CN103222685A - Method for using ethanol to prepare sheet carbonaceous heat sources for cigarettes - Google Patents
Method for using ethanol to prepare sheet carbonaceous heat sources for cigarettes Download PDFInfo
- Publication number
- CN103222685A CN103222685A CN2013101454435A CN201310145443A CN103222685A CN 103222685 A CN103222685 A CN 103222685A CN 2013101454435 A CN2013101454435 A CN 2013101454435A CN 201310145443 A CN201310145443 A CN 201310145443A CN 103222685 A CN103222685 A CN 103222685A
- Authority
- CN
- China
- Prior art keywords
- alginate
- carbon dust
- heat source
- ammonium
- potassium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 60
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 25
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 90
- 235000010408 potassium alginate Nutrition 0.000 claims abstract description 36
- 239000000737 potassium alginate Substances 0.000 claims abstract description 36
- MZYRDLHIWXQJCQ-YZOKENDUSA-L potassium alginate Chemical compound [K+].[K+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O MZYRDLHIWXQJCQ-YZOKENDUSA-L 0.000 claims abstract description 36
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 35
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 35
- 239000000661 sodium alginate Substances 0.000 claims abstract description 35
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 35
- 239000000728 ammonium alginate Substances 0.000 claims abstract description 34
- 235000010407 ammonium alginate Nutrition 0.000 claims abstract description 34
- KPGABFJTMYCRHJ-YZOKENDUSA-N ammonium alginate Chemical compound [NH4+].[NH4+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O KPGABFJTMYCRHJ-YZOKENDUSA-N 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000000203 mixture Substances 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 75
- 239000000463 material Substances 0.000 claims description 41
- 239000000428 dust Substances 0.000 claims description 40
- 238000002360 preparation method Methods 0.000 claims description 20
- 235000015110 jellies Nutrition 0.000 claims description 19
- 239000008274 jelly Substances 0.000 claims description 19
- 229920001131 Pulp (paper) Polymers 0.000 claims description 11
- 239000001913 cellulose Substances 0.000 claims description 11
- 229920002678 cellulose Polymers 0.000 claims description 11
- 239000011734 sodium Substances 0.000 claims description 11
- 241000208125 Nicotiana Species 0.000 claims description 8
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 3
- 239000003365 glass fiber Substances 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 description 11
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Abstract
The invention discloses a method for using ethanol to prepare sheet carbonaceous heat sources for cigarettes. The method comprises the following steps: mixing sodium alginate or ammonium alginate or potassium alginate with carbon powder and water, and stirring the mixture into a jelly-like substance, wherein the weight ratio of the sodium alginate or the ammonium alginate or the potassium alginate to carbon powder is 1:(5-45); then extruding the jelly-like substance into thin sheets, and intensively mixing the thin sheets with ethanol with a mass concentration of more than or equal to 66% to obtain a solidified substance; and rinsing and drying the solidified substance until the moisture content of the solidified substance reaches 10-20% to obtain the sheet carbonaceous heat sources for cigarettes. The method provided by the invention not only reduces the harm caused by inhalation of glass fiber into a human body, but also improves the flammability of carbonaceous heat sources, and has the characteristics of simple method, short production period, low cost and the like.
Description
Technical field
The invention belongs to the cigarette field, be specifically related to a kind of method of utilizing the cigarette that uses on the ethanol preparation low temperature cigarette to use sheet carbon heat source material.
Background technology
There are some researches show that nicotine and most tobacco flavor composition (300 ~ 500 ℃) at a lower temperature just can be transferred in the flue gas.If the cigarette temperature is reduced to (about 700 ℃ of tobacco burning-point) below 600 ℃, the multiple harmful components of flue gas can reduce significantly, and the influence that flavor component is subjected to is less relatively.Therefore, a kind of cigarette that uses carbon heat source to carry out the destructive distillation tobacco component is invented, wherein, what the Eclipse cigarette carbon heat source of R.J. Rainolds Tobacco CO. adopted is the mode of glass fibre parcel carbon-point, yet, carbon-point is that extruding forms, inner closely knit, need the ventilative glass fibre of outer parcel for forming thermal current, there is research to think, this particle promptly enables to be held back by filter tip material, but in processes such as packing, be adsorbed onto on the filter tip unavoidably, thereby cause sucking health risk, simultaneously, the closely knit also more very thin carbonaceous filamentary material difficult point of carbon-point is fired.
Summary of the invention
The objective of the invention is at above-mentioned deficiency, a kind of new cigarette sheet carbon heat source preparation methods is provided, adopt the carbon heat source material of this method preparation owing to when making carbon heat source, be deposited in together, itself is loose, there is the gap, thermal current can pass through smoothly, does not therefore need to adopt the glass fibre that is detrimental to health to wrap up.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of method of utilizing the ethanol preparation cigarette with sheet carbon heat source material, may further comprise the steps: sodium alginate or ammonium alginate or potassium alginate are mixed with carbon dust and water, stir the furnishing jelly, wherein the mass ratio of sodium alginate or ammonium alginate or potassium alginate and carbon dust is 1:5-45, then described jelly is squeezed into thin slice, the ethanol of described thin slice with mass concentration 〉=66% is fully contacted, obtain solidfied material; Described solidfied material makes water content reach 10-20% through rinsing, drying, promptly gets cigarette sheet carbon heat source material.
Preferably, the granularity of described carbon dust is 100 orders.
Preferably, described sheet thickness is 0.5-2.5mm.
Preferably, in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise the adding graphite powder, the mass ratio of described sodium alginate or ammonium alginate or potassium alginate and carbon dust and graphite powder is 1:5-45:0.4-3.6.Adding graphite powder is the heat transfer effect that is firing back carbon in order to improve, and reduces ignition temperature, reduces CO and generates.
Preferably, in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding CaCO
3, described sodium alginate or ammonium alginate or potassium alginate and carbon dust and CaCO
3Mass ratio be 1:5-45:0.1-2.Add CaCO
3Be to produce in order to help moulding and to reduce CO.
Preferably, in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise the adding wood pulp cellulose, the mass ratio of described sodium alginate or ammonium alginate or potassium alginate and carbon dust and wood pulp cellulose is 1:5-45:1-10.Adding wood pulp cellulose is in order to improve the processing characteristics of sheet carbon heat source.
Preferably, in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding Na
2CO
3The aqueous solution, described sodium alginate or ammonium alginate or potassium alginate and carbon dust and Na
2CO
3The mass ratio of solid is 1:5-45:0.05-1.Add Na
2CO
3Be in order to improve the combustibility of carbon dust after the moulding.
Further preferably, in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding graphite powder, CaCO
3, wood pulp cellulose and Na
2CO
3The aqueous solution, described sodium alginate or ammonium alginate or potassium alginate and carbon dust and graphite powder and CaCO
3With wood pulp cellulose and Na
2CO
3The mass ratio of solid is 1:5-45:0.4-3.6:0.1-2:1-10:0.05-1.
In order to improve igniting and sucking quality, in sodium alginate, ammonium alginate or potassium alginate and step that carbon dust and water mix, can also add tobacco powder or tobacco extract or essence.
In sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, the best sodium alginate or the mass ratio of ammonium alginate or potassium alginate and carbon dust and water are 1:20:100, this moment, sodium alginate or ammonium alginate or potassium alginate viscosity in aqueous solution were optimum, can stir the furnishing jelly with carbon dust at an easy rate.
The invention has the beneficial effects as follows:
When 1) preparing, jelly is when contacting with ethanol water, sodium alginate in the jelly, ammonium alginate or potassium alginate are separated out, form film, wrapped up carbon dust thereby form, the solidfied material of raw materials such as graphite powder, use this material, itself there is the space of nature in the latter made carbon heat source of chopping, and is flexible, is convenient to cigarette processing, and traditional carbon-point is extruding formation, inner closely knit, for forming the needs of ventilative and cigarette flexibility, skin will wrap up ventilative glass fibre, therefore the carbon heat source among the present invention no longer needs to wrap up with glass fibre, thereby has reduced glass fibre to suck human body and the harm that causes.
2) since sodium alginate or ammonium alginate or potassium alginate and raw materials such as carbon dust, graphite powder mix and parcel is to finish in ethanol water, belong to physical change, can not produce other harmful substances, and ethanol is volatile, can recycling, reduced production cost.
3) the inventive method is simple, and is with short production cycle, and cost is low.
The specific embodiment
The present invention is described in detail below in conjunction with embodiment.
Embodiment 1
A kind of cigarette sheet carbon heat source preparation methods, its step is as follows:
1) the 1g sodium alginate is mixed with 20g carbon dust (100 order) and 100g water, stir the furnishing jelly;
2) described jelly being squeezed into the thin slice that thickness is 2.5mm with the roller that rotates in opposite directions, is that 66% ethanol fully contacts (time that thin slice contacts with ethanol was at least 1 minute) with described thin slice and mass concentration, obtains solidfied material;
3) with described solidfied material through super-dry, make water content reach 10%, promptly get cigarette with sheet carbon heat source material.
Embodiment 2
A kind of cigarette sheet carbon heat source preparation methods, its step is as follows:
1) the 1g ammonium alginate is mixed with 5g carbon dust (100 order), 0.4g graphite powder and 60g water, stir the furnishing jelly;
2) described jelly is squeezed into the thin slice that thickness is 2mm with the roller that rotates in opposite directions, described thin slice is fully contacted with absolute ethyl alcohol, obtain solidfied material;
3) with the rinsing of described solidfied material process, drying, make water content reach 20%, promptly get cigarette sheet carbon heat source material.
Embodiment 3
A kind of cigarette sheet carbon heat source preparation methods, its step is as follows:
1) with 1g sodium alginate and 45g carbon dust (100 order), 0.1g CaCO
3Mix with 100g water, stir the furnishing jelly;
2) described jelly is squeezed into the thin slice that thickness is 1mm with the roller that rotates in opposite directions, described thin slice is fully contacted with 80% ethanol, obtain solidfied material;
3) with the rinsing of described solidfied material process, drying, make water content reach 15%, promptly get cigarette sheet carbon heat source material.
Embodiment 4
A kind of cigarette sheet carbon heat source preparation methods, its step is as follows:
1) the 1g potassium alginate is mixed with 30g carbon dust (100 order), 1g wood pulp cellulose and suitable quantity of water, stir the furnishing jelly;
2) described jelly is squeezed into the thin slice that thickness is 0.5mm with the roller that rotates in opposite directions, described thin slice is fully contacted with 95% ethanol, obtain solidfied material;
3) with the rinsing of described solidfied material process, drying, make water content reach 18%, promptly get cigarette sheet carbon heat source material.
Embodiment 5
A kind of cigarette sheet carbon heat source preparation methods, its step is as follows:
1) with 1g potassium alginate and 40g carbon dust (100 order), 0.05g Na
2CO
3Mix with suitable quantity of water, stir the furnishing jelly;
2) described jelly is squeezed into the thin slice that thickness is 1mm with the roller that rotates in opposite directions, described thin slice is fully contacted with 70% ethanol, obtain solidfied material;
3) with the rinsing of described solidfied material process, drying, make water content reach 12%, promptly get cigarette sheet carbon heat source material.
Embodiment 6
A kind of cigarette sheet carbon heat source preparation methods, its step is as follows:
1) with 1g potassium alginate and 10g carbon dust (100 order), 3.6g graphite powder, 2g CaCO
3, 10g wood pulp cellulose, 1g Na
2CO
3, 5g tobacco powder and suitable quantity of water mix, and stirs the furnishing jelly;
2) described jelly is squeezed into the thin slice that thickness is 0.8mm with the roller that rotates in opposite directions, described thin slice is fully contacted with 80% ethanol, obtain solidfied material;
3) with the rinsing of described solidfied material process, drying, make water content reach 10%, promptly get cigarette sheet carbon heat source material.
Claims (9)
1. method of utilizing the ethanol preparation cigarette with sheet carbon heat source material, it is characterized in that may further comprise the steps: sodium alginate or ammonium alginate or potassium alginate are mixed with carbon dust and water, stir the furnishing jelly, wherein the mass ratio of sodium alginate or ammonium alginate or potassium alginate and carbon dust is 1:5-45, then described jelly is squeezed into thin slice, the ethanol of described thin slice with mass concentration 〉=66% is fully contacted, obtain solidfied material; Described solidfied material makes water content reach 10-20% through rinsing, drying, promptly gets cigarette sheet carbon heat source material.
2. the method for utilizing the ethanol preparation cigarette with sheet carbon heat source material according to claim 1, it is characterized in that: the granularity of described carbon dust is 100 orders.
3. the method for utilizing the ethanol preparation cigarette with sheet carbon heat source material according to claim 1, it is characterized in that: described sheet thickness is 0.5-2.5mm.
4. according to each described method of utilizing the ethanol preparation cigarette with sheet carbon heat source material among the claim 1-3, it is characterized in that: in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise the adding graphite powder, the mass ratio of described sodium alginate or ammonium alginate or potassium alginate and carbon dust and graphite powder is 1:5-45:0.4-3.6.
5. according to each described method of utilizing the ethanol preparation cigarette with sheet carbon heat source material among the claim 1-3, it is characterized in that: in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding CaCO
3, described sodium alginate or ammonium alginate or potassium alginate and carbon dust and CaCO
3Mass ratio be 1:5-45:0.1-2.
6. according to each described method of utilizing the ethanol preparation cigarette with sheet carbon heat source material among the claim 1-3, it is characterized in that: in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise the adding wood pulp cellulose, the mass ratio of described sodium alginate or ammonium alginate or potassium alginate and carbon dust and wood pulp cellulose is 1:5-45:1-10.
7. according to each described method of utilizing the ethanol preparation cigarette with sheet carbon heat source material among the claim 1-3, it is characterized in that: in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding Na
2CO
3The aqueous solution, described sodium alginate or ammonium alginate or potassium alginate and carbon dust and Na
2CO
3The mass ratio of solid is 1:5-45:0.05-1.
8. according to each described method of utilizing the ethanol preparation cigarette with sheet carbon heat source material among the claim 1-3, it is characterized in that: in sodium alginate or ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding graphite powder, CaCO
3, wood pulp cellulose and Na
2CO
3The aqueous solution, described sodium alginate or ammonium alginate or potassium alginate and carbon dust and graphite powder and CaCO
3With wood pulp cellulose and Na
2CO
3The mass ratio of solid is 1:5-45:0.4-3.6:0.1-2:1-10:0.05-1.
9. the method for utilizing the ethanol preparation cigarette with sheet carbon heat source material according to claim 8, it is characterized in that: in sodium alginate, ammonium alginate or potassium alginate and step that carbon dust and water mix, also comprise adding tobacco powder or tobacco extract or essence.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310145443.5A CN103222685B (en) | 2013-04-24 | 2013-04-24 | Method for using ethanol to prepare sheet carbonaceous heat sources for cigarettes |
| PCT/CN2013/088343 WO2014173130A1 (en) | 2013-04-24 | 2013-12-02 | Method for preparing carbonaceous heat source materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310145443.5A CN103222685B (en) | 2013-04-24 | 2013-04-24 | Method for using ethanol to prepare sheet carbonaceous heat sources for cigarettes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103222685A true CN103222685A (en) | 2013-07-31 |
| CN103222685B CN103222685B (en) | 2014-04-30 |
Family
ID=48833515
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310145443.5A Active CN103222685B (en) | 2013-04-24 | 2013-04-24 | Method for using ethanol to prepare sheet carbonaceous heat sources for cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103222685B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014173130A1 (en) * | 2013-04-24 | 2014-10-30 | 湖北中烟工业有限责任公司 | Method for preparing carbonaceous heat source materials |
| CN105029708A (en) * | 2015-06-16 | 2015-11-11 | 安徽中烟工业有限责任公司 | Ash-dropping-resistant carbon heat source |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2907686A (en) * | 1954-12-23 | 1959-10-06 | Henry I Siegel | Cigarette substitute and method |
| US3258015A (en) * | 1964-02-04 | 1966-06-28 | Battelle Memorial Institute | Smoking device |
| JPS56131379A (en) * | 1979-11-16 | 1981-10-14 | Imuperiaru Guruupu Ltd | Smoking apparatus |
| CN1093556A (en) * | 1993-04-07 | 1994-10-19 | R·J·雷诺兹烟草公司 | Fuel element composition |
| CN1100453A (en) * | 1993-06-02 | 1995-03-22 | 菲利普莫里斯生产公司 | Imrpoved method for making a carbonaceous heat source containing metal oxide |
| US20070215168A1 (en) * | 2006-03-16 | 2007-09-20 | Banerjee Chandra K | Smoking article |
| CN101420876A (en) * | 2006-04-11 | 2009-04-29 | 日本烟草产业株式会社 | Carbonaceous heat source composition for non-combustible smoking article and non-combustible smoking article |
-
2013
- 2013-04-24 CN CN201310145443.5A patent/CN103222685B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2907686A (en) * | 1954-12-23 | 1959-10-06 | Henry I Siegel | Cigarette substitute and method |
| US3258015A (en) * | 1964-02-04 | 1966-06-28 | Battelle Memorial Institute | Smoking device |
| JPS56131379A (en) * | 1979-11-16 | 1981-10-14 | Imuperiaru Guruupu Ltd | Smoking apparatus |
| CN1093556A (en) * | 1993-04-07 | 1994-10-19 | R·J·雷诺兹烟草公司 | Fuel element composition |
| CN1100453A (en) * | 1993-06-02 | 1995-03-22 | 菲利普莫里斯生产公司 | Imrpoved method for making a carbonaceous heat source containing metal oxide |
| US20070215168A1 (en) * | 2006-03-16 | 2007-09-20 | Banerjee Chandra K | Smoking article |
| CN101420876A (en) * | 2006-04-11 | 2009-04-29 | 日本烟草产业株式会社 | Carbonaceous heat source composition for non-combustible smoking article and non-combustible smoking article |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014173130A1 (en) * | 2013-04-24 | 2014-10-30 | 湖北中烟工业有限责任公司 | Method for preparing carbonaceous heat source materials |
| CN105029708A (en) * | 2015-06-16 | 2015-11-11 | 安徽中烟工业有限责任公司 | Ash-dropping-resistant carbon heat source |
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| Publication number | Publication date |
|---|---|
| CN103222685B (en) | 2014-04-30 |
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