CN105326721A - Flaky microcapsule containing calendula extract - Google Patents
Flaky microcapsule containing calendula extract Download PDFInfo
- Publication number
- CN105326721A CN105326721A CN201510892164.4A CN201510892164A CN105326721A CN 105326721 A CN105326721 A CN 105326721A CN 201510892164 A CN201510892164 A CN 201510892164A CN 105326721 A CN105326721 A CN 105326721A
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- CN
- China
- Prior art keywords
- parts
- microcapsule
- flaky
- calendula extract
- present
- Prior art date
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a flaky microcapsule containing calendula extract, and belongs to the technical field of microcapsules. The flaky microcapsule containing calendula extract is prepared from, by weight, 50-55 parts of sodium alginate, 20-30 parts of carrageenan, 10-15 parts of hydroxyethyl cellulose, 5-8 parts of sodium hyaluronate, 10-15 parts of glycerinum, 0.1-0.5 part of the calendula extract, 0.1-0.3 part of D&G yellow number one, 0.1-0.3 part of titanium dioxide, 0.5-1 part of phenoxyethanol, 0.1-0.5 part of ethylhexylglycerin and 0.3-0.5 part of 1,2-octylene glycol. The flaky microcapsule has the moisturizing and oil control effects, aiming at the requirements of ensuring the effects and making stability of the prepared microcapsule high, it is found through creative research that only when the raw materials and the formula are selected, can the two requirements be met at the same time, and the prepared microcapsule is stable in character and high in quality.
Description
Technical field
The invention belongs to microcapsule technology field, be specifically related to a kind of lamellar microcapsule containing Flos Inulae extract.
Background technology
Consumer pursues the natural of cosmetic personal care's product and effect day by day, as an article of everyday use not only outward appearance want grace to be imbued with captivation and natural imaginative power, and to stablize with powerful.Now commercially add the interpolation product of plant, such as petal water, petal mile, perfume etc., but genuine plant is produce and preserve the problem all having a lot of stability in cosmetics: the cleaning of the plant material in such as production process, some plants keep insecticide, worm's ovums etc. are a very large polluter, and the composition in preservation process in plant soaks out and causes product unstable, the problems such as color is moved back and lost, the easy sensitization of pollen; The effective ingredient that a lot of plant proposes uses the problem that also there is various stability in cosmetics.
Present microcapsule product mostly is spherical shape, shape matching is single, do not have lamellar microcapsule, and lamellar more saves space compared to spherical microcapsule, can make cosmetic base while with the addition of lamellar microcapsule, can also ensure that the addition of substrate can not be restricted.Prior art does not prepare the correlational study of lamellar microcapsule, trace it to its cause is because usual gel solution can shrink balling-up or irregular gel piece due to surface tension, microcapsule raw material cannot be made to extend to surrounding, and then the microcapsule of slabbing or strip cannot be done, thus there is certain defect.
Summary of the invention
For prior art above shortcomings, technical problem to be solved by this invention is: how to provide a kind of lamellar microcapsule containing Flos Inulae extract, break the routine understanding that microcapsule product in prior art is spherical shape, and there is good stability, colory feature, and there is effect of moisturizing control oil, skin of releiving.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme: a kind of lamellar microcapsule containing Flos Inulae extract, with parts by weight, comprise following composition: 50 ~ 55 parts of sodium alginates, 20 ~ 30 parts of carrageenans, 10 ~ 15 parts of hydroxyethyl-celluloses, 5 ~ 8 parts of hyaluronate sodiums, 10 ~ 15 parts of glycerol, 0.1 ~ 0.5 part of Flos Inulae extract, 0.1 ~ 0.3 part of yellow No. 1,0.1 ~ 0.3 part titanium dioxide of D & C, 0.5 ~ 1 part of phenoxyethanol, 0.1 ~ 0.5 part of Sensiva SC50 and 0.3 ~ 0.5 part 1,2 ethohexadiols.
Compared to existing technology, the present invention has following beneficial effect:
1, the present invention utilizes alginate to run into divalent metal saline solution and can generate the principle of gel to prepare slice-shaped capsule, balling-up or irregular gel piece can be shunk due to surface tension time but alginic acid solution runs into divalent metal saline solution in prior art, therefore can not be prepared into lamellar microcapsule; For these reasons, the present invention finds by research in alginic acid solution, add the present invention's selection antiseptic or surfactant, the surface tension of colloid can be made to reduce, make composite after stock chart surface tension lower than saline solution, these reduce capillary material and open by the surface spreading of alginic acid solution at divalent metal saline solution, simultaneously and saline solution be reacted into class disk gel film, allow these gel film shapes be made a variation by the flowing of saline and arrive lamellar microcapsule.
2, because single alginate is unstable to a lot of material, easily by alkali, chelating agen, surfactants etc. are swelling and dissolve, so also composite other colloids or macromolecular material in raw material of the present invention, by the collaborative compatibility effect of each raw material, make lamellar microcapsule of the present invention base material such as mile, frost breast, bath gel, more stable in shampoo, well-behaved.
3, the collaborative compatibility effect in the present invention between each raw material, make lamellar microcapsule of the present invention easily softening and become and easily smear in containing base material, skinfeel is better.
4, the present invention is by the collaborative compatibility effect of Flos Inulae extract and hyaluronate sodium, makes the microcapsule obtained have effect of moisturizing control oil, skin of releiving.
5, the present invention is in order to while can ensureing this effect, and the product stability that obtains can also be made good, and the present invention is by creationary research, final discovery only has when selecting raw material of the present invention and formula, this two requirements could be taken into account simultaneously, the product property obtained is stablized, best in quality.
6, the inventive method can realize full automatic a large amount of commercial production, and without the need to manual operation, flow process is polluted few, and product quality is high, controllability and favorable reproducibility.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, in the present embodiment if no special instructions, raw materials used be commercially available.
The lamellar microcapsule that the present invention contains Flos Inulae extract is adopted and is prepared with the following method and obtain:
1) sodium alginate pure water is mixed with the solution that mass concentration is 2%, carrageenan pure water is mixed with the solution that mass concentration is 1%, hydroxyethyl-cellulose pure water is mixed with the solution that mass concentration is 1%, hyaluronate sodium pure water is mixed with the solution that mass concentration is 1%;
2), after the solution that step 1) is prepared being heated to 60 DEG C, mixed solution is also incubated, for subsequent use;
3) by glycerol and Flos Inulae extract mix homogeneously;
4) yellow for D & C No. 1 and titanium dioxide to be milled mixing, and be mixed in the mixed raw material of step 3), stir;
5) by phenoxyethanol, Sensiva SC50 and 1,2 ethohexadiols are mixed to join in the mixed material of step 4), obtain mixed material;
6) step 5) mixed material is added step 2) in mixed solution, carry out homogenizing, and the temperature keeping mixture is 60 ~ 70 DEG C, obtains equal pledge for subsequent use;
7) the equal pledge pump after equal for step 6) vacuum is exported and is added drop-wise on inclined-plane, on described inclined-plane trickling have mass concentration be 2% calcium chloride solution, obtain the lamellar microcapsule containing Flos Inulae extract.
embodiment 1:
A lamellar microcapsule containing Flos Inulae extract, component prescription is as shown in table 1 below:
Table 1 component prescription
embodiment 2
A lamellar microcapsule containing Flos Inulae extract, component prescription is as shown in table 2 below:
The lamellar microcapsule components formula of table 2 containing Flos Inulae extract
The present invention can also allow calcium chloride brine produce flowing, avoids colloid solution dropping point or streamline overlap, prepares lamellar microcapsule of the present invention.
What finally illustrate is, above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted, although applicant's reference preferred embodiment is to invention has been detailed description, those of ordinary skill in the art is to be understood that, technical scheme of the present invention is modified or equivalent replacement, and do not depart from the aim of technical solution of the present invention and scope, all should be encompassed in the middle of right of the present invention.
Claims (2)
1. the lamellar microcapsule containing Flos Inulae extract, is characterized in that, with parts by weight, comprise following composition:
50 ~ 55 parts of sodium alginates, 20 ~ 30 parts of carrageenans, 10 ~ 15 parts of hydroxyethyl-celluloses, 5 ~ 8 parts of hyaluronate sodiums, 10 ~ 15 parts of glycerol, 0.1 ~ 0.5 part of Flos Inulae extract, 0.1 ~ 0.3 part of yellow No. 1,0.1 ~ 0.3 part titanium dioxide of D & C, 0.5 ~ 1 part of phenoxyethanol, 0.1 ~ 0.5 part of Sensiva SC50 and 0.3 ~ 0.5 part 1,2 ethohexadiols.
2. the lamellar microcapsule according to claim 1 containing Flos Inulae extract, it is characterized in that, with parts by weight, comprise following composition: 50 parts of sodium alginates, 20 parts of carrageenans, 10 parts of hydroxyethyl-celluloses, 5 parts of hyaluronate sodiums, 10 parts of glycerol, 0.1 part of Flos Inulae extract, 0.1 part of yellow No. 1,0.1 part titanium dioxide of D & C, 0.5 part of phenoxyethanol, 0.1 part of Sensiva SC50 and 0.3 part 1,2 ethohexadiols.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892164.4A CN105326721B (en) | 2015-11-27 | 2015-11-27 | A kind of sheet microcapsules containing pot marigold extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892164.4A CN105326721B (en) | 2015-11-27 | 2015-11-27 | A kind of sheet microcapsules containing pot marigold extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105326721A true CN105326721A (en) | 2016-02-17 |
| CN105326721B CN105326721B (en) | 2018-07-10 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510892164.4A Active CN105326721B (en) | 2015-11-27 | 2015-11-27 | A kind of sheet microcapsules containing pot marigold extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105326721B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN102100713A (en) * | 2009-12-18 | 2011-06-22 | 中国科学院兰州化学物理研究所 | Method for preparing water-soluble marigold yellow pigment microcapsules |
| CN104490615A (en) * | 2014-12-16 | 2015-04-08 | 重庆小丸科贸有限公司 | Hydrogel microcapsule with pore minimizing efficacy |
-
2015
- 2015-11-27 CN CN201510892164.4A patent/CN105326721B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN102100713A (en) * | 2009-12-18 | 2011-06-22 | 中国科学院兰州化学物理研究所 | Method for preparing water-soluble marigold yellow pigment microcapsules |
| CN104490615A (en) * | 2014-12-16 | 2015-04-08 | 重庆小丸科贸有限公司 | Hydrogel microcapsule with pore minimizing efficacy |
Non-Patent Citations (2)
| Title |
|---|
| 宋丽晅: "《99%女人都在犯的护肤错误》", 31 January 2014 * |
| 王显伦: "锐孔法制备微胶囊技米研究", 《郑州粮食学院学报》 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105326721B (en) | 2018-07-10 |
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Address after: 401519 Chongqing Hechuan Industrial Park weir village two Patentee after: Chongqing Xiaowan Biotechnology Co., Ltd. Address before: 401519 Chongqing Hechuan Industrial Park weir village two Patentee before: CHONGQING XIAOWAN TRADE CO., LTD. |
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