that actuates a pair of microswitches 49 and 50 mounted on the support 46.
  • the crank arm 47 is adjustable in length, being formed like a turnbuckle, and the lower end can be mounted in alternate mounting holes 52 in the crank 45 for adjusting the throw of the crank and thus the distance the plungers 18 move in the syringe chambers 16 during each stroke.
  • the lobe 48 has just tripped the switch 49 so as to release the solenoid 40 and allow the spring 42 to shift the spool 30 to the left.
  • the pistons 19 will be drawn downwardly, pulling a precise, discrete sample volume into each of the syringes 15.
  • the switch 50 will be actuated to energize the solenoid 40 and shift the spool to the right. Further rotation of the crank 45 will lift the plungers 18 to drive the sample volumes in each of the syringes 15 through the outlet openings 33.
  • the sampler 10 is well suited for forcing the samples into and through a sorption column.
  • the inlet line 34 can be connected to a supply of suitable solvent and the sampler cycled to drive the desired volume of solvent through the column that has been isolating and collecting the impurity being tested for.
  • the crank 45 can be driven in any desired fashion, as for example, by a timing motor internal to the sampler 10 or by an external water flow meter that would cycle the sampler at desired incremental flow volumes.
  • sampler 10 utilizing conventional syringes, can be economically manufactured and serviced, while providing quite precise sample volumes.
  • the sliding of the pistons 19 in the glass chambers 16 and of the spool 30 in the glass tube 28 makes these parts virtually self-cleaning so that the sampler 10 is well suited for reliable use in relatively dirty water.

Abstract

A water sampler for delivering simultaneous multiple samples in which the samples are taken and discharged by a plurality of glass chambered syringes driven by a crank with water flow being controlled by a glass chambered valve having a valve spool shifted under the control of the crank.

Description

This invention relates generally to sampling pumps and more particularly concerns an automatic water sampler providing multiple samples from a source.
The great present day concern for the quality of naturally flowing water has produced a need for devices to monitor water quality, often in remote locations and for extended periods. Various testing strategies are available, ranging from simple storage of samples for later analysis to directing samples through sorption columns designed to isolate even trace amounts of organic impurities such as pesticides, vinyl chloride, benzenes and other possible industrial wastes.
It is the primary aim of the present invention to provide a water sampler suitable for taking and delivering discrete water samples, under pressure, for testing. Because the samples are delivered under pressure, the sampler is well suited for use with sorption columns. A related object of the invention is to provide such a sampler that is capable of simultaneously delivering multiple water samples so that different testing strategies can be simultaneously followed.
It is also an object of the invention to provide a sampler of the above kind which can be readily adjusted for both sample size and for the rate at which samples are taken. Another object is to provide a sampler as characterized above which has only inert materials in contact with the water being sampled, but which utilizes standard components for economy and convenience in servicing.
A further object is to provide a sampler of the above character which functions well even when handling relatively dirty water since the critical parts are virtually self-cleaning.
Other objects and advantages of the invention will become apparent upon considering the following detailed description and upon reference to the drawing, which is:
An elevation, partially sectioned and partially schematic, of an apparatus embodying the present invention.
While the invention will be described in connection with a preferred embodiment, it will be understood that we do not intend to limit the invention to that embodiment. On the contrary, we intend to cover all alternatives, modifications and equivalents as may be included within the spirit and scope of the invention as defined by the appended claims.
Turning to the drawing, there is shown a sampler 10 embodying the invention and having a valve assembly 11 and syringe assembly 12 mounted in a housing or frame 13. The assembly 12 includes a plurality of syringes 15, three in the illustrated sampler 10, which are of standard commercial type having glass chambers 16 with opening necks 17, and plungers 18 with pistons 19 slidably fitted in the chambers 16. The pistons 19 are preferably formed of non-wetting plastic like polytetrafluoroethylene, i.e., "Teflon".
In carrying out the invention, the syringes 15 are held by blocks 21 secured to a cross bar 22 on the frame 13, and the plungers 18 are releasably secured to a drive bar 23 mounted in the frame 13 for tightly confined linear reciprocation. In the illustrated embodiment, the drive bar 23 has bushings 24 which are slidably fitted on rods 25 fixed in parallel relationship on the frame 13 so that the bar 23 is confined for reciprocation in a path parallel to the axes of the syringes 15.
In keeping with the invention, the valve assembly 11 includes a housing 27 containing a glass tube 28 defining a valve chamber 29 in which a valve spool 30 is shiftably mounted. The valve chamber 29 is opened to each of the syringes through the necks 17, and O-rings 31 provide seals between the syringes and the valve assembly 11. The valve assembly 11 and glass tube 28 also have inlet openings 32 and outlet openings 33 for each of the syringes 15, and the inlet openings 32 are connected by a common line 34 to the source of the water being sampled. The outlet openings 33 are connected by lines 35 to independent devices such as a holding vessel to store samples for later analysis or sorption columns designed to isolate one or more specific possible impurities.
Preferably, the spool 30 is formed of non-wetting plastic as are the syringe pistons 19, and the spool 30 is also formed with relieved regions 37 for alternately connecting the syringe chambers 16 with the inlet and outlet openings 32, 33, respectively. In the position illustrated, the inlet openings 32 are connected to the syringes 15. Upon shifting movement of the spool 30 to the right in the drawing, the spool relieved regions 37 couple the outlet openings 33 to the syringes 15. In the preferred embodiment, the glass tube 28 and the spool 30 are cylindrical, and the spool portions defining the outer edges of the relieved portions 37 are slightly flared in diameter to define lips having firm wiping contact with the glass tube 28.
In the illustrated embodiment, the valve spool 30 is shifted by a solenoid 40 coupled to a rod-like extension 41 of the spool. The solenoid 40 acts like a locking relay, which, when energized, shifts the spool 30 to the right in the drawing against the bias of a spring 42, whereupon the solenoid is latched. When the latch, not shown, is released the spring 42 shifts the spool 30 to the left and into the position illustrated.
For driving the bar 23 and timing the operation of the solenoid 40, a crank 45 is journaled on a support 46 mounted on the frame 13. The crank 45 is connected by a crank arm 47 to the bar 23 and is also provided with a lobe 48 that actuates a pair of microswitches 49 and 50 mounted on the support 46. The crank arm 47 is adjustable in length, being formed like a turnbuckle, and the lower end can be mounted in alternate mounting holes 52 in the crank 45 for adjusting the throw of the crank and thus the distance the plungers 18 move in the syringe chambers 16 during each stroke. In the position illustrated, the lobe 48 has just tripped the switch 49 so as to release the solenoid 40 and allow the spring 42 to shift the spool 30 to the left. As the crank 45 continues to rotate clockwise, the pistons 19 will be drawn downwardly, pulling a precise, discrete sample volume into each of the syringes 15. At the bottom of the crank stroke, the switch 50 will be actuated to energize the solenoid 40 and shift the spool to the right. Further rotation of the crank 45 will lift the plungers 18 to drive the sample volumes in each of the syringes 15 through the outlet openings 33.
Use of the latching solenoid 40 to control the valve assembly 11 assures rapid changes in valve position and thus accurate control of the sample volumes being taken.
Because the samples are discharged under pressure, the sampler 10 is well suited for forcing the samples into and through a sorption column. If desired, at the end of a run, the inlet line 34 can be connected to a supply of suitable solvent and the sampler cycled to drive the desired volume of solvent through the column that has been isolating and collecting the impurity being tested for.
The crank 45 can be driven in any desired fashion, as for example, by a timing motor internal to the sampler 10 or by an external water flow meter that would cycle the sampler at desired incremental flow volumes.
It can be seen that the water being sampled contacts only inert glass and plastic, and the glass of the syringes and the glass tube 28 of the valve assembly 11 constitute mechanically stable parts coacting with the plastic parts which have a tendency to flow. This avoids the possibility of leakage from plastic deformation that exists if plastic is sealed against plastic as movable valve elements.
Those skilled in the art will readily see that the sampler 10, utilizing conventional syringes, can be economically manufactured and serviced, while providing quite precise sample volumes. The sliding of the pistons 19 in the glass chambers 16 and of the spool 30 in the glass tube 28 makes these parts virtually self-cleaning so that the sampler 10 is well suited for reliable use in relatively dirty water.

Claims (1)

We claim as our invention:
1. A sampler for delivering multiple independent water samples comprising, in combination, a frame, a drive bar mounted in said frame for linear reciprocation, a plurality of glass chambered syringes having movable plungers mounted in said frame with their axes parallel to the direction of said bar reciprocation, said plungers being coupled to said drive bar, a valve body on said frame having a chamber opening to the chambers of said syringes, said body having an inlet and an outlet opening for each of said syringes, a valve spool shiftably mounted in said valve body chamber and having relieved regions for alternately connecting said syringe chambers with said inlet and then said outlet openings upon shifting of said spool, and means for reciprocating said drive bar and shifting said spool so that said syringe will draw liquid from said inlet openings and then positively discharge that liquid through said outlet openings, said plungers having non-wetting plastic pistons in wiping contact with said glass chambers, said valve body chamber being defined by a glass tube, and said valve spool being formed of non-wetting plastic.
US06/066,518 1979-08-15 1979-08-15 Automatic multiple water sampler Expired - Lifetime US4288206A (en)

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4569236A (en) * 1982-06-08 1986-02-11 Michael John Ahern Biological fluid sampler
US4576054A (en) * 1983-07-12 1986-03-18 Lalin Hill S Dual mode gas sampler and pneumatic flow control system
US4854838A (en) * 1986-07-14 1989-08-08 Swain David O Hydraulic pump gate apparatus
US5403554A (en) * 1993-04-22 1995-04-04 Freeman; Michael J. Apparatus for depositing fluids on a chromatography plate
US20050106051A1 (en) * 2003-10-06 2005-05-19 Micro Mechatronic Technologies Ag Metering pump
US20080225295A1 (en) * 2007-03-12 2008-09-18 Resolved Technologies, Inc. Device for multiple tests from a single sample
US8051727B1 (en) 2008-04-22 2011-11-08 The United States Of America As Represented By The Secretary Of The Interior Pore-water profiler
DE102016005055B3 (en) * 2016-04-26 2016-09-15 Alfred-Wegener-Institut Helmholtz-Zentrum für Polar- und Meeresforschung Automated multi-sample processor with multiple piston pumps
US20170248129A1 (en) * 2014-10-13 2017-08-31 Alfa S.R.L. Positive-displacement pump and pumping group for fluid products and method for the use thereof
CN110844096A (en) * 2019-12-16 2020-02-28 杜志刚 Water sampling environmental protection unmanned aerial vehicle
CN113202719A (en) * 2021-04-07 2021-08-03 宁波新芝生物科技股份有限公司 Combined multi-channel full-automatic injection pump
USD949289S1 (en) * 2020-06-02 2022-04-19 Luxembourg Institute Of Science And Technology Housing of an automatic water sampler apparatus

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2515956A (en) * 1949-01-21 1950-07-18 Charles J Greenberg Syringe
US2541086A (en) * 1947-06-23 1951-02-13 Norton Co Pump and control
US2696174A (en) * 1951-02-16 1954-12-07 Frank J Cozzoli Filling machine for pharmaceutical liquids
US3098480A (en) * 1960-11-29 1963-07-23 William D Worthington System for fluid transfusion
US3259077A (en) * 1964-10-26 1966-07-05 Dow Chemical Co Multi-syringe-type pump
FR2005374A1 (en) * 1968-04-02 1969-12-12 Battelle Development Corp
US3572130A (en) * 1969-08-27 1971-03-23 Nat Instr Lab Inc Liquid sample pick-up and dispensing apparatus
US4006847A (en) * 1975-10-23 1977-02-08 Dooley Dynamics, Inc. Dispensing apparatus
US4141469A (en) * 1977-05-02 1979-02-27 Lee Thomas E Microdispensing dilution system

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2541086A (en) * 1947-06-23 1951-02-13 Norton Co Pump and control
US2515956A (en) * 1949-01-21 1950-07-18 Charles J Greenberg Syringe
US2696174A (en) * 1951-02-16 1954-12-07 Frank J Cozzoli Filling machine for pharmaceutical liquids
US3098480A (en) * 1960-11-29 1963-07-23 William D Worthington System for fluid transfusion
US3259077A (en) * 1964-10-26 1966-07-05 Dow Chemical Co Multi-syringe-type pump
FR2005374A1 (en) * 1968-04-02 1969-12-12 Battelle Development Corp
US3572130A (en) * 1969-08-27 1971-03-23 Nat Instr Lab Inc Liquid sample pick-up and dispensing apparatus
US4006847A (en) * 1975-10-23 1977-02-08 Dooley Dynamics, Inc. Dispensing apparatus
US4141469A (en) * 1977-05-02 1979-02-27 Lee Thomas E Microdispensing dilution system

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4569236A (en) * 1982-06-08 1986-02-11 Michael John Ahern Biological fluid sampler
US4576054A (en) * 1983-07-12 1986-03-18 Lalin Hill S Dual mode gas sampler and pneumatic flow control system
US4854838A (en) * 1986-07-14 1989-08-08 Swain David O Hydraulic pump gate apparatus
US5403554A (en) * 1993-04-22 1995-04-04 Freeman; Michael J. Apparatus for depositing fluids on a chromatography plate
US20050106051A1 (en) * 2003-10-06 2005-05-19 Micro Mechatronic Technologies Ag Metering pump
US20080225295A1 (en) * 2007-03-12 2008-09-18 Resolved Technologies, Inc. Device for multiple tests from a single sample
US9164111B2 (en) 2007-03-12 2015-10-20 Resolved Technologies, Inc. Device for multiple tests from a single sample
US8051727B1 (en) 2008-04-22 2011-11-08 The United States Of America As Represented By The Secretary Of The Interior Pore-water profiler
US11053930B2 (en) * 2014-10-13 2021-07-06 Alfa S. R. L. Positive-displacement pump and pumping group for fluid products and method for the use thereof
US20170248129A1 (en) * 2014-10-13 2017-08-31 Alfa S.R.L. Positive-displacement pump and pumping group for fluid products and method for the use thereof
DE102016005055B3 (en) * 2016-04-26 2016-09-15 Alfred-Wegener-Institut Helmholtz-Zentrum für Polar- und Meeresforschung Automated multi-sample processor with multiple piston pumps
US10393630B2 (en) 2016-04-26 2019-08-27 Alfred-Wegener-Institut Helmholtz-Zentrum Fuer Polar-Und Meeresforschung Automated multiple sample processor having a plurality of piston pumps
WO2017186214A1 (en) 2016-04-26 2017-11-02 Alfred-Wegener-Institut, Helmholtz-Zentrum für Polar- und Meeresforschung Automated multiple sample processor having a plurality of piston pumps
CN110844096A (en) * 2019-12-16 2020-02-28 杜志刚 Water sampling environmental protection unmanned aerial vehicle
USD949289S1 (en) * 2020-06-02 2022-04-19 Luxembourg Institute Of Science And Technology Housing of an automatic water sampler apparatus
CN113202719A (en) * 2021-04-07 2021-08-03 宁波新芝生物科技股份有限公司 Combined multi-channel full-automatic injection pump

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