US3313138A - Method of forging titanium alloy billets - Google Patents

Method of forging titanium alloy billets Download PDF

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Publication number
US3313138A
US3313138A US355048A US35504864A US3313138A US 3313138 A US3313138 A US 3313138A US 355048 A US355048 A US 355048A US 35504864 A US35504864 A US 35504864A US 3313138 A US3313138 A US 3313138A
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alloy
workpiece
forging
die
temperature
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US355048A
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Donald G Spring
Jack J Niebel
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Crucible Materials Corp
Cooper Industries LLC
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Crucible Steel Company of America
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Assigned to COLT INDUSTRIES OPERATING CORP. reassignment COLT INDUSTRIES OPERATING CORP. MERGER AND CHANGE OF NAME Assignors: CRUCIBLE CENTER COMPANY (INTO) CRUCIBLE INC. (CHANGED TO)
Assigned to COOPER INDUSTRIES, INC., A CORP. OF OHIO reassignment COOPER INDUSTRIES, INC., A CORP. OF OHIO ASSIGNMENT OF ASSIGNORS INTEREST. Assignors: BELDEN CORPORATION
Assigned to CRUCIBLE MATERIALS CORPORATION reassignment CRUCIBLE MATERIALS CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST. Assignors: COLT INDUSTRIES OPERATING CORP.
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/16Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
    • C22F1/18High-melting or refractory metals or alloys based thereon
    • C22F1/183High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S72/00Metal deforming
    • Y10S72/70Deforming specified alloys or uncommon metal or bimetallic work

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Forging (AREA)

Description

United States Patent This invention relates to a method of forging billets of alpha-beta titanium-base alloys. It has hitherto been the commercial practice to forge billets of such alloys by using flat forging dies and heating the billets to above the beta transus temperature of the alloy before forging. When such alloys are to be used to make complex close die forgings which, because of their size, receive little work or are subject to surface cracking during some part of the forging operation, it has been observed that the billet tends to develop a coarse grain size in its surface layers, with the result that extensive, time-consuming conditioning is required before the forging can be used or further forged. Moreover, at times the tensile ductility of the forging is less than optimal. We have discovered that these difiiculties can in large measure be overcome or avoided by using a V-die, rather than a flat die, and conducting the forging operation at a temperature below the beta transus temperature of the alpha-beta alloy being worked. We have also discovered that, for optimal reduction in cross-sectional area of the billet in drawing it to final size after the forging operation, it is preferable, although not absolutely essential, that the billets to be forged be upset.
A complete understanding of our invention may be had from the following detailed description thereof, illustrating with specific examples the best mode presently contemplated by us for its practice.
Example 1.-An ingot of alpha-beta titanium alloy (6% aluminum, 4% vanadium, ba-lance titanium) 32 inches in diameter and about 80 inches long was heated to about 2050 F. It was then placed on end in a forging press and upset to reduce its height by about 35% of its original length. The upset ingot was reheated to about 2050 F., and then drawn, in accordance with conventional practices, to a square of about 26 inches by 26 inches. This piece was then conditioned by swing grinding, heated to 1750 F., and drawn down to a 24-inch octagon. The octagon was reheated to about 1750 F., and then press-forged to a 22-inch diameter round, using a V-die. The sides of the V-die were at about a 45 angle with the horizontal. During the V-die forging, the workpiece was reheated to 1750 F. only as necessary, soaking being avoided. The workpiece was then skinground, grit-blasted, tested, and prepared for shipment.
Example 2.-Example 1 was repeated, except that after being conditioned by using a swing grinder and being heated to 1750" F., the workpiece was drawn down to a 20-inch octagon, reheated to 1750 F., and then pressforged, using a V-die, to a final size of 18 inches diameter.
The product of both the above examples exhibited a finer grain size than. do pieces of similar size produced by the usual practice of fiat-die forging at temperatures above the beta transus. The advantage of producing forgings of fine grain size is Well known in the art. Fine grain size imparts superior toughness and ductility to the forgings. To achieve this result with the method of the present invention, it is critical that the workpiece be forged at a temperature below the beta transus temperature of the alloy of the workpiece by simultaneously applying forces directly radially inward toward the longitudinal axis of the workpiece by means of at least three separate and distinct contacting surfaces arranged longitudinally 3,313,138. Patented Apr. 11, 1967 along the workpiece and'spaced substantially evenly about the periphery thereof. More specifically, this is achieved by the use of a V-shaped die.
Our invention finds use with all alpha-beta titaniumbase alloys, including the 6Al-4V alloy mentioned above as well as the 4Al-4Mn and the 7Al-4Mo alloys. Certain alloys that are considered alpha alloys but contain a small amount of beta micro-structure, such as Ti-8Al-lMo-1V, may also be processed in accordance with our invention.
The exact temperature to be used in each of the heating steps indicated above will depend upon the composition, and more specifically upon the beta transus temperature, of the specific alloy being worked. Variations in and modifications of the practices disclosed in the above examples will be discussed with reference to the 6Al-4V alloy, which has a beta transus temperature of about 1850 F.
It is desirable that the upsetting operation be conducted at about 2000 to 2100". With lower temperatures, the workpiece tends to be hard to upset, and with higher temperatures, hydrogen contamination of the surface of the workpiece is likely to be encountered.
For optimal performance in reduction of the crosssectional area of the workpiece to final size, it is desirable to upset the ingot about 35% of its original length, although substantial benefits can be obtained with upsets as low as 20% and as high as 50%.
It is important that the V-die forging step be done at a temperature below the beta transus temperature, preferably about to F. below the beta transus temperature. It is also essential that a V-die having sides that make a substantial acute angle with the horizontal, such as about 30 to 60%, be used. Either a press forge or a hammer forge can be used.
Although the invention has been described above with reference to the use of a V-shaped forging die, it will be apparent to those skilled in the art that other means can be used whereby substantially the same action and result are obtained, e.g., positioning three or more contacting members, contacting faces or surfaces substantially evenly about the periphery of the workpiece and simultaneously applying by means of them radially inwardly directed forces to form, forge, or otherwise substantially work the workpiece at a temperature below the beta transus.
It is essential that a certain amount of work be done on the workpiece in the V-die forging step; i.e., it is essential that such step reduce the, cross-sectional area of the workpiece by at least 10% or more, up to 50%, preferably about 30%. Also, it is possible to conduct some,
or even most, of the V-die forging step at temperatures above the beta transus, so long as such forging is followed by forging below the beta transus temperature to the extent of at least 10% reduction in cross-sectional area as a final part of the V-die forging step.
Although our invention has been described with respect to certain specific practices, it will be readily apparent to those skilled in the art that various modifications therein may be made to suit specific requirements without departing from the spirit and scope of the invention.
We claim: I
1. In a method of forging an alpha-beta titanium-base alloy billet, the step which comp-rises forging an elongated workpiece of said alloy at a temperature below the beta transus temperature of said alloy to such an extent as to reduce the cross-sectional area of said workpiece by about 10 to 50% by simultaneously applying forces directed radially inward toward the longitudinal axis of said workpiece by means of at least three separate and distinct contacting surfaces arranged longitudinally along said workpiece and spaced substantially evenly about the periphery of said workpiece.
2. A method of producing a forged billet of an alphabeta titanium-base alloy comprising in combination the steps of upsetting an elongated ingot of said alloy at a. temperature above the beta transus temperature of said alloy by about 20 to 50% of its original length, and then forging said alloy, at a temperature below the beta transus temperature of said alloy, to such an extent as to reduce the cross-sectional area of said workpiece by about to 50%, by simultaneously apply forces directed radially inward toward the longitudinal axis of said ingot by means of at least three separate and distinct contacting surface arranged longitudnially along said ingot and spaced substantially evenly about the periphery of said ingot.
3. In a method of forging a billet of a titanium-base alloy selected from the group consisting of Ti-6Al-4V, Ti-4Al-4Mn, Ti-7Al-4Mo and Ti-8Al-1Mo-1V, the step which comprises forging an elongated workpiece of said alloy at a temperature below the beta transus temperature of said alloy to such an extent as to reduce the crosssectional area of said workpiece by about 10 to 50% by simultaneously applying forces directed radially inward toward the longitudinal axis of said workpiece by means of at least three separate and distinct contacting surfaces arranged longitudinally along said workpiece and spaced substantially evenly about the periphery of said workpiece.
4. A method of producing a forged billet of an alphabeta titanium-base alloy selected from the group consisting -of Ti-6A1-4V, Ti-4Al-4Mn, Ti-7Al-4Mo, Ti-8Al-1Mo-1V, comprising, in combination, the steps of upsetting an elongated ingot of said alloy at a temperature above the beta transus temperature of said alloy by about 20 to 50% of its original length, and then forging said alloy, at a temperature below the beta transus temperature of said alloy, to such an extent as to reduce the cross-sectional area of said ingot by about 10 to 50%, by simultaneously applying forces directed radially inward toward the longitudinal axis of said ingot by means of at least three separate and distinct contacting surfaces arranged longitudinally along said ingot and spaced substantially evenly about the periphery of said ingot.
5. In a method of forging an alpha-beta titanium-base alloy billet, the step which compirses forging an elongated workpiece of said alloy at a temperature below the beta transus temperature of said alloy, to such an extent as to reduce the cross-sectional area of said workpiece by about 10 to 50%, using a die V-shaped in longitudinal cross-section, the sides of' said die forming an angle of about 30 to 60 with the horizontal.
6. A method of producing a forged billet of a nalphabeta titanium-base alloy comprising, in combination, the steps of upsetting an elongated ingot of said alloy at a temperature-above the beta transus temperature of said alloy by about 20 to 50% of its original length, and then forging said alloy, at a temperature below the beta transus temperature of said alloy, to such an extent as to reduce the cross-sectional area of said ingot by about 10 to 50%, using a die V-shaped in longitudinal crosssection, the sides of said die forming an'angle of about 30 to 60 with the horizontal.
' 7. In a method of forging a billet'of a titanium-base alloy selected from the group consisting of Ti-6Al-4V, Ti-4Al-4Mn, Ti-7Al-4Mo, and Ti-8Al-1Mo-1V, the step and beta titanium-base alloy selected from the group consisting of Ti-6Al-4V, Ti-4Al-4Mn, Ti-7Al-4Mo, and Ti-8A-lMo-1V, comprising, in combination, the steps of upsetting an elongated ingot of said alloy at a temperature above the beta transus temperature of said alloy by about 20 to 50% of its original length, and then forging said alloy, at a temperature below the beta transus temperature of said alloy, to such an extent as to reduce' the cross-sectional area of said ingot by about 10 to 50%, using a die V-shaped in longitudinal crosssection, the sides of said die forming an angle of about 30 to 60 with the horizontal.
9. In a method of forging .a billet of a titanium base alloy consisting essentially of about 6% aluminum, 4% vanadium, balance titanium, the step which comprsies forging an elongated workpiece of said alloy at a temperature below the beta transus temperature of said alloy, to such. an extent as to reduce the cross-sectional area of said workpiece by about 10 to 50%, using a die V-shaped in longitudinal cross-section, the sides of said die forming an angle of about 30 to 60 with the horizontal.
10. A method of producing a forged billet of a titanium-base alloy consisting essentially of about 6% aluminum, 4% vanadium, balance titanium, said method comprising, in combination, the steps of upsetting an elongated ingot of said alloy at a temperature above the beta transus temperature of said alloy by about 20 to 50% of its original length, and then forging said alloy, at a temperature below the beta transus temperature of said alloy, to such an extent as to reduce the cross-sectional area of said ingot by about 10 to 50%, using a die V-shaped in longitudinal cross-section, the sides of said die forming an angle of about 30 to 60 with the horizontal.
11. A method of producing a forged billet of a titanium-base alloyconsisting essentially of about 6% aluminum, 4% vanadium, balance titanium, said method comprising, in combination, the steps of upsetting an elongated ingot of said alloy at about 2000 to 2100" F. by about 35% of its original length, and then forging said alloy at a temperature of about 1750 F., to such an extent as to reduce the cross-sectional area of said ingot by about 10 to 50%, using a die V-shaped in longitudinal cross-section, the sides of said die forming an angle of about 45 with the horizontal.
References Cited by the Examiner UNITED STATES PATENTS 144,832 11/1873 Coes 72-474 503,481 8/1893 Horn 72-374 2,950,191 8/1960 Vordahl 1481l.5 3,194,693 7/1965 Solitis 14811.5
CHARLES W. LANHAM, Primary Examiner. L. A. LARSON, Assistant Examiner.

Claims (1)

1. IN A METHOD OF FORGING AN ALPH-BETA TITANIUM-BASE ALLOY BILLET, THE STEP WHICH COMPRISES FORGING AN ELONGATED WORKPEICE OF SAID ALLOY AT A TEMPERATURE BELOW THE BETA TRANSUS TEMPERATURE OF SAID ALLOY TO SUCH AN EXTENT AS TO REDUCE THE CROSS-SECTIONAL AREA OF SAID WORKPIECE BY ABOUT 10 TO 50% BY SIMULATANEOUSLY APPLYING FORCES DIRECTED RADIALLY INWARD TOWARD THE LONGITUDINAL AXIS OF SAID WORKPIECE BY MEANS OF AT LEAST THREE SEPARATE AND DISTINCT CONTACTING SURFACES ARRANGED LONGITUDINALLY ALONG SAID WORKPIECE AND SPACED SUBSTANTIALLY EVENLY ABOUT THE PERIPHERY OF SAID WORKPIECE.
US355048A 1964-03-24 1964-03-24 Method of forging titanium alloy billets Expired - Lifetime US3313138A (en)

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Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3383233A (en) * 1965-12-22 1968-05-14 Park Ohio Industries Inc Method and apparatus for inductively heating a workpiece formed from a highly oxidizable metal
US3489617A (en) * 1967-04-11 1970-01-13 Titanium Metals Corp Method for refining the beta grain size of alpha and alpha-beta titanium base alloys
US3867208A (en) * 1970-11-24 1975-02-18 Nikolai Alexandrovich Grekov Method for producing annular forgings
US4055975A (en) * 1977-04-01 1977-11-01 Lockheed Aircraft Corporation Precision forging of titanium
US4145903A (en) * 1978-04-03 1979-03-27 Textron Inc. Sheet forming method and apparatus
US4991419A (en) * 1988-11-18 1991-02-12 Sumitomo Metal Industries, Ltd. Method of manufacturing seamless tube formed of titanium material
US5026520A (en) * 1989-10-23 1991-06-25 Cooper Industries, Inc. Fine grain titanium forgings and a method for their production
US5795413A (en) * 1996-12-24 1998-08-18 General Electric Company Dual-property alpha-beta titanium alloy forgings
US20050257864A1 (en) * 2004-05-21 2005-11-24 Brian Marquardt Metastable beta-titanium alloys and methods of processing the same by direct aging
US20070193662A1 (en) * 2005-09-13 2007-08-23 Ati Properties, Inc. Titanium alloys including increased oxygen content and exhibiting improved mechanical properties
US20070193018A1 (en) * 2006-02-23 2007-08-23 Ati Properties, Inc. Methods of beta processing titanium alloys
US20110180188A1 (en) * 2010-01-22 2011-07-28 Ati Properties, Inc. Production of high strength titanium
US20110232349A1 (en) * 2003-05-09 2011-09-29 Hebda John J Processing of titanium-aluminum-vanadium alloys and products made thereby
US8499605B2 (en) 2010-07-28 2013-08-06 Ati Properties, Inc. Hot stretch straightening of high strength α/β processed titanium
US8652400B2 (en) 2011-06-01 2014-02-18 Ati Properties, Inc. Thermo-mechanical processing of nickel-base alloys
US20150050513A1 (en) * 2011-12-30 2015-02-19 Babasaheb Neelkanth Kalyani Method For Manufacturing Hollow Shafts
US9050647B2 (en) 2013-03-15 2015-06-09 Ati Properties, Inc. Split-pass open-die forging for hard-to-forge, strain-path sensitive titanium-base and nickel-base alloys
US9192981B2 (en) 2013-03-11 2015-11-24 Ati Properties, Inc. Thermomechanical processing of high strength non-magnetic corrosion resistant material
US9206497B2 (en) 2010-09-15 2015-12-08 Ati Properties, Inc. Methods for processing titanium alloys
US9255316B2 (en) 2010-07-19 2016-02-09 Ati Properties, Inc. Processing of α+β titanium alloys
US9777361B2 (en) 2013-03-15 2017-10-03 Ati Properties Llc Thermomechanical processing of alpha-beta titanium alloys
US9869003B2 (en) 2013-02-26 2018-01-16 Ati Properties Llc Methods for processing alloys
US10094003B2 (en) 2015-01-12 2018-10-09 Ati Properties Llc Titanium alloy
US10435775B2 (en) 2010-09-15 2019-10-08 Ati Properties Llc Processing routes for titanium and titanium alloys
US10502252B2 (en) 2015-11-23 2019-12-10 Ati Properties Llc Processing of alpha-beta titanium alloys
US10513755B2 (en) 2010-09-23 2019-12-24 Ati Properties Llc High strength alpha/beta titanium alloy fasteners and fastener stock
US11111552B2 (en) 2013-11-12 2021-09-07 Ati Properties Llc Methods for processing metal alloys

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US144832A (en) * 1873-11-25 Improvement in dies for forging wrench-bars
US503481A (en) * 1893-08-15 Method of forging axles
US2950191A (en) * 1951-05-31 1960-08-23 Crucible Steel Co America Titanium base alloys
US3194693A (en) * 1962-06-12 1965-07-13 Paul J Soltis Process for increasing mechanical properties of titanium alloys high in aluminum

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US144832A (en) * 1873-11-25 Improvement in dies for forging wrench-bars
US503481A (en) * 1893-08-15 Method of forging axles
US2950191A (en) * 1951-05-31 1960-08-23 Crucible Steel Co America Titanium base alloys
US3194693A (en) * 1962-06-12 1965-07-13 Paul J Soltis Process for increasing mechanical properties of titanium alloys high in aluminum

Cited By (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3383233A (en) * 1965-12-22 1968-05-14 Park Ohio Industries Inc Method and apparatus for inductively heating a workpiece formed from a highly oxidizable metal
US3489617A (en) * 1967-04-11 1970-01-13 Titanium Metals Corp Method for refining the beta grain size of alpha and alpha-beta titanium base alloys
US3867208A (en) * 1970-11-24 1975-02-18 Nikolai Alexandrovich Grekov Method for producing annular forgings
US4055975A (en) * 1977-04-01 1977-11-01 Lockheed Aircraft Corporation Precision forging of titanium
US4145903A (en) * 1978-04-03 1979-03-27 Textron Inc. Sheet forming method and apparatus
US4991419A (en) * 1988-11-18 1991-02-12 Sumitomo Metal Industries, Ltd. Method of manufacturing seamless tube formed of titanium material
US5026520A (en) * 1989-10-23 1991-06-25 Cooper Industries, Inc. Fine grain titanium forgings and a method for their production
US5795413A (en) * 1996-12-24 1998-08-18 General Electric Company Dual-property alpha-beta titanium alloy forgings
US8597443B2 (en) 2003-05-09 2013-12-03 Ati Properties, Inc. Processing of titanium-aluminum-vanadium alloys and products made thereby
US9796005B2 (en) 2003-05-09 2017-10-24 Ati Properties Llc Processing of titanium-aluminum-vanadium alloys and products made thereby
US8597442B2 (en) 2003-05-09 2013-12-03 Ati Properties, Inc. Processing of titanium-aluminum-vanadium alloys and products of made thereby
US20110232349A1 (en) * 2003-05-09 2011-09-29 Hebda John J Processing of titanium-aluminum-vanadium alloys and products made thereby
US8048240B2 (en) 2003-05-09 2011-11-01 Ati Properties, Inc. Processing of titanium-aluminum-vanadium alloys and products made thereby
US9523137B2 (en) 2004-05-21 2016-12-20 Ati Properties Llc Metastable β-titanium alloys and methods of processing the same by direct aging
US20110038751A1 (en) * 2004-05-21 2011-02-17 Ati Properties, Inc. Metastable beta-titanium alloys and methods of processing the same by direct aging
US10422027B2 (en) 2004-05-21 2019-09-24 Ati Properties Llc Metastable beta-titanium alloys and methods of processing the same by direct aging
US20100307647A1 (en) * 2004-05-21 2010-12-09 Ati Properties, Inc. Metastable Beta-Titanium Alloys and Methods of Processing the Same by Direct Aging
US7837812B2 (en) 2004-05-21 2010-11-23 Ati Properties, Inc. Metastable beta-titanium alloys and methods of processing the same by direct aging
US8623155B2 (en) 2004-05-21 2014-01-07 Ati Properties, Inc. Metastable beta-titanium alloys and methods of processing the same by direct aging
US20050257864A1 (en) * 2004-05-21 2005-11-24 Brian Marquardt Metastable beta-titanium alloys and methods of processing the same by direct aging
US8568540B2 (en) 2004-05-21 2013-10-29 Ati Properties, Inc. Metastable beta-titanium alloys and methods of processing the same by direct aging
US20070193662A1 (en) * 2005-09-13 2007-08-23 Ati Properties, Inc. Titanium alloys including increased oxygen content and exhibiting improved mechanical properties
US8337750B2 (en) 2005-09-13 2012-12-25 Ati Properties, Inc. Titanium alloys including increased oxygen content and exhibiting improved mechanical properties
US9593395B2 (en) 2005-09-13 2017-03-14 Ati Properties Llc Titanium alloys including increased oxygen content and exhibiting improved mechanical properties
US7611592B2 (en) 2006-02-23 2009-11-03 Ati Properties, Inc. Methods of beta processing titanium alloys
US20070193018A1 (en) * 2006-02-23 2007-08-23 Ati Properties, Inc. Methods of beta processing titanium alloys
US10053758B2 (en) 2010-01-22 2018-08-21 Ati Properties Llc Production of high strength titanium
US20110180188A1 (en) * 2010-01-22 2011-07-28 Ati Properties, Inc. Production of high strength titanium
US10144999B2 (en) 2010-07-19 2018-12-04 Ati Properties Llc Processing of alpha/beta titanium alloys
US9255316B2 (en) 2010-07-19 2016-02-09 Ati Properties, Inc. Processing of α+β titanium alloys
US9765420B2 (en) 2010-07-19 2017-09-19 Ati Properties Llc Processing of α/β titanium alloys
US8499605B2 (en) 2010-07-28 2013-08-06 Ati Properties, Inc. Hot stretch straightening of high strength α/β processed titanium
US8834653B2 (en) 2010-07-28 2014-09-16 Ati Properties, Inc. Hot stretch straightening of high strength age hardened metallic form and straightened age hardened metallic form
US9206497B2 (en) 2010-09-15 2015-12-08 Ati Properties, Inc. Methods for processing titanium alloys
US10435775B2 (en) 2010-09-15 2019-10-08 Ati Properties Llc Processing routes for titanium and titanium alloys
US9624567B2 (en) 2010-09-15 2017-04-18 Ati Properties Llc Methods for processing titanium alloys
US10513755B2 (en) 2010-09-23 2019-12-24 Ati Properties Llc High strength alpha/beta titanium alloy fasteners and fastener stock
US10287655B2 (en) 2011-06-01 2019-05-14 Ati Properties Llc Nickel-base alloy and articles
US8652400B2 (en) 2011-06-01 2014-02-18 Ati Properties, Inc. Thermo-mechanical processing of nickel-base alloys
US9616480B2 (en) 2011-06-01 2017-04-11 Ati Properties Llc Thermo-mechanical processing of nickel-base alloys
US9446445B2 (en) * 2011-12-30 2016-09-20 Bharat Forge Ltd. Method for manufacturing hollow shafts
US20150050513A1 (en) * 2011-12-30 2015-02-19 Babasaheb Neelkanth Kalyani Method For Manufacturing Hollow Shafts
US10570469B2 (en) 2013-02-26 2020-02-25 Ati Properties Llc Methods for processing alloys
US9869003B2 (en) 2013-02-26 2018-01-16 Ati Properties Llc Methods for processing alloys
US9192981B2 (en) 2013-03-11 2015-11-24 Ati Properties, Inc. Thermomechanical processing of high strength non-magnetic corrosion resistant material
US10337093B2 (en) 2013-03-11 2019-07-02 Ati Properties Llc Non-magnetic alloy forgings
US9050647B2 (en) 2013-03-15 2015-06-09 Ati Properties, Inc. Split-pass open-die forging for hard-to-forge, strain-path sensitive titanium-base and nickel-base alloys
US10370751B2 (en) 2013-03-15 2019-08-06 Ati Properties Llc Thermomechanical processing of alpha-beta titanium alloys
US9777361B2 (en) 2013-03-15 2017-10-03 Ati Properties Llc Thermomechanical processing of alpha-beta titanium alloys
US11111552B2 (en) 2013-11-12 2021-09-07 Ati Properties Llc Methods for processing metal alloys
US10094003B2 (en) 2015-01-12 2018-10-09 Ati Properties Llc Titanium alloy
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