CN105213282A - A kind of microcapsule-type becomes clear the preparation method of eye cream - Google Patents
A kind of microcapsule-type becomes clear the preparation method of eye cream Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention discloses a kind of microcapsule-type to become clear the preparation method of eye cream, with ammonium alginate, sodium polyacrylate, hyaluronic acid, mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, corn porous starch, wych-elm ethanol extract, arabidopsis ethanol extract, Lac regis apis, bisabolol, coenzyme Q10 and span 20 for raw material, first prepare capsule wall solution A and capsule-core solution B, A and B is mixed, first dispersed with stirring again homogenizing obtains homogenizing fluid C, homogenizing fluid C is instilled in magnesium chloride solution, wash after filtration, obtain described bright eye cream.The microcapsule-type that the present invention obtains becomes clear eye cream in use, can make to be adsorbed on active component in corn porous starch and oils and fats slowly evenly discharges, and can not discharge in a large number the short time and bring too much nutrition and oil content to skin, and then can not cause the generation of fat granule, and the present invention also has the feature of good penetrability.
Description
Technical field
The invention belongs to microcapsule technology field, be specifically related to a kind of microcapsule-type and become clear the preparation method of eye cream.
Background technology
Eye skin is the thinnest skin of human body, is again activity position the most frequently simultaneously, but also is pull the maximum place of skin number of times in making up, and is very easy to grow wrinkle.The FAQs of eye has following several: black eye, eye pouch, edema, microgroove, dry stricture of vagina, crows-feet, fat granule, eyes lack expression etc., and these eye problems, once occur, are easy to make people seem aged without god.Eye cream is one of skin type product, and it can moisten eye part skin, alleviates the generation of wrinkle, microgroove, effectively prevents the generation of black eye, eye pouch problem, totally plays the effect alleviating eye part skin aging.Based on above-mentioned effect of eye cream, the personage that more and more likes to be beautiful using eye cream as one of daily indispensable skin care item.
If but the eye cream used is improper, also can bring certain harmful effect to eye skin.As most higher containing lubricant component in existing eye cream, contained neutraceutical active ingredients discharges too fast and is not easily absorbed, these oils and fatss or nutritional labeling are deposited on eye part skin, be easy to the generation causing fat granule for a long time in the past, fat granule, once produce elimination in the very difficult short time, can not be despised on the impact that eye part skin causes; If but the eye cream using quality comparatively frivolous, the moist degree of eye cream can be made again to decline, do not reach good maintenance effect.Moreover; the active substance adopted in existing eye cream is most not through certain protection, and directly contacts with external environment, along with the prolongation of time; these active substances be easy to be oxidized by the external world, photodissociation and lose the activity that should possess, and then cause product failure.
Summary of the invention
For prior art above shortcomings, technical problem to be solved by this invention is: how to provide the preparation method that a kind of microcapsule-type becomes clear eye cream, the product Middle nutrition active component making the method obtained evenly can discharge in use and be easy to absorb, have nourish effective, can not cause that fat granule produces, active substance is not easily by feature that external environment is destroyed.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme: a kind of microcapsule-type becomes clear the preparation method of eye cream, comprises the steps:
1) material of following weight portion is taken: 48 ~ 54 parts of ammonium alginates, 10 ~ 16 parts of sodium polyacrylate, 6 ~ 12 parts of hyaluronic acids, 20 ~ 24 parts of mink oils, 7 ~ 11 parts of squalanes, 3 ~ 4 parts of lecithin, 4 ~ 7 parts of Jojoba waxes, 16 ~ 18 parts of glycerol, 2 ~ 6 parts of batilols, 4 ~ 6 parts of serines, 6 ~ 10 parts of corn porous starch, 3 ~ 5 parts of wych-elm ethanol extract, 3 ~ 4 parts of arabidopsis ethanol extract, 2 ~ 3 parts of Lac regis apis, 1 ~ 2 part of bisabolol, 2 ~ 5 parts of coenzyme Q10s and 2 ~ 8 parts of span 20s;
2) add in deionized water by the ammonium alginate taken, sodium polyacrylate and hyaluronic acid, at 50 ~ 60 DEG C, Ultrasonic Heating dissolves 3 ~ 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 35 ~ 55 times of ammonium alginate, sodium polyacrylate and hyaluronic acid gross mass; Ultrasonic power is 400 ~ 450W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, corn porous starch, wych-elm ethanol extract, arabidopsis ethanol extract, Lac regis apis, bisabolol, coenzyme Q10 and the surfactant mix homogeneously that will take, under 75 ~ 80 DEG C of water bath condition, stir 0.5 ~ 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 220 ~ 260r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 10 ~ 15min, homogenizing 5 ~ 8min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 300 ~ 350r/min, and the homogenization pressure of described homogenizing is 50 ~ 55MPa;
5) homogenizing fluid C is heated to 75 ~ 80 DEG C, using glue head dropper that the homogenizing fluid C after heating is slowly added dropwise to mass concentration is in the magnesium chloride solution of 3% ~ 6%;
6) magnesium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, obtain described microcapsule-type and to become clear eye cream.
Compared to existing technology, the present invention has following beneficial effect:
1, the present invention adopts corn porous starch, lubricant component in core materials and active component are adsorbed, and then the microcapsule-type making the present invention obtain becomes clear eye cream in use, can make to be adsorbed on active component in corn porous starch and oils and fats slowly evenly discharges, and can not discharge in a large number the short time and bring too much nutrition and oil content to skin, and then the generation of fat granule can not be caused.
2, the microcapsule-type obtained to strengthen the present invention becomes clear the permeability of eye cream, the present invention is special by a large amount of experimental studies, choose mink oil, squalane, Jojoba wax, batilol is as core materials, and the collaborative compatibility relationship that further study between a few person, final discovery is when using " 20 ~ 24 parts of mink oils, 7 ~ 11 parts of squalanes, 4 ~ 7 parts of Jojoba waxes and 2 ~ 6 parts of batilols " time, the moist degree of this product can either be ensured, again can not be too greasy, and what is more important is when this several material plays collaborative compatibility effect with this ratio, the permeability of this product can be strengthened, and then enable skin fully absorb nutritional labeling, import respond well.
3, the present invention adopts microcapsule technology, neutraceutical active ingredients embedding is got up, makes this product in use, can not the impact that in external environment, light, heat, oxygen etc. are too much be subject to, effectively ensure that the activity of active substance is not destroyed, the effect extending product keeps the phase.
4, the present invention adopts active skull cap components as nutrient, and this several natural materials is carried out composite, them are made farthest to play collaborative compatibility effect, give preparation method that microcapsule-type of the present invention becomes clear eye cream to eliminate black eye, to promote the composite efficacy of eye skin blood circulation, nourishing, and bisabolol also has good antiinflammatory action, to scytitis, there is good curative effect.
5, cyst wall hydrogel material of the present invention brings certain water moisture feeling to this product, and hyaluronic interpolation further increases the performance of keeping humidity of product, make this product in use, it is easier that eye part skin is pushed open, only need massage gently with finger and get final product uniform application, use convenient, the overnutrition at this position will be made to cause fat granule because product is deposited in a certain position of eye part skin.
6, shape of product of the present invention is regular, cyst wall has uniform thickness, and has uniform intensity, can retain the perfect shape of microcapsule and not be destroyed, the problem that capsule-core is revealed can not be caused, can not be damaged during effectively ensureing product stock, transport, shelf life.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, in the present embodiment if no special instructions, raw materials used be commercially available.
Described wych-elm ethanol extract, arabidopsis ethanol extract are after the ethanol water of employing 70% carries out alcohol extraction to wych-elm, arabidopsis respectively, successively the extract that obtains of decompression recycling ethanol, lyophilization.
Embodiment 1:
The present embodiment microcapsule-type eye cream that becomes clear is a kind of microcapsule of nucleocapsid structure, and cyst material is: 48 parts of ammonium alginates, 10 parts of sodium polyacrylate and 6 parts of hyaluronic acids; Core materials is: 20 parts of mink oils, 7 parts of squalanes, 3 parts of lecithin, 4 parts of Jojoba waxes, 16 parts of glycerol, 2 parts of batilols, 4 parts of serines, 6 parts of corn porous starch, 3 parts of wych-elm ethanol extract, 3 parts of arabidopsis ethanol extract, 2 parts of Lac regis apis, 1 part of bisabolol, 2 parts of coenzyme Q10s and 2 parts of span 20s 0.
Adopt and be prepared with the following method:
1) material of above-mentioned weight portion is taken;
2) add in deionized water by the ammonium alginate taken, sodium polyacrylate and hyaluronic acid, at 50 DEG C, Ultrasonic Heating dissolves 3min, obtains capsule wall solution A; Wherein, the deionized water volume added is 35 times of ammonium alginate, sodium polyacrylate and hyaluronic acid gross mass; Ultrasonic power is 400W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, corn porous starch, wych-elm ethanol extract, arabidopsis ethanol extract, Lac regis apis, bisabolol, coenzyme Q10 and the surfactant mix homogeneously that will take, under 75 DEG C of water bath condition, stir 0.5h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 220r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 10min, homogenizing 5min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 300r/min, and the homogenization pressure of described homogenizing is 50MPa;
5) homogenizing fluid C is heated to 75 DEG C, using glue head dropper that the homogenizing fluid C after heating is slowly added dropwise to mass concentration is in the magnesium chloride solution of 3%;
6) magnesium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, obtain described microcapsule-type and to become clear eye cream.
Embodiment 2:
The present embodiment microcapsule-type eye cream that becomes clear is a kind of microcapsule of nucleocapsid structure, and cyst material is: 54 parts of ammonium alginates, 16 parts of sodium polyacrylate and 12 parts of hyaluronic acids; Core materials is: 24 parts of mink oils, 11 parts of squalanes, 4 parts of lecithin, 7 parts of Jojoba waxes, 18 parts of glycerol, 6 parts of batilols, 6 parts of serines, 10 parts of corn porous starch, 5 parts of wych-elm ethanol extract, 4 parts of arabidopsis ethanol extract, 3 parts of Lac regis apis, 2 parts of bisabolols, 5 parts of coenzyme Q10s and 8 parts of span 20s.
Adopt and be prepared with the following method:
1) material of above-mentioned weight portion is taken;
2) add in deionized water by the ammonium alginate taken, sodium polyacrylate and hyaluronic acid, at 60 DEG C, Ultrasonic Heating dissolves 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 55 times of ammonium alginate, sodium polyacrylate and hyaluronic acid gross mass; Ultrasonic power is 450W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, corn porous starch, wych-elm ethanol extract, arabidopsis ethanol extract, Lac regis apis, bisabolol, coenzyme Q10 and the surfactant mix homogeneously that will take, under 80 DEG C of water bath condition, stir 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 260r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 15min, homogenizing 8min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 350r/min, and the homogenization pressure of described homogenizing is 55MPa;
5) homogenizing fluid C is heated to 80 DEG C, using glue head dropper that the homogenizing fluid C after heating is slowly added dropwise to mass concentration is in the magnesium chloride solution of 6%;
6) magnesium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, obtain described microcapsule-type and to become clear eye cream.
Embodiment 3:
The present embodiment microcapsule-type eye cream that becomes clear is a kind of microcapsule of nucleocapsid structure, and cyst material is: 52 parts of ammonium alginates, 14 parts of sodium polyacrylate and 10 parts of hyaluronic acids; Core materials is: 22 parts of mink oils, 10 parts of squalanes, 4 parts of lecithin, 6 parts of Jojoba waxes, 18 parts of glycerol, 5 parts of batilols, 6 parts of serines, 8 parts of corn porous starch, 5 parts of wych-elm ethanol extract, 3 parts of arabidopsis ethanol extract, 2 parts of Lac regis apis, 1 part of bisabolol, 4 parts of coenzyme Q10s and 6 parts of span 20s.
Adopt and be prepared with the following method:
1) material of above-mentioned weight portion is taken;
2) add in deionized water by the ammonium alginate taken, sodium polyacrylate and hyaluronic acid, at 55 DEG C, Ultrasonic Heating dissolves 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 45 times of ammonium alginate, sodium polyacrylate and hyaluronic acid gross mass; Ultrasonic power is 400W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, corn porous starch, wych-elm ethanol extract, arabidopsis ethanol extract, Lac regis apis, bisabolol, coenzyme Q10 and the surfactant mix homogeneously that will take, under 80 DEG C of water bath condition, stir 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 240r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 12min, homogenizing 6min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 330r/min, and the homogenization pressure of described homogenizing is 52MPa;
5) homogenizing fluid C is heated to 78 DEG C, using glue head dropper that the homogenizing fluid C after heating is slowly added dropwise to mass concentration is in the magnesium chloride solution of 6%;
6) magnesium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, obtain described microcapsule-type and to become clear eye cream.
The present invention adopts corn porous starch, lubricant component in core materials and active component are adsorbed, and then the microcapsule-type making the present invention obtain becomes clear eye cream in use, can make to be adsorbed on active component in corn porous starch and oils and fats slowly evenly discharges, and can not discharge in a large number the short time and bring too much nutrition and oil content to skin, and then the generation of fat granule can not be caused.
The microcapsule-type obtained to strengthen the present invention becomes clear the permeability of eye cream, the present invention is special by a large amount of experimental studies, choose mink oil, squalane, Jojoba wax, batilol is as core materials, and the collaborative compatibility relationship that further study between a few person, final discovery is when using " 20 ~ 24 parts of mink oils, 7 ~ 11 parts of squalanes, 4 ~ 7 parts of Jojoba waxes and 2 ~ 6 parts of batilols " time, the moist degree of this product can either be ensured, again can not be too greasy, and what is more important is when this several material plays collaborative compatibility effect with this ratio, the permeability of this product can be strengthened, and then enable skin fully absorb nutritional labeling, import respond well.
What finally illustrate is, above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted, although applicant's reference preferred embodiment is to invention has been detailed description, those of ordinary skill in the art is to be understood that, technical scheme of the present invention is modified or equivalent replacement, and do not depart from the aim of technical solution of the present invention and scope, all should be encompassed in the middle of right of the present invention.
Claims (5)
1. microcapsule-type becomes clear a preparation method for eye cream, it is characterized in that, comprises the steps:
1) material of following weight portion is taken: 48 ~ 54 parts of ammonium alginates, 10 ~ 16 parts of sodium polyacrylate, 6 ~ 12 parts of hyaluronic acids, 20 ~ 24 parts of mink oils, 7 ~ 11 parts of squalanes, 3 ~ 4 parts of lecithin, 4 ~ 7 parts of Jojoba waxes, 16 ~ 18 parts of glycerol, 2 ~ 6 parts of batilols, 4 ~ 6 parts of serines, 6 ~ 10 parts of corn porous starch, 3 ~ 5 parts of wych-elm ethanol extract, 3 ~ 4 parts of arabidopsis ethanol extract, 2 ~ 3 parts of Lac regis apis, 1 ~ 2 part of bisabolol, 2 ~ 5 parts of coenzyme Q10s and 2 ~ 8 parts of span 20s;
2) add in deionized water by the ammonium alginate taken, sodium polyacrylate and hyaluronic acid, at 50 ~ 60 DEG C, Ultrasonic Heating dissolves 3 ~ 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 35 ~ 55 times of ammonium alginate, sodium polyacrylate and hyaluronic acid gross mass; Ultrasonic power is 400 ~ 450W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, corn porous starch, wych-elm ethanol extract, arabidopsis ethanol extract, Lac regis apis, bisabolol, coenzyme Q10 and the surfactant mix homogeneously that will take, under 75 ~ 80 DEG C of water bath condition, stir 0.5 ~ 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 220 ~ 260r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 10 ~ 15min, homogenizing 5 ~ 8min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 300 ~ 350r/min, and the homogenization pressure of described homogenizing is 50 ~ 55MPa;
5) homogenizing fluid C is heated to 75 ~ 80 DEG C, using glue head dropper that the homogenizing fluid C after heating is slowly added dropwise to mass concentration is in the magnesium chloride solution of 3% ~ 6%;
6) magnesium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, obtain described microcapsule-type and to become clear eye cream.
2. microcapsule-type becomes clear the preparation method of eye cream according to claim 1, it is characterized in that, step 2) in ultrasonic power be 400W.
3. microcapsule-type becomes clear the preparation method of eye cream according to claim 1, and it is characterized in that, mixing speed described in step 3) is 240r/min.
4. microcapsule-type becomes clear the preparation method of eye cream according to claim 1, it is characterized in that, with after blender dispersion 12min in step 4), and homogenizing 6min.
5. microcapsule-type becomes clear the preparation method of eye cream according to claim 1, and it is characterized in that, the rotating speed of blender described in step 4) is 330r/min, and the homogenization pressure of described homogenizing is 52MPa.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN103202469A (en) * | 2013-03-28 | 2013-07-17 | 吉林大学 | Egg yolk lecithin microcapsules and preparation method thereof |
| CN104398392A (en) * | 2014-12-01 | 2015-03-11 | 重庆小丸科贸有限公司 | Hydrogel microcapsule and application thereof in anti-ageing cosmetic |
-
2015
- 2015-10-30 CN CN201510721492.8A patent/CN105213282A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN103202469A (en) * | 2013-03-28 | 2013-07-17 | 吉林大学 | Egg yolk lecithin microcapsules and preparation method thereof |
| CN104398392A (en) * | 2014-12-01 | 2015-03-11 | 重庆小丸科贸有限公司 | Hydrogel microcapsule and application thereof in anti-ageing cosmetic |
Non-Patent Citations (4)
| Title |
|---|
| 吴克刚等: "《食品微胶囊技术》", 31 July 2006, 中国轻工业出版社 * |
| 杨晓东等: "《日用化学品生产技术》", 31 July 2008, 化学工业出版社 * |
| 王建新: "《化妆品天然功能成分》", 31 January 2007, 化学工业出版社 * |
| 马振友等: "《皮肤美容化妆品制剂手册》", 31 March 2004, 中医古籍出版社 * |
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