CA2214155A1 - Method for determining true boiling point for crude oils - Google Patents

Method for determining true boiling point for crude oils

Info

Publication number
CA2214155A1
CA2214155A1 CA002214155A CA2214155A CA2214155A1 CA 2214155 A1 CA2214155 A1 CA 2214155A1 CA 002214155 A CA002214155 A CA 002214155A CA 2214155 A CA2214155 A CA 2214155A CA 2214155 A1 CA2214155 A1 CA 2214155A1
Authority
CA
Canada
Prior art keywords
true boiling
boiling point
crude oils
fraction
volume percent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002214155A
Other languages
French (fr)
Other versions
CA2214155C (en
Inventor
William Patrick Fitzgerald
James W. Fedora
Stilianos George Roussis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Oil Ltd
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2214155A1 publication Critical patent/CA2214155A1/en
Application granted granted Critical
Publication of CA2214155C publication Critical patent/CA2214155C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; viscous liquids; paints; inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; viscous liquids; paints; inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G01N33/2823—Oils, i.e. hydrocarbon liquids raw oil, drilling fluid or polyphasic mixtures
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/86—Signal analysis
    • G01N30/8624—Detection of slopes or peaks; baseline correction
    • G01N30/8644—Data segmentation, e.g. time windows

Abstract

This invention relates to a method for rapidly determining weight and volume percent true boiling point curves for crude oils and fractions thereof.
The method involves at least a partial separation of the crude oil or fraction into constituent chemical components, obtaining mass spectra of the chemical components, correlating retention time windows with boiling points for standard hydrocarbon mixtures, and converting the total ion current obtained from the mass spectra for selected components to weight and volume percent true boiling points by comparison with data obtained from a standard crude oil or fraction thereof.
CA002214155A 1996-09-12 1997-09-09 Method for determining true boiling point for crude oils Expired - Fee Related CA2214155C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/711,621 US5808180A (en) 1996-09-12 1996-09-12 Direct method for determination of true boiling point distillation profiles of crude oils by gas chromatography/mass spectrometry
US08/711,621 1996-09-12

Publications (2)

Publication Number Publication Date
CA2214155A1 true CA2214155A1 (en) 1998-03-12
CA2214155C CA2214155C (en) 2003-04-29

Family

ID=24858831

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002214155A Expired - Fee Related CA2214155C (en) 1996-09-12 1997-09-09 Method for determining true boiling point for crude oils

Country Status (7)

Country Link
US (1) US5808180A (en)
EP (1) EP0833155B1 (en)
JP (1) JPH10185875A (en)
AU (1) AU720346B2 (en)
CA (1) CA2214155C (en)
DE (1) DE69711308T2 (en)
SG (1) SG53056A1 (en)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE367580T1 (en) * 1998-09-01 2007-08-15 Analytical Controls Holding Ac METHOD AND APPARATUS FOR PREDICTING A DISTILLATION TEMPERATURE RANGE OF A COMPOUND CONTAINING HYDROCARBONS
US6711532B1 (en) 1998-09-01 2004-03-23 A.C. Analytical Controls Holding, B.V. Method and apparatus for predicting a distillation temperature range of a hydrocarbon-containing compound
FR2787576B1 (en) 1998-12-22 2001-01-12 Inst Francais Du Petrole INTEGRATED ANALYSIS METHOD AND DEVICE FOR THE CHARACTERIZATION OF HYDROCARBONS, BY SIMULATION OF DISTILLATION
US6598464B1 (en) * 1999-10-02 2003-07-29 Sergio Rossi Oil and contaminants analyzer
US20020121462A1 (en) * 2000-12-15 2002-09-05 Roussis Stilianos George Atmospheric equivalent temperature analysis
JP4551451B2 (en) * 2004-09-17 2010-09-29 ビーピー オイル インターナショナル リミテッド Portable device for analysis of refinery feedstock or refinery process products
US20060125826A1 (en) * 2004-12-10 2006-06-15 Lubkowitz Joaquin A Method and system for mass spectrometry and gas chromatographic data analysis
EP1946087A4 (en) * 2005-10-18 2010-02-10 Separation Systems Inc Method and system for chemical and physical characterization of complex samples
US8413484B2 (en) * 2005-10-18 2013-04-09 Separation Systems, Inc. Method and system for chemical and physical characterization of complex samples
US7598487B2 (en) * 2005-11-22 2009-10-06 Exxonmobil Research And Engineering Company Micro-hydrocarbon analysis
US9116104B2 (en) * 2006-03-22 2015-08-25 Agar Corporation, Ltd. Method and apparatus for detecting water in a fluid media
CA2659402C (en) * 2006-06-29 2015-02-03 Separation Systems, Inc. Method and system for chemical and physical characterization of complex samples
US10393723B2 (en) 2012-01-13 2019-08-27 Aspen Technology, Inc. Method to represent metal content in crude oils, reactor feedstocks, and reactor products
EP2788754B1 (en) * 2012-01-13 2019-07-03 Aspen Technology Inc. Method of characterizing chemical composition of crude oil for petroleum refinery processing
JP6123300B2 (en) * 2013-01-11 2017-05-10 株式会社島津製作所 Chromatographic data processor
JP6148468B2 (en) * 2013-01-11 2017-06-14 株式会社島津製作所 Data processing equipment for distillation gas chromatograph analysis
FR3008797A1 (en) * 2013-07-19 2015-01-23 Total Sa METHOD FOR IDENTIFYING COMPOUNDS OF AN ORGANIC MIXTURE AND KIT FOR IMPLEMENTING SAID METHOD
US10386345B2 (en) * 2015-03-19 2019-08-20 Ford Global Technologies, Llc Method and system for an oxygen sensor
CN106556653A (en) * 2016-08-30 2017-04-05 北京碧水源膜科技有限公司 Tributyl phosphate content assaying method in a kind of IsoparG
JP6887562B2 (en) 2017-04-24 2021-06-16 アスペン テクノロジー インコーポレイテッド Molecular characterization methods and systems
CN110470749A (en) * 2018-05-11 2019-11-19 中国石油化工股份有限公司 A method of the analysis thick aromatic hydrocarbons boiling range of carbon ten
KR102073856B1 (en) * 2018-05-28 2020-02-05 부경대학교 산학협력단 Method for simultaneous modeling and complexity reduction of bio-crudes for process simulation
US11232936B2 (en) * 2020-05-28 2022-01-25 Thermo Finnigan Llc Absolute quantitation of a target analyte using a mass spectrometer
CN114563518B (en) * 2020-11-27 2024-03-26 中国石油天然气集团有限公司 Method for tracing leakage of underground water oil products
CN116297635B (en) * 2023-03-16 2023-12-29 青岛锐丰源化工有限公司 Boiling point detection device of arene chromaticity

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US4507555A (en) * 1983-03-04 1985-03-26 Cherng Chang Parallel mass spectrometer
US4631687A (en) * 1983-11-03 1986-12-23 Rohrback Technology Corporation Method and apparatus for analysis employing multiple separation processes
IT1196389B (en) * 1984-12-28 1988-11-16 Erba Strumentazione METHOD AND EQUIPMENT FOR SIMULATED DISTILLATION BY GAS-CHROMATOGRAPHY WITH DIRECT NON-STEAM INJECTION
US4971915A (en) * 1987-05-15 1990-11-20 Applied Biosystems, Inc. Simulated distillation of petroleum residues by capillary SFC
US5121377A (en) * 1988-04-19 1992-06-09 Bose Corporation Error detection method and apparatus for reducing the number of errors generated when reading digital data stored on a recording medium such as film
US5119315A (en) * 1989-04-28 1992-06-02 Amoco Corporation Method of correlating a record of sample data with a record of reference data
JPH0750101B2 (en) * 1989-09-13 1995-05-31 株式会社コスモ総合研究所 Method and apparatus for measuring cetane number or cetane index
US5218529A (en) * 1990-07-30 1993-06-08 University Of Georgia Research Foundation, Inc. Neural network system and methods for analysis of organic materials and structures using spectral data
MY107650A (en) * 1990-10-12 1996-05-30 Exxon Res & Engineering Company Method of estimating property and / or composition data of a test sample
US5175430A (en) * 1991-05-17 1992-12-29 Meridian Instruments, Inc. Time-compressed chromatography in mass spectrometry
US5699269A (en) * 1995-06-23 1997-12-16 Exxon Research And Engineering Company Method for predicting chemical or physical properties of crude oils
US5600134A (en) * 1995-06-23 1997-02-04 Exxon Research And Engineering Company Method for preparing blend products
US5602755A (en) * 1995-06-23 1997-02-11 Exxon Research And Engineering Company Method for predicting chemical or physical properties of complex mixtures

Also Published As

Publication number Publication date
AU720346B2 (en) 2000-05-25
EP0833155B1 (en) 2002-03-27
US5808180A (en) 1998-09-15
JPH10185875A (en) 1998-07-14
SG53056A1 (en) 1998-09-28
DE69711308D1 (en) 2002-05-02
EP0833155A1 (en) 1998-04-01
DE69711308T2 (en) 2002-09-12
CA2214155C (en) 2003-04-29
AU3748797A (en) 1998-03-19

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