CN104146922A - Sun-blocking and moisturizing composition and preparation method thereof - Google Patents
Sun-blocking and moisturizing composition and preparation method thereof Download PDFInfo
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- CN104146922A CN104146922A CN201410425431.2A CN201410425431A CN104146922A CN 104146922 A CN104146922 A CN 104146922A CN 201410425431 A CN201410425431 A CN 201410425431A CN 104146922 A CN104146922 A CN 104146922A
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Abstract
The invention provides a sun-blocking and moisturizing composition and a preparation method thereof. The composition is composed of following components including, by weight, 4-6% of propylene glycol laurate/ethyecellulose/propylene glycol isostearate, 1-2% of shea butter, 0.2-0.3% of tocopheryl acetate, 2% of ethylhexyl methoxycinnamate, 2.5% of butyl methoxydibenzoylmethane, 3-4% of isononyl isononanoate, 2% of decamethylcyclopentasiloxane, 1% of polydimethylsiloxane, 0.3-0.4% of an acrylic acid (ester)/C10-30 alkanolacrylate crosslinking polymer, 0.1% of xanthan gum, 0.02% of disodium EDTA, 0.02% of sodium hyaluronate, 3-4% of butanediol, 3-4% of glycerin, 3% of glyceryl polyether-26, 0.15-0.2% of an aminomethyl propanol/water premixed substance, 3% of water/butanediol/purslane extract, 0.5% of a bacteriostatic agent, 2% of a water/glycerin/phenoxyethanol/[beta]-glucan premixed substance and the balance deionized water. The sun-blocking and moisturizing composition is suitable for sensitive skin, has a touching-melt texture, can form a compact and soft residual film on a skin surface and enable active components to be absorbed better by the skin.
Description
Technical field
The invention belongs to filed of daily-use chemical industry, particularly skin care field, is specifically related to a kind of sun-proof moisture-keeping composition, and the preparation method of this sun-proof moisture-keeping composition.
Background technology
Skin is the first barrier that human body stops the harmful substances such as extraneous antibacterial, virus, dust, when skin is accepted after ultraviolet overexposure, can damage epidermis cell; Activation Tyrosinase, accelerates pigment synthesis, destroys the moisture-keeping functions of skin, makes skin become dry, makes the elastic fibers in skin corium impaired, and microgroove is produced, and under acute irradiation, also can cause skin inflammation, burn.While having abnormal case, can become the skin carcinoma of pigment etc.In the time that air themperature reduces, keratodermatitis can not regulate enough Moisture factor in time, and oils and fats gland liveness declines, and oils and fats, moisture decline on the face, and skin there will be tight phenomenon, even now and the existing microgroove of nose branch.Therefore, in daily life, should focus on the moisturizing of skin and sun-proof.
As everyone knows, when surfactant and cleaning agent are used on sensitive skin, can cause stimulating and dehydration problem.But both to have had the material that hydrophilic component also has lipophilic constituent be necessary in order moisture and nutritional labeling to be provided to skin, to add simultaneously, usual way is: adopt surfactant to make emulsified body.But surfactant but can disturb the balance of nature of skin.In addition, more thick and heavy containing the cream frost texture of emulsifying agent, can not form fine and close soft residual film, in the time of perspiration and humidity change, may take away fast the active component on skin.
Summary of the invention
The object of the invention is the problem that will solve for above, provide a kind of texture frivolous, applicable responsive skin, performance of keeping humidity and sun-proof well behaved sun-proof moisture-keeping composition.
Another object of the present invention is to provide the preparation method of described sun-proof moisture-keeping composition.
To achieve these goals, the invention provides a kind of sun-proof moisture-keeping composition, its component by following percentage by weight forms: propylene glycol laurate/ethyl cellulose/propylene glycol isostearate 4~6%, Butyrospermum parkii fruit fat 1~2%, tocopherol acetas 0.2~0.3%, ethylhexyl methoxy cinnamate 2%, PAROSOL 1789 2.5%, isononyl isononanoate 3~4%, encircle five polydimethylsiloxane 2%, polydimethylsiloxane 1%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.3~0.4%, xanthan gum 0.1%, EDETATE SODIUM 0.02%, hyaluronate sodium 0.02%, butanediol 3~4%, glycerol 3~4%, glycerin polyether-263%, aminomethyl propanol/water pre-composition 0.15~0.2%, water/butanediol/Herba portulacae extract 3%, antibacterial 0.5%, water/glycerol/phenoxyethanol/beta glucan pre-composition 2%, deionized water surplus.
Preferably, described sun-proof moisture-keeping composition is made up of the component of following percentage by weight: propylene glycol laurate/ethyl cellulose/propylene glycol isostearate 5%, Butyrospermum parkii fruit fat 1%, tocopherol acetas 0.2%, ethylhexyl methoxy cinnamate 2%, PAROSOL 1789 2.5%, isononyl isononanoate 3%, encircle five polydimethylsiloxane 2%, polydimethylsiloxane 1%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.4%, xanthan gum 0.1%, EDETATE SODIUM 0.02%, hyaluronate sodium 0.02%, butanediol 4%, glycerol 3%, glycerin polyether-263%, aminomethyl propanol/water pre-composition 0.2%, water/butanediol/Herba portulacae extract pre-composition 3%, antibacterial 0.5%, water/glycerol/phenoxyethanol/beta glucan pre-composition 2%, deionized water surplus.
Preferably, described antibacterial is caprylyl glycol/1,2-hexanediol/methyl-benzyl alcohol pre-composition.More preferably, described caprylyl glycol/1, in 2-hexanediol/methyl-benzyl alcohol pre-composition, each composition weight ratio is: caprylyl glycol 50%, methyl-benzyl alcohol 10~25%, 1,2-hexanediol 10~25%.
Preferably, in described aminomethyl propanol/water pre-composition, the mass ratio of aminomethyl propanol and water is 19:1.
Preferably, in described water/butanediol/Herba portulacae extract pre-composition, each composition weight ratio is: water 69.4~69.8, butanediol 30%, Herba portulacae extract 0.2~0.6%.。
Preferably, in described water/glycerol/phenoxyethanol/beta glucan pre-composition, each composition weight ratio is: water 79~79.4%, glycerol 20%, phenoxyethanol 0.4%, beta glucan 0.2~0.6%.
The present invention also provides the preparation method of described sun-proof moisture-keeping composition, and its step is as follows:
(1) by propylene glycol laurate/ethyl cellulose/propylene glycol isostearate, isononyl isononanoate, tocopherol acetas, ethylhexyl methoxy cinnamate, PAROSOL 1789, Butyrospermum parkii (BUTYROSPERMUM PARKII) fruit fat, ring five polydimethylsiloxane, polydimethylsiloxane premixing evenly and be heated to 80~82 DEG C, form oil phase gel;
(2) by deionized water, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, xanthan gum, EDETATE SODIUM, hyaluronate sodium, butanediol, glycerol, glycerin polyether-26 mix homogeneously, and be warming up to 80~82 DEG C; Add aminomethyl propanol/water pre-composition to stir, form gel aqueous phase;
(3), under stirring, the oil phase gel that step (1) is obtained evenly adds in the gel aqueous phase that step (2) obtains, and homogenizing;
(4) stir and be cooled to 45 DEG C when following, add water/butanediol/Herba portulacae extract pre-composition, antibacterial, water/glycerol/phenoxyethanol/beta glucan pre-composition, stir.
Preferably, in described step (3), the speed of stirring is 600~700rpm.
Compared with prior art, sun-proof moisture-keeping composition of the present invention is frivolous soft, moisturizing and sun-proof functional, not containing surfactant, being applicable to responsive skin uses, and have and texture as white incomparable tactile the melting of common cream, it can form fine and close soft residual film at skin surface after smearing, and active component is better absorbed by skin.
Brief description of the drawings
Fig. 1 is organoleptic analysis's assessment result of the moisture-keeping composition of embodiments of the invention 1~3.
Fig. 2 is the water-resistance assessment result of the moisture-keeping composition of embodiments of the invention 1~3.
Fig. 3 is the moisture-keeping composition of embodiments of the invention 1~3 and the moisture-keeping efficacy assessment result that contains the common moisturiser of emulsifying agent.
Detailed description of the invention
Further set forth the present invention below in conjunction with specific embodiment.Should be understood that these embodiment are only not used in restriction range of application of the present invention for the present invention is described.The raw material that following examples are used all can be buied by market sale channel.Wherein, propylene glycol laurate/ethyl cellulose/propylene glycol isostearate, propylene glycol laurate (with) ethyl cellulose (with) propylene glycol isostearate (EMULFREE P, Gattefoss é).Described aminomethyl propanol/water pre-composition is the AMP-ULTRA PC 2000 that aminomethyl propanol (moisture 5wt%) provides purchased from DOW CHEMICAL.Water (with) glycerol (with) phenoxyethanol (with) SC Glucan that beta glucan pre-composition provides purchased from Bioland, wherein each composition weight ratio is: water 79~79.4%, glycerol 20%, phenoxyethanol 0.4%, beta glucan 0.2~0.6%.Water (with) butanediol (with) Portulaca that provides for Bioland of the pre-composition of Herba Portulacae (PORTULACAOLERACEA) extract, wherein each composition weight ratio is: water 69.4~69.8, butanediol 30%, Herba portulacae extract 0.2~0.6%.Caprylyl glycol (with) methyl-benzyl alcohol (with) 1, the SymTriol that 2-hexanediol pre-composition provides for Symrise, wherein each composition weight ratio is: caprylyl glycol 50%, methyl-benzyl alcohol 10~25%, 1,2-hexanediol 10~25%.
In accordance with the following steps, the moisturiser of Preparation Example 1~3:
1. by the premixing of A component evenly and be heated to 80~82 DEG C, form oil phase gel;
2. by B component mix homogeneously, and be warming up to 80~82 DEG C; Add C component to stir, form gel aqueous phase;
3. under middling speed (600~700rpm) stirring, A component is evenly added to B, C blending ingredients, and homogenizing;
4. stir and be cooled to 45 DEG C when following, add D component, stir;
5. be up to the standards, discharging fill, pH value scope: 5.5~7.5.
The moisture-keeping composition of embodiment 1~3 is carried out to zest assessment, organoleptic analysis's assessment, the test of keratodermatitis water content and water-resistance evaluation test.The common moisturiser that use contains emulsifying agent in contrast.
1. zest assessment (human skin patch result)
1.1 evaluation methodologys:
1.2 tested materials: cosmetics finished product.
1.3 negative controls: blank.
1.4 experimenters: totally 30 people, male 10 people, female 20 people, at 21~49 years old age, meet experimenter and volunteer inclusion criteria.
1.5 speckle method for testing: select qualified speckle examination device, with closed patch test method, about tested material 0.02ml~0.025ml is applied in speckle examination device, external special adhesive tape sticks in the bent side of experimenter's forearm, after 24 hours, remove tested material, 30min after removing tested material speckle examination device observes dermoreaction after impression disappears, and records its result by dermoreaction grade scale in " cosmetics health specification " (version in 2007).
Evaluation of result: record reaction result by table 1 (skin adverse reaction grade scale).
Table 1 skin adverse reaction grade scale
Result of the test shows: the dermoreaction of embodiment 1,2,3 is 0 grade, little to skin irritation.
2. organoleptic analysis's assessment
2.1 tested materials: cosmetics finished product.
2.2 experimenters: totally 30 people, male 10 people, female 20 people, at 21~49 years old age, meet experimenter and volunteer inclusion criteria.
2.3 appraisal procedures:
The sample of 70ul is applied to the back of the hand, mildly circle round and smear 8 times with another, then in (0~10 point of the mode of marking, mark is higher, represents texture, spreadability, flexibility, the absorbability, better with rear comfort sense of this product) evaluate successively sample texture, spreadability, flexibility, absorbability, use rear comfort sense.The sample of 70ul is applied to the back of the hand, mildly circles round and smear 8 times with another, until absorb completely, wait 1 minute, the thickness of assessment residual film, 0 refers to and does not feel residual film, 10 refer to the residual film of feeling very thick and heavy.
2.4 assessment results: be coated with rear comprehensive experimenter's scoring and add up, result as shown in Figure 1.
Assessment result shows, the texture of embodiment 1,2,3, spreadability, flexibility, absorbability, residual film, is significantly higher than reference examples with rear comfort sense.
3. water-resistance assessment
, be coated with the SPF measuring after 20 minutes with water-bath after using and carry out statistical before water-bath, as shown in Figure 2 according to the COLIPA way of recommendation by 11 professional test personnel.
Diagram shows, the sun-proof moisture-keeping composition of the embodiment of the present invention 1~3 not only water-resistance is good, and can also slightly promote spf value.Thereby can draw, the water-resistance of embodiment 1,2,3 is significantly higher than reference examples.
4. keratodermatitis water content test
According to QB/T 4256-2011 " cosmetics moisture-keeping efficacy evaluation guide ", the sun-proof moisture-keeping composition of embodiment 1~3 is carried out to the test of keratodermatitis water content, result shows, use after the sun-proof moisture-keeping composition of embodiment 1~3, keratodermatitis water content is higher than contrast, and its performance of keeping humidity is significantly better than contrast.
The sun-proof moisture-keeping composition of 4.1 each embodiment 1~3 and the common moisturiser that contains emulsifying agent are respectively looked for 9 experimenters, experimenter's feature: women, 38.5 ± 11.2 years old mean age.
4.2 tested positions: two forearms inner side, labelling is tested position everywhere, random assortment Wei Tuyang district 1, Tu Yang district 2, Tu Yang district 3 and check plot, the sun-proof moisture-keeping composition of embodiment 1~3 is smeared in Tu Yang district, and the common moisturiser that contains emulsifying agent is smeared in check plot
4.3 products are smeared dosage: application area: 3cm × 3cm, smears dosage: 2mg/cm2.
4.4 test indexs: keratodermatitis water content.
Test environment: temperature: 20-22 DEG C, relative humidity: 40-60%.
4.5 test procedures: experimenter sits quietly after 20min, (T0) keratodermatitis water content before testing tested position sample and smearing, then dosage is smeared tested material in accordance with regulations, Tu Yang district 1, Tu Yang district 2, Tu Yang district 3 and check plot are respectively at smearing 1 hour (T1) after tested material, and 4 hours (T2) and 8 hours (T3) tests tested position keratodermatitis water content.Before test, remove the residual product of skin surface (also using twice of dry napkin wiping skin before smearing sample and before the skin test of blank position) with dry napkin wiping.In process of the test, experimenter's forearm exposes, and is test mode and places, and keeps loosening.
Statistical method: if test data is normal distribution, adopt t inspection; If test data is nonnormal distribution, adopt rank test, two-tailed test, inspection level α=0.05.
Result as shown in Figure 3, is used after the sun-proof moisture-keeping composition of embodiment 1~3, and keratodermatitis water content is higher than contrast, and its performance of keeping humidity is significantly better than contrast.
Claims (9)
1. a sun-proof moisture-keeping composition, it is characterized in that being formed by the component of following percentage by weight: propylene glycol laurate/ethyl cellulose/propylene glycol isostearate 4~6%, Butyrospermum parkii fruit fat 1~2%, tocopherol acetas 0.2~0.3%, ethylhexyl methoxy cinnamate 2%, PAROSOL 1789 2.5%, isononyl isononanoate 3~4%, encircle five polydimethylsiloxane 2%, polydimethylsiloxane 1%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.3~0.4%, xanthan gum 0.1%, EDETATE SODIUM 0.02%, hyaluronate sodium 0.02%, butanediol 3~4%, glycerol 3~4%, glycerin polyether-263%, aminomethyl propanol/water pre-composition 0.15~0.2%, water/butanediol/Herba portulacae extract 3%, antibacterial 0.5%, water/glycerol/phenoxyethanol/beta glucan pre-composition 2%, deionized water surplus.
2. sun-proof moisture-keeping composition according to claim 1, it is characterized in that being formed by the component of following percentage by weight: propylene glycol laurate/ethyl cellulose/propylene glycol isostearate 5%, Butyrospermum parkii fruit fat 1%, tocopherol acetas 0.2%, ethylhexyl methoxy cinnamate 2%, PAROSOL 1789 2.5%, isononyl isononanoate 3%, encircle five polydimethylsiloxane 2%, polydimethylsiloxane 1%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.4%, xanthan gum 0.1%, EDETATE SODIUM 0.02%, hyaluronate sodium 0.02%, butanediol 4%, glycerol 3%, glycerin polyether-263%, aminomethyl propanol/water pre-composition 0.2%, water/butanediol/Herba portulacae extract pre-composition 3%, antibacterial 0.5%, water/glycerol/phenoxyethanol/beta glucan pre-composition 2%, deionized water surplus.
3. sun-proof moisture-keeping composition according to claim 1, is characterized in that: described antibacterial is caprylyl glycol/1,2-hexanediol/methyl-benzyl alcohol pre-composition.
4. sun-proof moisture-keeping composition according to claim 3, is characterized in that: described caprylyl glycol/1, in 2-hexanediol/methyl-benzyl alcohol pre-composition, each composition weight ratio is: caprylyl glycol 50%, methyl-benzyl alcohol 10~25%, 1,2-hexanediol 10~25%.
5. sun-proof moisture-keeping composition according to claim 1, is characterized in that: in described aminomethyl propanol/water pre-composition, the mass ratio of aminomethyl propanol and water is 19:1.
6. sun-proof moisture-keeping composition according to claim 1, is characterized in that: in described water/butanediol/Herba portulacae extract pre-composition, each composition weight ratio is: water 69.4~69.8, butanediol 30%, Herba portulacae extract 0.2~0.6%.。
7. sun-proof moisture-keeping composition according to claim 1, it is characterized in that: in described water/glycerol/phenoxyethanol/beta glucan pre-composition, each composition weight ratio is: water 79~79.4%, glycerol 20%, phenoxyethanol 0.4%, beta glucan 0.2~0.6%.
8. the preparation method of sun-proof moisture-keeping composition described in claim 1 to 7 any one, its step is as follows:
(1) by propylene glycol laurate/ethyl cellulose/propylene glycol isostearate, isononyl isononanoate, tocopherol acetas, ethylhexyl methoxy cinnamate, PAROSOL 1789, Butyrospermum parkii fruit fat, ring five polydimethylsiloxane, polydimethylsiloxane premixing evenly and be heated to 80~82 DEG C, form oil phase gel;
(2) by deionized water, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, xanthan gum, EDETATE SODIUM, hyaluronate sodium, butanediol, glycerol, glycerin polyether-26 mix homogeneously, and be warming up to 80~82 DEG C; Add aminomethyl propanol/water pre-composition to stir, form gel aqueous phase;
(3), under stirring, the oil phase gel that step (1) is obtained evenly adds in the gel aqueous phase that step (2) obtains, and homogenizing;
(4) stir and be cooled to 45 DEG C when following, add water/butanediol/Herba portulacae extract pre-composition, antibacterial, water/glycerol/phenoxyethanol/beta glucan pre-composition, stir.
9. method according to claim 8, is characterized in that: in described step (3), the speed of stirring is 600~700rpm.
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Cited By (11)
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CN104367516A (en) * | 2014-11-24 | 2015-02-25 | 广州神采化妆品有限公司 | Mild eye and lip cleansing gel and preparation method thereof |
CN104382758A (en) * | 2014-11-25 | 2015-03-04 | 广州神采化妆品有限公司 | Zero-added emulsion and preparation method thereof |
CN105434839A (en) * | 2015-05-28 | 2016-03-30 | 孟宏 | Externally applied skin-care composition and gel with effects of proofing radiation and repairing skin barrier and preparation method of externally applied skin-care composition and gel |
CN105496815A (en) * | 2015-12-21 | 2016-04-20 | 韩后化妆品有限公司 | Stable sun cream adopting double gel systems and preparation method of sun cream |
CN105520850A (en) * | 2016-01-29 | 2016-04-27 | 曼秀雷敦(中国)药业有限公司 | Sunscreen composition and preparation method and application thereof |
CN105616591A (en) * | 2016-01-28 | 2016-06-01 | 无限极(中国)有限公司 | Traditional Chinese medicine composition and preparation method and application thereof |
CN106691882A (en) * | 2016-12-05 | 2017-05-24 | 佛山市芊茹化妆品有限公司 | Plant-derived sunscreen composition and application thereof to makeup |
CN107174548A (en) * | 2017-06-20 | 2017-09-19 | 广东盛美化妆品有限公司 | A kind of micro emulsion spraying of the fat of fruit containing Butyrospermum parkii and preparation method thereof |
CN109260032A (en) * | 2018-09-18 | 2019-01-25 | 广州达人研选生物科技有限公司 | A kind of combined type easily tears mud film and its application method |
CN110339072A (en) * | 2019-07-29 | 2019-10-18 | 广州雅纯化妆品制造有限公司 | A kind of anti-sweat composition of waterproof and the sun-screening agent containing the composition |
CN110496065A (en) * | 2019-08-29 | 2019-11-26 | 陕西博鸿生物科技集团有限公司 | Moisturizing composition |
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CN104367516A (en) * | 2014-11-24 | 2015-02-25 | 广州神采化妆品有限公司 | Mild eye and lip cleansing gel and preparation method thereof |
CN104382758A (en) * | 2014-11-25 | 2015-03-04 | 广州神采化妆品有限公司 | Zero-added emulsion and preparation method thereof |
CN104382758B (en) * | 2014-11-25 | 2017-08-22 | 广州神采化妆品有限公司 | One kind zero adds emulsion and preparation method thereof |
CN105434839B (en) * | 2015-05-28 | 2019-02-05 | 孟宏 | Have effects that radiation protection and repair the external skin-care composition of skin barrier, gel and preparation method thereof |
CN105434839A (en) * | 2015-05-28 | 2016-03-30 | 孟宏 | Externally applied skin-care composition and gel with effects of proofing radiation and repairing skin barrier and preparation method of externally applied skin-care composition and gel |
CN105496815A (en) * | 2015-12-21 | 2016-04-20 | 韩后化妆品有限公司 | Stable sun cream adopting double gel systems and preparation method of sun cream |
CN105616591A (en) * | 2016-01-28 | 2016-06-01 | 无限极(中国)有限公司 | Traditional Chinese medicine composition and preparation method and application thereof |
CN105520850A (en) * | 2016-01-29 | 2016-04-27 | 曼秀雷敦(中国)药业有限公司 | Sunscreen composition and preparation method and application thereof |
CN106691882A (en) * | 2016-12-05 | 2017-05-24 | 佛山市芊茹化妆品有限公司 | Plant-derived sunscreen composition and application thereof to makeup |
CN107174548A (en) * | 2017-06-20 | 2017-09-19 | 广东盛美化妆品有限公司 | A kind of micro emulsion spraying of the fat of fruit containing Butyrospermum parkii and preparation method thereof |
CN109260032A (en) * | 2018-09-18 | 2019-01-25 | 广州达人研选生物科技有限公司 | A kind of combined type easily tears mud film and its application method |
CN110339072A (en) * | 2019-07-29 | 2019-10-18 | 广州雅纯化妆品制造有限公司 | A kind of anti-sweat composition of waterproof and the sun-screening agent containing the composition |
CN110496065A (en) * | 2019-08-29 | 2019-11-26 | 陕西博鸿生物科技集团有限公司 | Moisturizing composition |
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