CN103084227A - Device for chemical experiment aiming at magnetic composite particle turbid liquid separation procedure - Google Patents

Device for chemical experiment aiming at magnetic composite particle turbid liquid separation procedure Download PDF

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Publication number
CN103084227A
CN103084227A CN2012105869781A CN201210586978A CN103084227A CN 103084227 A CN103084227 A CN 103084227A CN 2012105869781 A CN2012105869781 A CN 2012105869781A CN 201210586978 A CN201210586978 A CN 201210586978A CN 103084227 A CN103084227 A CN 103084227A
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China
Prior art keywords
permanent magnet
packaging bag
composite particle
non magnetic
magnetic composite
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CN2012105869781A
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Chinese (zh)
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CN103084227B (en
Inventor
李榕生
周汉坤
曾少林
任元龙
孙杰
李天华
干宁
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Ningbo University
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Ningbo University
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Abstract

The invention relates to a device for a chemical experiment aiming at a magnetic composite particle turbid liquid separation procedure, belonging to the field of an analysis test. The scheme aims at solving the problems that the existing commonly-used device aiming at the separation of magnetic composite particle turbid liquid in an analytical chemistry laboratory is too simple so as to influence the convenience of relative separation operation. According to the scheme, two sticking belts which are in a mutual sticking state and are easy to detach are connected with a pocket-shaped permanent magnet packaging bag containing a flexible material of a permanent magnet left to right from two sides; the pocket-shaped permanent magnet packaging bag is bundled and positioned on the outer surface of the side wall of a non-magnetic container and an outline shape of the attached forms looks like a waist bag; therefore, in a whole operation process of separating a capturing agent by a magnetic field, one high-tension-degree movement of utilizing a hand to take and pinch, and press and position the smooth permanent magnet by a relative analytic experiment operator is avoided; and with the adoption of the device applying the scheme, the relative analytic experiment operator can relatively easily carry out relative magnetic composite particle turbid liquid separation operation.

Description

Chemical experiment device for magnetic composite particle suspension segregation program
Technical field
The present invention relates to a kind of chemical experiment device for magnetic composite particle suspension segregation program, belong to the analytical test field.
Background technology
In the analytical test experimental work, for the water analysis object, with micron order or nano level magnetic composite particle trapping agent absorption object, then separate with permanent magnet the magnetic composite particle trapping agent that has adsorbed object, adsorbed from this through elution program again the magnetic composite particle trapping agent of object and isolated object, for Instrumental Analysis sample introduction thereafter, this is the standby sample means of a kind of very efficient Instrumental Analysis among at present flourish.
Described standby sample means can also be expressed as the pre-treatment means.
The standby sample means of described Instrumental Analysis take analytical test as purpose only relate to tens of milligrams usually to micron order or the nano level magnetic composite particle trapping agent of number gram, and its volume of water analysis object that relates to also only has hundreds of milliliters usually to the amount of several liters.
micron order or nano level magnetic composite particle trapping agent are scattered among the water analysis object, form suspension, with the close non magnetic container that holds this suspension of permanent magnet, effect due to magnetic field, magnetic composite particle trapping agent in suspension carries its object that captures and moves, assembles to high magnetic field area together, and this moves, accumulation process continues approximately tens of seconds to the number minutes, this case institute problems of concern just appears at this trapping agent isolation operation link: situation about recognizing at present is, experiment and correlation analysis operating personnel are being affectedly bashful the naked permanent magnet without any additional equipment to remove to be adjacent to described non magnetic container with hand, always like this in whole trapping agent isolation operation process, at toppling over of thereafter remaining liquid, in the discharging operation process, also like this, namely, be affectedly bashful on the other hand, press permanent magnet, the described non magnetic container of another holds, carry out toppling over of remaining liquid with a kind of relatively nervous operating attitude, discharging operation.The normally hundreds of milliliters of described non magnetic container are to several glass beakers that rise capacity, comprise above-mentioned the whole trapping agent isolation operation process that remaining liquid topples over, equally be smooth glass and so on container wall on hard, smooth permanent magnet by being pressed in hand, carry out simultaneously described remaining liquid and topple over action, its operation tensity is apparent.If be engaged in for a long time the operation that such needs tighten one's nerve, so, it will cause to experiment and correlation analysis personnel's physical and mental health recessive infringement.
Therefore, how improving the simple operation of magnetic composite particle suspension segregation link in relevant chemical experiment, is a problem that merits attention.
Its research and development and the application in the analytical test field of related magnetic composite particle trapping agent as an example, can be 201210099400.3 Chinese invention patent application case referring to application number.
About its research and development and the application in the analytical test field of magnetic composite particle trapping agent, also can be referring to following paper information: Zhang S X, Niu H Y, Cai Y Q, et al.Barium alginate cagedFe 3O 4@C18magnetic nanoparticles for the pre-concentration of polycyclicaromatic hydrocarbons and phthalate esters from environmental watersamples[J] .Analytica Chimica Acta, 2010,665:167-175.
Summary of the invention
Technical problem to be solved by this invention is, for the present situation not easily of magnetic composite particle suspension segregation link operation in above-mentioned chemical experiment, research and develop a kind of magnetic composite particle suspension that is applicable to chemical laboratory that helps to address this problem and emanate and use device.
the present invention is by the described technical problem of following solution, this scheme provides a kind of chemical experiment device for magnetic composite particle suspension segregation program, this installs its construction package and comprises tubbiness, the non magnetic container of cup-shaped or ampuliform, described its material of non magnetic container is glass, pottery, plastics or stainless steel, and, tabular, block, strip, disc-shaped, cylindric, the permanent magnet of pie or ring-type, this permanent magnet is Nd-Fe-B permanent magnet or hard ferrite permanent magnet, emphasis is, the structure of this device also comprises the permanent magnet packaging bag of flexible material, this permanent magnet packaging bag is satchel or pocketed thing, offer on this permanent magnet packaging bag for the sack to the inner filling of this permanent magnet packaging bag permanent magnet, described permanent magnet is the inside that filling is installed in this permanent magnet packaging bag, and, article two, magic tape, the both sides of this permanent magnet packaging bag respectively connect a described magic tape, its position that is connected with the permanent magnet packaging bag of the described magic tape of each is a termination at this magic tape, the remainder of these two magic tapes like as two arms around filling the span of a man's arms on the sidewall outer surface of described non magnetic container, these two magic tapes and mutual sticking taking, described magic tape has another name called the glochild pull stap, mutually sticking these two magic tapes of taking its pull strength and cause described permanent magnet packaging bag to be close on the sidewall outer surface of this non magnetic container, one of function of these two magic tapes is that described permanent magnet packaging bag is positioned on the sidewall outer surface of this non magnetic container together with its content constraint, two of the function of these two magic tapes is to give this apparatus structure dismounting mobility convenient to both, attach around ground these two magic tapes be installed on described non magnetic container side wall outer surface together with its overall profile shape of described permanent magnet packaging bag that combines with these two magic tapes like purse, this permanent magnet packaging bag can sticking taken the releasing of its state and removed from non magnetic container side wall outer surface in the lump with these two magic tapes along with described together with its content.
Itself art-recognized meanings of described flexible material one word is known.
The flexible material that can be selected for the described permanent magnet packaging bag of preparation is of a great variety, can be selected arbitrarily as required.Related flexible material market is on sale.
Itself art-recognized meanings of described magic tape one word is known for the manufacturing professional of magic tape.
Preferred magic tape is to have the flexible stretch sticking cingulum of degree of tightness.It is on sale that this has the flexible stretch sticking cingulum of degree of tightness market.Described degree of tightness elasticity is optional.
Described permanent magnet can be the permanent magnet of cited any shape, and its direction of magnetization can be any selected direction of magnetization, and its material can be any in Nd-Fe-B permanent magnet or hard ferrite permanent magnet.
Described non magnetic container can be the non magnetic container of cited any material, and described non magnetic container can be the non magnetic container of cited any shape, and still, preferably this non magnetic container is glass beaker.
For reaching better this case target, can also install rubber membrane or application elastic coating layer attaching of this permanent magnet packaging bag on that face of non magnetic container, this rubber membrane or elastic coating layer thickness between 0.5 millimeter and 3.0 millimeters, the function of this rubber membrane or elastic coating layer is to increase frictional resistance and contain by this its sliding transfer of permanent magnet packaging bag.
The material markets such as related rubber membrane and elastic coating are on sale.
The described non magnetic word of this case refers to its material does not here have serious obstruction for penetrating of magnetic field, rather than says that its material is to the response of magnetic field without any magnitude.
The sack of permanent magnet packaging bag can take various ways to seal, described sealing mode for example: slide fastener sealing mode, sticking sealing mode or the hasp sealing mode of taking.
Its assembly of this device of this case can also comprise some annexes, described annex for example: be used for to observe the Special illuminating light of magnetic trapping agent absorption running process terminal point, as shot-light etc.; Described annex is also for example: be used for determining the Chronograph timepiece of magnetic trapping agent absorption running process terminal point, as timer clock etc.; Described annex is more for example: the glass bar that uses with the liquid cooperation that inclines etc.; Described annex is optional.
Advantage of the present invention is, mutually stickingly take two magic tapes that state is easy to disassemble and permanent magnet is fettered in the lump together with the packaging bag of the pocketed of its flexible material be positioned on non magnetic container side wall outer surface with it, its profile shape that adheres to form is like purse, so, in the whole operating process with magnetic field segregation trapping agent, exempted experiment and correlation analysis operating personnel and be affectedly bashful, pressed the smooth higher action of a kind of like this tensity of permanent magnet in location with hand; Use this case device, experiment and correlation analysis personnel can relatively carry out magnetic composite particle suspension isolation operation with loosening.
Its structure of this case device and be easy to the dismounting; This structure is a kind of structure that facilitates independent assortment to use.
Description of drawings
Fig. 1 is the schematic diagram of this case apparatus structure.
In figure, 1,7 is respectively the different magic tape in two-strip structure position, the 2nd, the permanent magnet packaging bag of flexible material, the 3rd, permanent magnet, the 4th, non magnetic container, the 5th, slide fastener, the 6th, the pull head of slide fastener, two of the left and right in figure arrow are indicated two of left and right magic tape mutually to close up and are mutually glued the direction of action of taking.
The specific embodiment
in this case embodiment that Fig. 1 shows, this installs its construction package and comprises tubbiness, the non magnetic container 4 of cup-shaped or ampuliform, described non magnetic container 4 its materials are glass, pottery, plastics or stainless steel, and, tabular, block, strip, disc-shaped, cylindric, the permanent magnet 3 of pie or ring-type, this permanent magnet 3 is Nd-Fe-B permanent magnet or hard ferrite permanent magnet, emphasis is, the structure of this device also comprises the permanent magnet packaging bag 2 of flexible material, this permanent magnet packaging bag 2 is satchel or pocketed thing, offer on this permanent magnet packaging bag 2 for the sack to the inner filling permanent magnet 3 of this permanent magnet packaging bag 2, described permanent magnet 3 is the inside that filling is installed in this permanent magnet packaging bag 2, and, article two, magic tape, these two magic tapes are respectively magic tape 1 and magic tape 7, the both sides of this permanent magnet packaging bag 2 are connected with magic tape 1 and magic tape 7 respectively, magic tape 1 and magic tape 7 are all to be connected with permanent magnet packaging bag 2 with separately a termination, the remainder of magic tape 1 and magic tape 7 like as two arms around filling the span of a man's arms on the sidewall outer surface of described non magnetic container 4, magic tape 1 and magic tape 7 and mutual sticking taking, described magic tape has another name called the glochild pull stap, mutually the sticking magic tape 1 of taking and magic tape 7 its pull strength and cause described permanent magnet packaging bag 2 to be close on the sidewall outer surface of this non magnetic container 4, one of function of magic tape 1 and magic tape 7 is that described permanent magnet packaging bag 2 is positioned on the sidewall outer surface of this non magnetic container 4 together with its content constraint, two of the function of magic tape 1 and magic tape 7 is to give this apparatus structure dismounting mobility convenient to both, attach around ground the magic tape 1 be installed on described non magnetic container 4 sidewall outer surfaces and magic tape 7 together with described permanent magnet packaging bag 2 its overall profile shapes that combine with magic tape 1 and magic tape 7 like purse, this permanent magnet packaging bag 2 can sticking taken the releasing of its state and removed from non magnetic container 4 sidewall outer surfaces in the lump with magic tape 1 and magic tape 7 along with described together with its content.
This is a kind of apparatus structure that is easy to disassemble.
Itself art-recognized meanings of related flexible material one word is known.
Described magic tape market is on sale.
Implement related magic tape and preferably have the flexible stretch sticking cingulum of degree of tightness.Stretch sticking cingulum market is on sale.
Described permanent magnet 3 can be the permanent magnet of cited any shape, and its direction of magnetization can be any selected direction of magnetization, and its material can be any in Nd-Fe-B permanent magnet or hard ferrite permanent magnet.
Described non magnetic container 1 can be the non magnetic container of cited any material, and described non magnetic container 1 can be the non magnetic container of cited any shape, and still, preferably this non magnetic container 1 is glass beaker.The instant glass beaker of non magnetic container of showing in legend; Glass beaker is only an example.
Among enforcement, can also install rubber membrane or application elastic coating layer attaching of this permanent magnet packaging bag 2 on that face of non magnetic container 1, this rubber membrane or elastic coating layer thickness between 0.5 millimeter and 3.0 millimeters, any selected one-tenth-value thickness 1/10 in this thickness range is all the thickness enforcement value that this case allows, and the function of this rubber membrane or elastic coating layer is increase frictional resistance and contain by this permanent magnet packaging bag 2 its sliding transfers.
The material markets such as related rubber membrane and elastic coating are on sale.
Do not show this rubber layer or elastic coating layer in legend.
Described permanent magnet packaging bag can utilize any selected flexible material to make by techniques such as sewing, bonding, splicings.
The sack of permanent magnet packaging bag 2 can take various ways to seal, described sealing mode for example: slide fastener sealing mode, sticking sealing mode or the hasp sealing mode of taking.What show in legend is slide fastener sealing mode, and this is only an example; The sealing mode of described sack is not limited to this; Other sealing mode of described sack is not showed with legend.
This case device also is applicable to the indoor experiment of chemical experiment certainly with itself a small amount of preparation procedure of magnetic composite particle material, also is suitable for the isolation operation of the magnetic composite particle suspension under this situation.
The concrete enforcement of this case is not limited to this case accompanying drawing legend.

Claims (5)

1. for the chemical experiment device of magnetic composite particle suspension segregation program, this installs its construction package and comprises tubbiness, the non magnetic container of cup-shaped or ampuliform, described its material of non magnetic container is glass, pottery, plastics or stainless steel, and, tabular, block, strip, disc-shaped, cylindric, the permanent magnet of pie or ring-type, this permanent magnet is Nd-Fe-B permanent magnet or hard ferrite permanent magnet, it is characterized in that, the structure of this device also comprises the permanent magnet packaging bag of flexible material, this permanent magnet packaging bag is satchel or pocketed thing, offer on this permanent magnet packaging bag for the sack to the inner filling of this permanent magnet packaging bag permanent magnet, described permanent magnet is the inside that filling is installed in this permanent magnet packaging bag, and, article two, magic tape, the both sides of this permanent magnet packaging bag respectively connect a described magic tape, its position that is connected with the permanent magnet packaging bag of the described magic tape of each is a termination at this magic tape, the remainder of these two magic tapes like as two arms around filling the span of a man's arms on the sidewall outer surface of described non magnetic container, these two magic tapes and mutual sticking taking, described magic tape has another name called the glochild pull stap, mutually sticking these two magic tapes of taking its pull strength and cause described permanent magnet packaging bag to be close on the sidewall outer surface of this non magnetic container, one of function of these two magic tapes is that described permanent magnet packaging bag is positioned on the sidewall outer surface of this non magnetic container together with its content constraint, two of the function of these two magic tapes is to give this apparatus structure dismounting mobility convenient to both, attach around ground these two magic tapes be installed on described non magnetic container side wall outer surface together with its overall profile shape of described permanent magnet packaging bag that combines with these two magic tapes like purse, this permanent magnet packaging bag can sticking taken the releasing of its state and removed from non magnetic container side wall outer surface in the lump with these two magic tapes along with described together with its content.
2. the chemical experiment device for magnetic composite particle suspension segregation program according to claim 1, is characterized in that, these two magic tapes are all to have the flexible stretch sticking cingulum of degree of tightness.
3. the chemical experiment device for magnetic composite particle suspension segregation program according to claim 1, is characterized in that, this non magnetic container is glass beaker.
4. the chemical experiment device for magnetic composite particle suspension segregation program according to claim 1, it is characterized in that, be equiped with rubber membrane or the flexible dope layer of application attaching of this permanent magnet packaging bag on that face of non magnetic container, this rubber membrane or elastic coating layer thickness between 0.5 millimeter and 3.0 millimeters, the function of this rubber membrane or elastic coating layer is to increase frictional resistance and contain by this its sliding transfer of permanent magnet packaging bag.
5. the chemical experiment device for magnetic composite particle suspension segregation program according to claim 1, is characterized in that, the sealing mode of described its sack of permanent magnet packaging bag is slide fastener sealing mode, sticking sealing mode or the hasp sealing mode of taking.
CN201210586978.1A 2012-12-13 2012-12-13 Chemical experiment device for magnetic composite particle suspension isolation procedures Expired - Fee Related CN103084227B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112570050A (en) * 2019-09-27 2021-03-30 厦门大学 Fluid transportation control system and method

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US4793973A (en) * 1985-07-08 1988-12-27 Serono Diagnostic Partners Container for adding antibodies or antigens to a biological liquid
US5647994A (en) * 1993-06-21 1997-07-15 Labsystems Oy Method and apparatus for separating magnetic particles from a solution
WO2004011146A1 (en) * 2002-07-29 2004-02-05 Campbell Andrew T A device and method for manipulating magnetic particles
US7105357B1 (en) * 1998-05-27 2006-09-12 Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften E. V. Method and device for processing extremely small substance quantities
CN101010592A (en) * 2004-07-26 2007-08-01 拜奥默里克斯有限公司 Device and method for separating, mixing and concentrating magnetic particles with a fluid and use thereof in purification methods
CN101423973A (en) * 2008-10-21 2009-05-06 宁波大学 Experimental device applying to researching intervention of magnetic field conditional for complex crystallization
CN201345894Y (en) * 2008-12-12 2009-11-18 司徒家超 Self-service feeding air neckerchief
CN201375355Y (en) * 2009-04-02 2010-01-06 赵延 Heat insulating cup cover
CN201602296U (en) * 2009-12-31 2010-10-13 徐琨 Extensible water cup heat preservation bag
CN102362183A (en) * 2009-03-23 2012-02-22 皇家飞利浦电子股份有限公司 Manipulation of magnetic particles in a biological sample

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4793973A (en) * 1985-07-08 1988-12-27 Serono Diagnostic Partners Container for adding antibodies or antigens to a biological liquid
US5647994A (en) * 1993-06-21 1997-07-15 Labsystems Oy Method and apparatus for separating magnetic particles from a solution
US7105357B1 (en) * 1998-05-27 2006-09-12 Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften E. V. Method and device for processing extremely small substance quantities
WO2004011146A1 (en) * 2002-07-29 2004-02-05 Campbell Andrew T A device and method for manipulating magnetic particles
CN101010592A (en) * 2004-07-26 2007-08-01 拜奥默里克斯有限公司 Device and method for separating, mixing and concentrating magnetic particles with a fluid and use thereof in purification methods
CN101423973A (en) * 2008-10-21 2009-05-06 宁波大学 Experimental device applying to researching intervention of magnetic field conditional for complex crystallization
CN201345894Y (en) * 2008-12-12 2009-11-18 司徒家超 Self-service feeding air neckerchief
CN102362183A (en) * 2009-03-23 2012-02-22 皇家飞利浦电子股份有限公司 Manipulation of magnetic particles in a biological sample
CN201375355Y (en) * 2009-04-02 2010-01-06 赵延 Heat insulating cup cover
CN201602296U (en) * 2009-12-31 2010-10-13 徐琨 Extensible water cup heat preservation bag

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112570050A (en) * 2019-09-27 2021-03-30 厦门大学 Fluid transportation control system and method

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